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公开(公告)号：US09353071B2
公开(公告)日：2016-05-31
申请号：US14432589
申请日：2013-10-04
发明人： Takashi Abe
IPC分类号： C07D275/03 , C07D275/02
CPC分类号： C07D275/03 , C07D275/02
摘要： An industrially preferred process for producing an isothiazole compound, particularly 3,4-dichloro-5-cyanoisothiazole, provides a safer industrial production process by avoiding the simultaneous use of an aprotic polar solvent such as N,N-dimethylformamide and chlorine. In addition, a production process which is economically preferred because an aprotic polar solvent, which is highly likely to become a part of waste, is not used.A process for producing an isothiazole compound represented by a general formula (3), wherein R is a cyano group or the like; and X is a chlorine atom or the like, which comprises heating a nitrile compound represented by a general formula (1), wherein R is as defined above, and sulfur, and then carrying out a reaction between the nitrile compound represented by the general formula (1), the sulfur and a halogen represented by a general formula (2), wherein X is as defined above.
摘要翻译： 用于制备异噻唑化合物，特别是3,4-二氯-5-氰基异噻唑的工业上优选的方法通过避免同时使用非质子极性溶剂如N，N-二甲基甲酰胺和氯而提供更安全的工业生产方法。 此外，不使用非常有可能成为废物的一部分的非质子极性溶剂，因此经济上优选的制造方法。 一种制备由通式（3）表示的异噻唑化合物的方法，其中R是氰基等; X是氯原子等，其包括加热由通式（1）表示的腈化合物，其中R定义如上，和硫，然后进行由通式 （1）表示的硫和由通式（2）表示的卤素，其中X如上所定义。
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公开(公告)号：US09774042B2
公开(公告)日：2017-09-26
申请号：US14784337
申请日：2014-04-11
IPC分类号： H01M4/90 , B01J31/22 , C08G69/42 , C08G73/06 , C08L79/04 , H01M4/88 , C08F226/06 , B01J31/20 , H01M8/1018
CPC分类号： H01M4/9083 , B01J31/22 , C08F226/06 , C08G69/42 , C08G73/0672 , C08L79/04 , H01M4/88 , H01M4/8882 , H01M4/9008 , H01M2008/1095
摘要： The present invention relates to a metal phthalocyanine polymer that includes a repeating structural unit obtained by amide bonding of a structural unit represented by the following general formula (1a) to a structural unit represented by the following general formula (2a): With general formula (1a), L is a divalent or trivalent metal ion belonging to Period 3 to Period 5 on the long-form periodic table. With general formula (2a), M is a divalent or trivalent metal ion belonging to Period 3 to Period 5 on the long-form periodic table.
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公开(公告)号：US20170197920A1
公开(公告)日：2017-07-13
申请号：US15314999
申请日：2015-06-24
发明人： Kentaro KAWAZOE , Kotaro YOSHIOKA
IPC分类号： C07D235/10 , C07C29/38 , C07C319/14 , C07D333/16 , C07C67/343 , C07C319/20 , C07D213/30
CPC分类号： C07D235/10 , C07B61/00 , C07C29/38 , C07C31/38 , C07C67/343 , C07C319/14 , C07C319/20 , C07C323/12 , C07D213/30 , C07D333/16
摘要： Problem to be SolvedIt is intended to provide an industrially preferable fluoroalkylating agent and use thereof.SolutionThe present invention provides a fluoroalkylating agent represented by the general formula (1) wherein R1 is a C1 to C8 fluoroalkyl group; R2 and R3 are each independently a C1 to C12 alkyl group or the like; Y1 to Y4 are each independently a hydrogen atom, a halogen atom, or the like; and X− is a monovalent anion. A compound of the general formula (3): R4—S—R1 having an introduced C1 to C8 fluoroalkyl group is easily obtained by reacting a compound of the general formula (2): R4—S—Z wherein R4 is a hydrocarbon group or the like; and Z is a leaving group, with the compound of the general formula (1).
