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1.发明申请公开(公告)号：US20130071553A1
公开(公告)日：2013-03-21
申请号：US13613889
申请日：2012-09-13
申请人： Naoto OHIRA , Ryuta Sugiura , Shohei Yokoyama , Miho Endo , Koji Kimura , Tsutomu Nanataki
发明人： Naoto OHIRA , Ryuta Sugiura , Shohei Yokoyama , Miho Endo , Koji Kimura , Tsutomu Nanataki
IPC分类号： B05D5/12
CPC分类号： H01M4/0471 , H01M4/1391 , H01M10/052 , Y02E60/122 , Y02P70/54
摘要： The present invention relates to a method for manufacturing cathode active material for a lithium secondary battery. The manufacturing method according to the present invention is characterized by including: (1) an intermediate generation process, wherein an intermediate which is powder or a shaped object containing the first material compound which is a compound of the transition metal other than lithium, which constitutes said lithium composite oxide, is generated, (2) a lithium source compound addition process, wherein the second material compound which is a lithium compound is added so that the second material compound in the shape of film may adhere to the surface of said intermediate, and (3) a sintering process, wherein lithium composite oxide is generated by sintering said intermediate in the state where said second material compound has adhered to its surface.
摘要翻译： 本发明涉及锂二次电池用正极活性物质的制造方法。 根据本发明的制造方法的特征在于包括：（1）中间生成工序，其中，作为粉末或成形体的中间体，其含有除锂以外的过渡金属的化合物的第一原料化合物，其构成 所述锂复合氧化物，（2）锂源化合物添加工序，其中添加作为锂化合物的第二材料化合物，使得膜形状的第二材料化合物可能粘附到所述中间体的表面， 和（3）烧结工艺，其中通过在所述第二材料化合物粘附到其表面的状态下烧结所述中间体而产生锂复合氧化物。
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公开(公告)号：US20120258369A1
公开(公告)日：2012-10-11
申请号：US13367813
申请日：2012-02-07
申请人： Shohei YOKOYAMA , Nobuyuki KOBAYASHI , Tsutomu NANATAKI , Koichi KONDO , Yukinobu YURA , Kei SATO
发明人： Shohei YOKOYAMA , Nobuyuki KOBAYASHI , Tsutomu NANATAKI , Koichi KONDO , Yukinobu YURA , Kei SATO
CPC分类号： H01M4/02 , H01M4/131 , H01M10/052 , H01M2004/021
摘要： The lithium secondary battery cathode active material having a layered rock salt structure is characterized in that the material is formed of a plurality of primary particles having a mean particle size of 0.01 to 5 μm, and contains secondary particles having a mean particle size of 1 to 100 μm and an aspect ratio, which is a ratio of long axis diameter to short axis diameter, of 1.0 or more and less than 2; and that the primary particles forming the secondary particles have a (003) plane orientation degree of 50% or higher.
摘要翻译： 具有层状岩盐结构的锂二次电池正极活性物质的特征在于，该材料由平均粒径为0.01〜5μm的多个一次粒子形成，并且含有平均粒径为1〜 100μm，纵轴直径与短轴直径的比例为1.0以上且小于2的纵横比; 并且形成二次粒子的一次粒子的（003）面取向度为50％以上。
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3.发明申请CATHODE ACTIVE MATERIAL PRECURSOR PARTICLE, CATHODE ACTIVE MATERIAL PARTICLE FOR LITHIUM SECONDARY BATTERY AND LITHIUM SECONDARY BATTERY 审中-公开阴极活性材料前体颗粒，阴极二次电池和锂二次电池的阴极活性材料颗粒公开(公告)号：US20120258365A1
公开(公告)日：2012-10-11
申请号：US13367827
申请日：2012-02-07
IPC分类号： H01M4/131 , H01M10/052
CPC分类号： H01M4/525 , C01G51/42 , C01G53/42 , C01P2002/52 , C01P2004/03 , C01P2004/54 , C01P2004/62 , C01P2006/40 , H01M4/131 , H01M10/052 , H01M2004/021 , Y10T428/2982
摘要： The invention provides lithium secondary battery cathode active material particle, which is formed as a secondary particle that is a mass of a plurality of single-crystal primary particles of a lithium-nickel-based complex oxide having a layered rock salt structure, wherein the primary particles have a mean particle size of 0.01 to 5 μm, and the secondary particle has an aspect ratio, which is a ratio of long axis diameter to short axis diameter, of 1.0 or more and less than 2 and a mean particle size of 1 to 100 μm, wherein the (003) planes of the second particle are substantially uniaxially oriented.
