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公开(公告)号：US10773253B2
公开(公告)日：2020-09-15
申请号：US16043094
申请日：2018-07-23
申请人： Paul L. Frattini , Leon Yengoyan
发明人： Paul L. Frattini , Leon Yengoyan
IPC分类号： B01J39/20 , C08F212/36 , C08F212/08 , C02F1/42 , C08F8/34
摘要： The invention provides chemical compounds for binding to a liquid phase cation having the formula R1—SO2—S—R2—SH, wherein R1 comprises a support molecule, such as a polymer, and R2 comprises an alkyl. The polymer may be a crosslinked, polystyrene divinylbenzene copolymer having a plurality of pendant benzyl groups to which the —SO2—S—R2—SH ligand is attached. The alkyl group may be ethyl or propyl. The chemical compound may be used to complex cation lead or mercury, in which the cation is complexed with mercapto-sulfur of the thio-sulfonyl moiety and the terminal mercaptan to form a heterocyclic ring-like geometry incorporating the cation. A method for removing cations from a liquid stream using the chemical compounds of the present invention is also provided.
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公开(公告)号：US20200023347A1
公开(公告)日：2020-01-23
申请号：US16043094
申请日：2018-07-23
申请人： Paul L. Frattini , Leon Yengoyan
发明人： Paul L. Frattini , Leon Yengoyan
IPC分类号： B01J39/20 , C08F212/36 , C08F212/08 , C08F8/34 , C02F1/42
摘要： The invention provides chemical compounds for binding to a liquid phase cation having the formula R1—SO2—S—R2—SH, wherein R1 comprises a support molecule, such as a polymer, and R2 comprises an alkyl. The polymer may be a crosslinked, polystyrene divinylbenzene copolymer having a plurality of pendant benzyl groups to which the —SO2—S—R2—SH ligand is attached. The alkyl group may be ethyl or propyl. The chemical compound may be used to complex cation lead or mercury, in which the cation is complexed with mercapto-sulfur of the thio-sulfonyl moiety and the terminal mercaptan to form a heterocyclic ring-like geometry incorporating the cation. A method for removing cations from a liquid stream using the chemical compounds of the present invention is also provided.
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公开(公告)号：US09214248B2
公开(公告)日：2015-12-15
申请号：US13303218
申请日：2011-11-23
申请人： Paul L. Frattini , Roger Howard Asay , Keith Paul Fruzzetti , Susan Elaine Garcia , Leon Yengoyan , Lisa Maxine Edwards
发明人： Paul L. Frattini , Roger Howard Asay , Keith Paul Fruzzetti , Susan Elaine Garcia , Leon Yengoyan , Lisa Maxine Edwards
摘要： The present invention relates to a method of capturing radioactive species in an aqueous solution and removing the radioactive species for disposal. The method includes the steps of providing a macroporous bead form sequestration resin including a sequestration ligand coupled to a sulfonic acid based polymer resin, subjecting the bead form sequestration resin to radioactive species contained in the aqueous solution to allow the bead form sequestration resin to capture the radioactive species; using an acid to lower a pH of the resin to release the radioactive species; and disposing the radioactive species in a radioactive storage facility.
摘要翻译： 本发明涉及一种在水溶液中捕获放射性物质并除去放射性物质进行处置的方法。 该方法包括以下步骤：提供大孔珠形隔离树脂，其包括耦合到基于磺酸的聚合物树脂的螯合配体，将珠形隔离树脂经受含在水溶液中的放射性物质以允许珠形隔离树脂捕获 放射性物种 使用酸降低树脂的pH以释放放射性物质; 并将放射性物质处置在放射性储存设施中。
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4.发明授权公开(公告)号：US08975340B2
公开(公告)日：2015-03-10
申请号：US13303201
申请日：2011-11-23
IPC分类号： C02F1/42 , B01J39/04 , B01J39/18 , B01J45/00 , G21F9/12 , B01J20/32 , C02F101/00 , C02F101/20 , C02F103/34
CPC分类号： B01J39/20 , B01J20/3219 , B01J20/3221 , B01J20/3248 , B01J20/3251 , B01J39/04 , B01J39/19 , B01J45/00 , C02F1/42 , C02F2001/425 , C02F2101/006 , C02F2101/20 , C02F2101/203 , C02F2103/34 , G21F9/12
摘要： An organic synthesis of materials to achieve removal of low molecular weight ionic species, such as transition metal ions including cobalt, iron, nickel, and zinc, from aqueous solutions. The synthesis includes the steps of providing a cation exchange resin, functionalizing the cation exchange resin using a chloride intermediate to form a sulfonyl chloride resin, and reacting a multi-amine based ligand with the sulfonyl chloride resin to form a sequestration resin. The synthesis further includes the steps of cooling the sequestration resin, and washing and drying the sequestration resin.