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公开(公告)号：US09550724B2
公开(公告)日：2017-01-24
申请号：US14361313
申请日：2012-12-05
发明人： Minoru Ito , Akiko Ikumi
IPC分类号： C07C209/10 , C07C213/02 , C07C211/56 , C07C217/92
CPC分类号： C07C209/10 , C07C211/56 , C07C213/02 , C07C217/92
摘要： An inexpensive and convenient production method of diphenylamine compounds is provided, that can solve problems in the conventional technology such as decrease in reactivity, restriction of substituents, high temperature, high pressure, by-products or the like. Further, diphenylamine compounds useful as intermediates of medicine and agricultural chemicals are provided. Diphenylamine compounds are produced, represented by general formula (3): which is characterized by reacting aniline compounds represented by general formula (2): under the presence of base and ethers solvent, with 2,6-dichloronitrobenzene compound represented by general formula (1): and a diphenylamine compound represented by general formula (3).
摘要翻译： 本发明的目的是提供一种廉价且方便的二苯胺化合物的制造方法，其可以解决现有技术中的问题，如反应性的降低，取代基的限制，高温，高压，副产物或 喜欢。 此外，提供了可用作医药和农药的中间体的二苯胺化合物。 [溶液]通式（3）表示的二苯胺化合物的制造方法，其特征在于使通式（2）表示的苯胺化合物与碱式醚类溶剂与醚类溶剂的存在下，与2,6-二氯硝基苯化合物 通式（1）和由通式（3）表示的二苯胺化合物。
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公开(公告)号：US20160194268A1
公开(公告)日：2016-07-07
申请号：US14905645
申请日：2014-07-03
发明人： Shinki TAni , Minekazu Koga , Izumi Matsumoto
IPC分类号： C07C67/313
CPC分类号： C07C67/313 , C07C67/31 , C07C69/716 , C07C69/675
摘要： Provided is a method for producing an industrially useful ketomalonic acid compound such as ketomalinic acid diesters, or a hydrate thereof, by a method more favorable from an economic and environmental standpoint and from a safety standpoint. The present invention relates to a method involving reacting a malonic acid compound represented by general formula (1) (in the formula, The each Rs indicate an alkyl group, a cycloalkyl group, etc.) with chlorine dioxide to produce a ketomalonic acid compound represented by the general formula (2) (in the formula, R has the same meaning as above), or a hydrate thereof.
摘要翻译： 本发明提供从经济和环境的观点出发，从安全性的观点出发，通过更有利的方法制造工业上有用的酮咯酸化合物如酮三酸二酯或其水合物的方法。 本发明涉及使通式（1）表示的丙二酸化合物（式中，各Rs表示烷基，环烷基等）与二氧化氯反应，制备代表性的酮咯酸化合物 通式（2）（式中，R与上述相同）或其水合物。
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公开(公告)号：US20140288184A1
公开(公告)日：2014-09-25
申请号：US14360527
申请日：2012-11-19
发明人： Shunichirou Fukumoto , Daisuke Shikama , Toshihiro Nagata , Katsuya Kato , Kei Kawamoto , Masaaki Komatsu , Takeshi Matsuda , Seisuke Ito
CPC分类号： A01N37/52 , A01N37/18 , C07C259/14 , C07C2601/02 , C07C2601/04 , C07C2601/08 , C07C2601/14
摘要： The present invention provides a glyoxime derivative displaying excellent pesticidal effect or a salt thereof and a pesticide containing the same as an active ingredient. This pesticide is characterized by containing as an active ingredient, a glyoxime derivative expressed by the general formula [I] (in which X represents a cyano group or a carbamoyl group, R1 represents a C1˜C8 alkyl group, a C3˜C6 cycloalkyl C1˜C6 alkyl group, etc, and IV represents a hydrogen atom, a C1˜C8 alkyl group, a C3˜C6 cycloalkyl C1˜C6 alkyl group, etc.) or an agriculturally acceptable salt thereof.
