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1.发明授权Apparatuses, methods and compositions for ionization of samples and mass calibrants 有权用于电离样品和质量卡尺的装置，方法和组合物公开(公告)号：US07737395B2
公开(公告)日：2010-06-15
申请号：US11757369
申请日：2007-06-02
IPC分类号： B01D59/44
CPC分类号： H01J49/168 , H01J49/0009
摘要： The present invention provides, inter alia, apparatuses and methods for ionizing samples that are in gaseous phase or can be vaporized/sublimated. The samples include samples to be analyzed and mass calibrants that serve as standards. In addition, the present invention also provides calibrant formulations that release mass calibrants in a slow, controlled manner.
摘要翻译： 本发明尤其提供了用于电离处于气相或可蒸发/升华的样品的装置和方法。 样品包括要分析的样品和用作标准品的质量标准。 此外，本发明还提供了以缓慢且受控的方式释放大量校准物的校准剂制剂。
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2.发明申请Peptide derivatization method to increase fragmentation information from MS/MS spectra 有权肽衍生化方法从MS / MS谱增加碎片信息公开(公告)号：US20080026479A1
公开(公告)日：2008-01-31
申请号：US11494383
申请日：2006-07-27
IPC分类号： G01N33/00
CPC分类号： G01N33/6821 , G01N33/6848 , Y10T436/24
摘要： A method of facilitating analysis of a peptide in a mass spectrometer comprising derivatizing the C-terminus of the peptide with an amino acid residue via a reaction with a carbodiimide reagent, yielding a derivative peptide, ionizing the derivative peptide with a double charge, and fragmenting the ionized derivative peptide in a mass spectrometry system, wherein binary fragments of the ionized derivative each include a charge, facilitating sequence analysis of the peptide.
摘要翻译： 一种促进质谱分析肽的方法，包括通过与碳二亚胺试剂的反应将肽的C末端与氨基酸残基衍生化，产生衍生肽，以双电荷离子化衍生肽，并将其断裂 质谱系统中的离子化衍生肽，其中电离衍生物的二元片段各自包含电荷，便于肽的序列分析。
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公开(公告)号：US06608318B1
公开(公告)日：2003-08-19
申请号：US09629467
申请日：2000-07-31
IPC分类号： G21F502
CPC分类号： H01J27/02
摘要： The present invention relates to a mass spectrometer that includes an ionization source having a chamber for ionizing a fluid sample. The ionization chamber has surfaces to reduce the overall interaction with reactive samples. The inner surface walls of the ionization chamber may be formed from an inorganic conductive nitride or disulfide material or may be applied to a substrate as a coating. The invention also includes a method for reducing the interaction of a reactive analyte with the inner wall of the chamber by application or coating the inner wall of the chamber with an inert conductive material.
摘要翻译： 本发明涉及一种质谱仪，其包括具有用于离子化流体样品的室的电离源。 电离室具有减少与反应性样品的整体相互作用的表面。 电离室的内表面壁可以由无机导电氮化物或二硫化物材料形成，或者可以作为涂层施加到基材上。 本发明还包括通过用惰性导电材料施加或涂覆室的内壁来减少反应性分析物与室内壁的相互作用的方法。
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公开(公告)号：US06545271B1
公开(公告)日：2003-04-08
申请号：US09655758
申请日：2000-09-06
IPC分类号： B01D5944
CPC分类号： H01J49/4215 , H01J49/06
摘要： An apparatus and method for removing neutral noise from a quadrupole mass filter ion beam. A mask plate has a lobed aperture centered on a longitudinal axis and positioned between a quadrupole mass filter exit end and an ion detector. The mask plate operates to remove neutral atoms from the ion beam that may interfere with instrument sensitivities. The lobed aperture passes the ion beam with little loss of the ion beam intensity. The invention substantially maintains signal intensity and removes unwanted noise from a mass spectrometer.
摘要翻译： 一种用于从四极质量过滤器离子束去除中性噪声的装置和方法。 掩模板具有以纵向轴线为中心并且位于四极质量过滤器出口端和离子检测器之间的裂纹孔。 掩模板用于从离子束去除可能干扰仪器灵敏度的中性原子。 叶片的孔径通过离子束，几乎没有离子束强度的损失。 本发明基本上保持信号强度并从质谱仪中去除不想要的噪声。
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公开(公告)号：US4654449A
公开(公告)日：1987-03-31
申请号：US448112
申请日：1982-12-09
CPC分类号： C07C17/10
摘要： Hydrocarbons and other compounds are halogenated to halocarbon products by contact with a halocarbon in the presence of an acidic zeolite catalyst such as ZSM-5. The process is particularly useful for the halogenation of methane to form chemicals of higher value.