摘要翻译： 有机合成材料，以从水溶液中除去低分子量离子物质，如过渡金属离子，包括钴，铁，镍和锌。 该合成包括提供阳离子交换树脂的步骤，使用氯化物中间体官能化阳离子交换树脂以形成磺酰氯树脂，并使多胺基配体与磺酰氯树脂反应以形成螯合树脂。 该合成还包括冷却隔离树脂以及洗涤和干燥隔离树脂的步骤。
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5.发明申请公开(公告)号：US20120157556A1
公开(公告)日：2012-06-21
申请号：US13303201
申请日：2011-11-23
IPC分类号： B01J39/20
CPC分类号： B01J39/20 , B01J20/3219 , B01J20/3221 , B01J20/3248 , B01J20/3251 , B01J39/04 , B01J39/19 , B01J45/00 , C02F1/42 , C02F2001/425 , C02F2101/006 , C02F2101/20 , C02F2101/203 , C02F2103/34 , G21F9/12
摘要： An organic synthesis of materials to achieve removal of low molecular weight ionic species, such as transition metal ions including cobalt, iron, nickel, and zinc, from aqueous solutions. The synthesis includes the steps of providing a cation exchange resin, functionalizing the cation exchange resin using a chloride intermediate to form a sulfonyl chloride resin, and reacting a multi-amine based ligand with the sulfonyl chloride resin to form a sequestration resin. The synthesis further includes the steps of cooling the sequestration resin, and washing and drying the sequestration resin.
摘要翻译： 有机合成材料，以从水溶液中除去低分子量离子物质，如过渡金属离子，包括钴，铁，镍和锌。 该合成包括提供阳离子交换树脂的步骤，使用氯化物中间体官能化阳离子交换树脂以形成磺酰氯树脂，并使多胺基配体与磺酰氯树脂反应以形成螯合树脂。 该合成还包括冷却隔离树脂以及洗涤和干燥隔离树脂的步骤。
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6.发明申请公开(公告)号：US20120184796A1
公开(公告)日：2012-07-19
申请号：US13303218
申请日：2011-11-23
申请人： Paul L. Frattini , Roger Howard Asay , Keith Paul Fruzzetti , Susan Elaine Garcia , Leon Yengoyan , Lisa Maxine Edwards
发明人： Paul L. Frattini , Roger Howard Asay , Keith Paul Fruzzetti , Susan Elaine Garcia , Leon Yengoyan , Lisa Maxine Edwards
IPC分类号： G21F9/12
摘要： The present invention relates to a method of capturing radioactive species in an aqueous solution and removing the radioactive species for disposal. The method includes the steps of providing a macroporous bead form sequestration resin, subjecting the bead form sequestration resin to radioactive species contained in the aqueous solution to allow the bead form sequestration resin to capture the radioactive species; and disposing the radioactive species in a radioactive storage facility.
摘要翻译： 本发明涉及一种在水溶液中捕获放射性物质并除去放射性物质进行处置的方法。 该方法包括以下步骤：提供大孔珠形隔离树脂，将珠形隔离树脂经受水溶液中所含的放射性物质，以使珠粒密封树脂捕获放射性物质; 并将放射性物质处置在放射性储存设施中。
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公开(公告)号：US20060065530A1
公开(公告)日：2006-03-30
申请号：US11233353
申请日：2005-09-21
申请人： Leon Yengoyan , Paul Frattini
发明人： Leon Yengoyan , Paul Frattini
IPC分类号： C07K1/26 , G01N27/447 , G01N27/26
CPC分类号： G01N27/44747 , G01N27/44726
摘要： A novel class of capillary electrophoresis probes and a method of employing the same are described. The novel class of capillary electrophoresis probes are comprised of one or more vinylogous carboxylic acid compounds or their derivatives. In another aspect of the present invention, a method of detecting ions in water by capillary electrophoresis is provided wherein: water is introduced into a capillary filled with an electrolyte which contains UV absorbing species comprised of one or more vinylogous carboxylic acid compounds. An electric voltage is applied along the capillary to cause ions present in the water to move along the capillary and separate. The ions displace the UV absorbing species and are detected indirectly by a UV/visible light photometric detector.
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公开(公告)号：US20050045543A1
公开(公告)日：2005-03-03
申请号：US10920922
申请日：2004-08-17
申请人： Douglas Gjerde , Ronald Jones , Allen Burge , Christopher Hanna , Leon Yengoyan
发明人： Douglas Gjerde , Ronald Jones , Allen Burge , Christopher Hanna , Leon Yengoyan
CPC分类号： B01J20/285 , B01D15/22 , B01J20/286 , B01J2220/54 , B01J2220/58 , B01J2220/64 , B01L3/0275 , B01L2200/0631 , B82Y30/00 , G01N1/405 , G01N30/02 , G01N30/56 , G01N2035/1053 , B01D15/3804
摘要： The invention provides extraction columns for the purification of an analyte (e.g., a biological macromolecule, such as a peptide, protein or nucleic acid) from a sample solution, as well as methods for making and using such columns. The columns typically include a bed of extraction media positioned in the column between two frits. In some embodiments, the extraction columns employ modified pipette tips as column bodies. In some embodiments, the invention provides methods of storing columns in a wet state.
摘要翻译： 本发明提供了用于从样品溶液中纯化分析物（例如生物大分子，如肽，蛋白质或核酸）的提取柱，以及制备和使用这些色谱柱的方法。 柱通常包括位于两个玻璃料之间的柱中的提取介质床。 在一些实施方案中，提取柱使用改进的移液管尖作为柱体。 在一些实施方案中，本发明提供了在湿状态下储存塔的方法。
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