摘要翻译： 本发明提供显示出优异的杀虫作用的乙二醛衍生物或其盐和含有活性成分的农药。 该农药的特征在于含有作为活性成分的由通式[I]表示的乙二醛衍生物（其中X表示氰基或氨基甲酰基，R1表示C1〜C8烷基，C3〜C6环烷基C1 -C6烷基等，IV表示氢原子，C1〜C8烷基，C3〜C6环烷基C1〜C6烷基等）或其农业上可接受的盐。
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7.发明申请ARYL (1H-1,2,4-TRIAZOL-1-YL) COMPOUND, AND PROCESS FOR PRODUCTION THEREOF 失效ARYL（1H-1,2,4-三唑-1-基）化合物及其生产方法公开(公告)号：US20130023666A1
公开(公告)日：2013-01-24
申请号：US13624107
申请日：2012-09-21
发明人： Kentaro KAWAZOE
IPC分类号： C07D249/14 , C07D249/08
CPC分类号： C07D249/08 , C07D249/14
摘要： A process for production of a (1H-1,2,4-triazol-1-yl)benzene compound represented the general formula (5) [wherein R is a C1 to C6 alkyl group or a cyclic C1 to C6 alkyl group; A1 is a hydrogen atom, an amino group, a mono(C1 to C6 alkyl)amino group or a di(C1 to C6 alkyl)amino group; and A2 is a halogen atom, a C1 to C6 alkyl group or a cyclic C1 to C6 alkyl group], which comprises reacting a triazole compound represented by the general formula (2) (wherein A1 has the same definition as given above) with a phenylboronic acid compound represented by the general formula (3) (wherein R and A2 have the same definitions as given above) or a phenylboroxine compound represented by the general formula (4) (wherein R and A2 have the same definitions as given above) in the presence of a copper catalyst.
摘要翻译： 代表通式（5）的（1H-1,2,4-三唑-1-基）苯化合物的制备方法[其中R是C1至C6烷基或环C1至C6烷基; A1是氢原子，氨基，单（C1-C6烷基）氨基或二（C1-C6烷基）氨基; 和A2是卤素原子，C1-C6烷基或环C1至C6烷基]，其包括使由通式（2）表示的三唑化合物（其中A1具有与上述相同的定义）与 由通式（3）表示的苯基硼酸化合物（其中R和A2具有与上述相同的定义）或由通式（4）表示的苯基环硼氧烷化合物（其中R和A2具有与上述相同的定义）在 铜催化剂的存在。
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公开(公告)号：US09499469B2
公开(公告)日：2016-11-22
申请号：US14905645
申请日：2014-07-03
发明人： Shinki Tani , Minekazu Koga , Izumi Matsumoto
IPC分类号： C07C69/66 , C07C67/313
CPC分类号： C07C67/313 , C07C67/31 , C07C69/716 , C07C69/675
摘要： Provided is a method for producing an industrially useful ketomalonic acid compound such as ketomalinic acid diesters, or a hydrate thereof, by a method more favorable from an economic and environmental standpoint and from a safety standpoint. The present invention relates to a method involving reacting a malonic acid compound represented by general formula (1) (in the formula, The each Rs indicate an alkyl group, a cycloalkyl group, etc.) with chlorine dioxide to produce a ketomalonic acid compound represented by the general formula (2) (in the formula, R has the same meaning as above), or a hydrate thereof.
