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    Preparation of cycloalkanones and cycloalkanols
    5.
    发明授权
    Preparation of cycloalkanones and cycloalkanols 失效
    环烷酮和环烷醇的制备

    公开(公告)号：US3923895A

    公开(公告)日：1975-12-02

    申请号：US14347271

    申请日：1971-05-14

    申请人： RHONE POULENC SA

    发明人： COSTANTINI MICHEL ,  CRENNE NOEL ,  JOUFFRET MICHEL ,  NOUVEL JACQUES

    IPC分类号： C07C29/132 ,  C07C29/50 ,  C07C45/33 ,  C07C45/53 ,  C07C49/30 ,  C07C35/08

    CPC分类号： C07C29/50 ,  C07C29/132 ,  C07C45/33 ,  C07C45/53 ,  C07C2601/14 ,  C07C35/08

    摘要： A process for the continuous preparation of a mixture of a cycloalkanone and cycloalkanol by oxidation of a cycloalkane in the liquid phase by means of a gas containing molecular oxygen, followed by heating the resulting solution of cycloalkyl hydroperoxide in the corresponding cycloalkane, at 80*-150*C. in the presence of a soluble chromium derivative as a catalyst, wherein at least a part of the heating of the hydroperoxide solution is carried out in the presence of a monoester or diester of ortho-phosphoric acid which is soluble in the reaction medium. The presence of the phosphate ester prevents buildup of a deposit on the walls of the dehydroperoxidation reactor.

    摘要翻译： 通过含有分子氧的气体在液相中氧化环烷烃连续制备环烷酮和环烷醇的混合物的方法，然后在80℃下将得到的环烷基氢过氧化物的溶液在相应的环烷烃中加热， 在可溶性铬衍生物作为催化剂的存在下，150℃，其中氢过氧化物溶液的加热的至少一部分在可溶于反应的正磷酸的单酯或二酯的存在下进行 中。 磷酸酯的存在防止沉积物沉积在脱氢过氧化反应器的壁上。

    Insecticidal and acaricidal phenylhydrazone derivatives
    6.
    发明授权
    Insecticidal and acaricidal phenylhydrazone derivatives 失效
    杀虫和杀螨苯乙酮衍生物

    公开(公告)号：US3917849A

    公开(公告)日：1975-11-04

    申请号：US46421274

    申请日：1974-04-25

    申请人： RHONE POULENC SA

    发明人： BOESCH ROGER

    IPC分类号： A01N9/20 ,  A01N9/24

    CPC分类号： C07C251/72

    摘要： Phenylhydrazone derivatives of the formula:
    WHEREIN R represents alkyl of 1 to 10 carbon atoms and Ar represents phenyl substituted by three atoms or radicals selected from halogen, alkyl or 1 to 4 carbon atoms, alkoxy of 1 to 4 carbon atoms, alkenyloxy of 2 to 4 carbon atoms and alkynyloxy of 2 to 4 carbon atoms, at least one of the substituents on the phenyl radical being an alkoxy, alkenyloxy or alkynyloxy radical, which are new compounds, possess insecticidal and acaricidal properties.

    摘要翻译： 下式的腙腙衍生物：Ar-NH-N = CR | Cl WHEREIN R表示1-10个碳原子的烷基，Ar表示被三个原子取代的苯基或选自卤素，烷基或1-4个碳原子的基团，烷氧基为1 至4个碳原子，2至4个碳原子的链烯氧基和2至4个碳原子的炔氧基，苯基上的至少一个取代基是作为新化合物的烷氧基，烯氧基或炔氧基，具有杀虫和杀螨性质 。

    Process for improving the adhesion of coating made of photoresistant polymers to surfaces of inorganic oxides
    7.
    发明授权
    Process for improving the adhesion of coating made of photoresistant polymers to surfaces of inorganic oxides 失效
    用于改善由光致抗蚀剂聚合物制成的涂层与无机氧化物表面的粘附性的方法

    公开(公告)号：US3911169A

    公开(公告)日：1975-10-07

    申请号：US38350773

    申请日：1973-07-30

    申请人： RHONE POULENC SA

    发明人： LESAICHERRE ANDRE ,  LINGUENHELD LOUIS

    IPC分类号： G03F7/16 ,  B32B9/00 ,  C09D5/00 ,  C09D183/00 ,  C09J5/00 ,  C09J5/02 ,  C09J11/00 ,  C09J183/00 ,  G03F7/00 ,  G03F7/075 ,  G03F7/09 ,  G03F7/11 ,  H01L21/027 ,  H01L21/312 ,  B44D1/092

    CPC分类号： H01L21/02222 ,  G03F7/0751 ,  H01L21/02282 ,  H01L21/02345 ,  H01L21/3125 ,  Y10S430/136

    摘要： The adhesion between inorganic oxides and photoresistant polymers is improved by, prior to contacting the oxide and the polymer, treating the oxide with (a) an aminosilane of the formulae R3SiNHR'' and R2Si(NHR'')2; or a polysilazane, with the exception of hexaalkyldisilazanes, having 0.8 to 3 organic groups per silicon atom, and having units of the formulae R3Si(NH)0.5, R2SiNH, RSi(NH)1.5 or Si(NH)2, in which formulae each R, which may be identical or different, represents hydrogen or an alkyl radical of 1 to 8 carbon atoms, an alkenyl radical of 2 to 4 carbon atoms, a cycloalkyl radical of 5 to 6 carbon atoms in the ring, an aryl radical of 6 to 8 carbon atoms, a benzyl radical, an alkoxy radical of 1 to 6 carbon atoms or an aryloxy radical of 6 to 8 carbon atoms; each R'' represents hydrogen or an alkyl radical of 1 to 4 carbon atoms; or (b) a cyclopolysiloxazane of the general formulae:

    IN WHICH FORMULAE EACH R'''', which may be identical or different, represents a methyl or phenyl radical, at least 40% of these radicals being methyl radicals; m represents an integer of 2 to 5 and the symbols n, which are identical, each is 1 to 2.

    摘要翻译： 在与氧化物和聚合物接触之前，通过用（a）式R3SiNHR'和R2Si（NHR'）2的氨基硅烷处理氧化物，改善了无机氧化物和光致抗蚀剂聚合物之间的粘合性。 或除了六烷基二硅氮烷之外的聚硅氮烷，每个硅原子具有0.8至3个有机基团，并且具有式R3Si（NH）0.5，R2SiNH，RSi（NH）1.5或Si（NH）2）的单元，其中各个 R可以相同或不同，表示氢或碳原子数1〜8的烷基，碳原子数2〜4的烯基，环中的碳原子数5〜6的环烷基，芳基6 至8个碳原子，苄基，1至6个碳原子的烷氧基或6至8个碳原子的芳氧基; 每个R'表示氢或1至4个碳原子的烷基; 或（b）通式为：R''R''R''R''R''R“'||| -Si-O-Si-NH--Si-O的环氧硅氧烷 -Si-NH-Si-O-Si-NH- ||||| R''mR''R''R''R''R''n，其中每个R“ 相同或不同，表示甲基或苯基，这些基团中至少40％是甲基; m表示2〜5的整数，相同的符号n分别为1〜2。