摘要翻译： 在酸性沸石催化剂如ZSM-5的存在下，碳氢化合物和其它化合物通过与卤代烃接触卤代卤代烃产物。 该方法特别适用于卤化甲烷以形成更高价值的化学品。
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公开(公告)号：US4395554A
公开(公告)日：1983-07-26
申请号：US369296
申请日：1982-04-16
IPC分类号： C07D213/06 , C07D213/08 , C07D213/09 , C07D213/16
CPC分类号： C07D213/06 , C07D213/08 , Y02P20/582
摘要： Alpha-picolines are produced by containing aniline or substituted anilines, such as alkyl-, cyclo alkyl-, halo- ; alkoxy- or substituted alkyl-anilines with a crystalline zeolite catalyst having a silica:alumina ratio of at least 12 and a constraint index of 1 to 12. ZSM-5 type catalysts are contacted at elevated temperature to yield alpha-picolines selectively.
摘要翻译： 通过含有苯胺或取代的苯胺如烷基 - ，环烷基 - ，卤代 - 烷氧基或取代的烷基苯胺与具有至少12的二氧化硅：氧化铝比的结晶沸石催化剂和1至12的约束指数。ZSM-5型催化剂在升高的温度下接触以选择性地产生α-吡啶甲酸。
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7.发明申请APPARATUSES, METHODS AND COMPOSITIONS FOR IONIZATION OF SAMPLES AND MASS CALIBRANTS 有权用于离子化和大量校准的装置，方法和组合物公开(公告)号：US20080067336A1
公开(公告)日：2008-03-20
申请号：US11757369
申请日：2007-06-02
CPC分类号： H01J49/168 , H01J49/0009
摘要： The present invention provides, inter alia, apparatuses and methods for ionizing samples that are in gaseous phase or can be vaporized/sublimated. The samples include samples to be analyzed and mass calibrants that serve as standards. In addition, the present invention also provides calibrant formulations that release mass calibrants in a slow, controlled manner.
摘要翻译： 本发明尤其提供了用于电离处于气相或可蒸发/升华的样品的装置和方法。 样品包括要分析的样品和用作标准品的质量标准。 此外，本发明还提供了以缓慢且受控的方式释放大量校准物的校准剂制剂。
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8.发明授权Peptide derivatization method to increase fragmentation information from MS/MS spectra 有权肽衍生化方法从MS / MS谱增加碎片信息公开(公告)号：US07838303B2
公开(公告)日：2010-11-23
申请号：US11494383
申请日：2006-07-27
IPC分类号： G01N24/00
CPC分类号： G01N33/6821 , G01N33/6848 , Y10T436/24
摘要： A method of facilitating analysis of a peptide in a mass spectrometer comprising derivatizing the C-terminus of the peptide with an amino acid residue via a reaction with a carbodiimide reagent, yielding a derivative peptide, ionizing the derivative peptide with a double charge, and fragmenting the ionized derivative peptide in a mass spectrometry system, wherein binary fragments of the ionized derivative each include a charge, facilitating sequence analysis of the peptide.
摘要翻译： 一种促进质谱分析肽的方法，包括通过与碳二亚胺试剂的反应将肽的C末端与氨基酸残基衍生化，产生衍生肽，以双电荷离子化衍生肽，并将其断裂 质谱系统中的离子化衍生肽，其中电离衍生物的二元片段各自包含电荷，便于肽的序列分析。
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公开(公告)号：US06974956B2
公开(公告)日：2005-12-13
申请号：US10810396
申请日：2004-03-25
申请人： Patrick D. Perkins
发明人： Patrick D. Perkins
摘要： The present invention relates to an ionization source having a chamber for ionizing a sample. The ionization chamber has surfaces to reduce the overall interaction with reactive samples. The inner surface walls of the ionization chamber or the ionization chamber may be formed from an inert super alloy. For instance, Inconel™ 625, Inconel™ 601 or Hastelloy® may comprise the ionization chamber or the surface walls of the ionization chamber. The invention also includes a method for reducing the interaction of a reactive analyte with an ion source.
摘要翻译： 本发明涉及一种具有用于离子化样品的室的电离源。 电离室具有减少与反应性样品的整体相互作用的表面。 电离室或电离室的内表面壁可以由惰性超级合金形成。 例如，Inconel TM 625，Inconel TM 601或Hastelloy可以包括电离室或电离室的表面壁。 本发明还包括减少反应性分析物与离子源的相互作用的方法。
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公开(公告)号：US4440668A
公开(公告)日：1984-04-03
申请号：US395403
申请日：1982-07-06
IPC分类号： B01J23/75 , B01J23/84 , B01J37/03 , C07C29/154 , C07C29/156 , B01J21/06 , B01J23/72 , B01J23/78
CPC分类号： C07C29/156 , B01J23/002 , B01J23/75 , B01J23/84 , C07C29/154 , B01J2523/00 , B01J37/03 , Y02P20/52
摘要： Synthesis gas is converted with high selectivity to higher alcohols over a three component oxide catalyst based on(i) copper(ii) a metal of Group VIA, VIIA or VIIIA(iii) a metal of Group IVA or VA.The preferred catalyst is based on copper, cobalt and zirconium with the first two components being formed by co-precipitation in the presence of the oxide third component.
摘要翻译： 基于（i）铜（ii）VIA，VIIA或VIIIA族的金属（iii）IVA或VA族的金属，合成气体以高分子量的醇被转化成三组分氧化物催化剂。 优选的催化剂是基于铜，钴和锆，其前两个组分通过在氧化物第三组分存在下共沉淀形成。
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