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公开(公告)号：US20150291540A1
公开(公告)日：2015-10-15
申请号：US14432589
申请日：2013-10-04
发明人： Takashi Abe
IPC分类号： C07D275/03
CPC分类号： C07D275/03 , C07D275/02
摘要： An industrially preferred process for producing an isothiazole compound, particularly 3,4-dichloro-5-cyanoisothiazole, provides a safer industrial production process by avoiding the simultaneous use of an aprotic polar solvent such as N,N-dimethylformamide and chlorine. In addition, a production process which is economically preferred because an aprotic polar solvent, which is highly likely to become a part of waste, is not used.A process for producing an isothiazole compound represented by a general formula (3), wherein R is a cyano group or the like; and X is a chlorine atom or the like, which comprises heating a nitrile compound represented by a general formula (1), wherein R is as defined above, and sulfur, and then carrying out a reaction between the nitrile compound represented by the general formula (1), the sulfur and a halogen represented by a general formula (2), wherein X is as defined above.
摘要翻译： 用于制备异噻唑化合物，特别是3,4-二氯-5-氰基异噻唑的工业上优选的方法通过避免同时使用非质子极性溶剂如N，N-二甲基甲酰胺和氯而提供更安全的工业生产方法。 此外，不使用非常有可能成为废物的一部分的非质子极性溶剂，因此经济上优选的制造方法。 一种制备由通式（3）表示的异噻唑化合物的方法，其中R是氰基等; X是氯原子等，其包括加热由通式（1）表示的腈化合物，其中R定义如上，和硫，然后进行由通式 （1）表示的硫和由通式（2）表示的卤素，其中X如上所定义。
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公开(公告)号：US20150087833A1
公开(公告)日：2015-03-26
申请号：US14394438
申请日：2013-04-11
发明人： Kei Domon , Keiji Toriyabe , Yutaka Ogawa , Junichiro Bessho , Kei Kawamoto , Akira Watanabe , Masaaki Komatsu , Takeshi Matsuda , Seisuke Ito
IPC分类号： A01N31/16 , A01N37/34 , C07C317/32 , C07C323/12 , C07C323/25 , C07C323/18 , A01N37/10 , A01N37/38 , C07D231/12 , A01N43/56 , A01N43/50 , C07D233/64 , C07D249/08 , A01N43/653 , C07D277/26 , C07D213/34 , C07D239/26 , A01N43/78 , A01N43/40 , A01N43/54 , C07C317/22
CPC分类号： C07C321/28 , A01N31/16 , A01N33/20 , A01N37/10 , A01N37/32 , A01N37/34 , A01N37/38 , A01N39/00 , A01N41/10 , A01N41/12 , A01N43/08 , A01N43/40 , A01N43/50 , A01N43/54 , A01N43/56 , A01N43/653 , A01N43/78 , A01N47/02 , A01N47/48 , A01N55/00 , C07C317/14 , C07C317/22 , C07C317/32 , C07C317/46 , C07C323/12 , C07C323/18 , C07C323/20 , C07C323/25 , C07C323/62 , C07C331/10 , C07D213/34 , C07D231/12 , C07D233/64 , C07D239/26 , C07D249/08 , C07D277/26
摘要： An alkyl phenyl sulfide derivative represented by the general formula [I] or an agriculturally acceptable salt thereof, and a pest control agent containing the derivative or the salt as an active ingredient. [in the above formula, R1 is, for example, a C1˜C6 alkyl group which is mono- or poly-substituted with halogen atom; R2 is, for example, a halogen atom or a C1˜C6 alkyl group; R3 is, for example, a hydrogen atom or a halogen atom; and R4 is, for example, a hydrogen atom or a C1˜C12 alkyl group.] The derivative or the salt has an excellent pest control effect.
摘要翻译： 由通式[I]表示的烷基苯基硫醚衍生物或其农业上可接受的盐，以及含有该衍生物或盐作为有效成分的害虫控制剂。 [在上式中，R 1为例如被卤素原子单取代或多取代的C 1 -C 6烷基; R2是例如卤素原子或C1〜C6烷基; R3是例如氢原子或卤素原子; R4为例如氢原子或C1〜C12烷基。]该衍生物或盐具有优异的防虫效果。
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