摘要翻译： 本发明提供了锂二次电池正极活性物质颗粒，其形成为具有层状岩盐结构的锂镍系复合氧化物的多个单晶一次粒子的质量的二次粒子，其中，初级 粒子的平均粒径为0.01〜5μm，二次粒子的长轴径与短轴直径的纵横比为1.0以上且小于2，平均粒径为1〜 100μm，其中第二颗粒的（003）面基本上是单向取向的。
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4.发明授权公开(公告)号：US08158255B2
公开(公告)日：2012-04-17
申请号：US12017567
申请日：2008-01-22
IPC分类号： B32B5/66
CPC分类号： C04B35/495 , C01G29/006 , C01G33/006 , C01G35/006 , C01P2002/34 , C01P2002/72 , C01P2004/03 , C04B35/475 , C04B35/493 , C04B2235/3201 , C04B2235/3203 , C04B2235/3206 , C04B2235/3251 , C04B2235/3279 , C04B2235/3284 , C04B2235/3291 , C04B2235/3298 , C04B2235/365 , C04B2235/5436 , C04B2235/5445 , C04B2235/6025 , C04B2235/762 , C04B2235/786 , C04B2235/79 , Y10T428/2982 , Y10T428/2991
摘要： A plate-like polycrystalline particle is produced by forming inorganic particles into a self-supported, sheet-like shaped body with a predetermined thickness, firing the shaped body, and crushing and classifying the fired shaped body by passing through a mesh having openings with a predetermined size. The inorganic particles are composed of an oxide having a perovskite structure and grow into crystal grains with an isotropic and polyhedral shape. Since grain growth in the thickness direction is limited and grain growth in the surface direction of the sheet is promoted, it is possible to obtain crystal grains having a high aspect ratio and a high degree of orientation. Therefore, in the plate-like polycrystalline particle, in most parts, the number of crystal grains present in the thickness direction of the particle at any one point is one, and a high aspect ratio and a high degree of orientation are achieved.
摘要翻译： 通过将无机粒子形成为具有预定厚度的自支撑的片状体，制成板状多晶粒子，烧成成形体，通过具有开口的网状物进行粉碎分级， 预定尺寸。 无机颗粒由具有钙钛矿结构的氧化物组成并且生长成具有各向同性和多面体形状的晶粒。 由于厚度方向的晶粒生长受到限制，并且促进了片材的表面方向的晶粒生长，因此可以获得具有高纵横比和高取向度的晶粒。 因此，在板状多晶粒子中，在大多数部分中，任何一点存在于粒子的厚度方向上的晶粒的数量为一个，并且实现高纵横比和高取向度。
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5.发明申请公开(公告)号：US20100159326A1
公开(公告)日：2010-06-24
申请号：US12644405
申请日：2009-12-22
IPC分类号： H01M4/525
CPC分类号： C01G53/42 , C01P2002/52 , C01P2002/74 , C01P2004/20 , C01P2004/54 , C01P2004/62 , H01M4/0471 , H01M4/131 , H01M4/525 , H01M10/0525 , H01M2004/021
摘要： An object of the present invention is to provide a lithium secondary battery which has improved capacity, durability, and rate characteristic as compared with conventional lithium secondary batteries. A plate-like particle or a film for a lithium secondary battery cathode active material is represented by the following general formula: General formula: Lip(Nix,Coy,Alz)O2 (wherein 0.9≦p≦1.3, 0.6
摘要翻译： 本发明的目的是提供一种与常规锂二次电池相比具有改进的容量，耐久性和速率特性的锂二次电池。 锂二次电池正极活性物质的板状颗粒或膜由以下通式表示：通式：Lip（Nix，Coy，Alz）O 2（其中0.9＆nlE; p＆nlE; 1.3,0.6
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公开(公告)号：US20090185971A1
公开(公告)日：2009-07-23
申请号：US12035491
申请日：2008-02-22
CPC分类号： C01G23/003 , C01G25/00 , C01G33/006 , C01G35/006 , C01P2002/34 , C01P2002/52 , C01P2002/72 , C01P2006/40 , C04B35/493 , C04B35/495 , C04B2235/3201 , C04B2235/3203 , C04B2235/3206 , C04B2235/3249 , C04B2235/3251 , C04B2235/3255 , C04B2235/3279 , C04B2235/36 , C04B2235/6025 , C04B2235/787 , C04B2235/80 , H01L41/1873 , H01L41/1876 , H01L41/43
摘要： A crystallographically-oriented ceramic including first regions, in which crystal nuclei remain and which contain a specific element in a predetermined concentration range and extend at least partially in a layered shape along a crystal plane, and second regions, which contain the specific element in a different concentration range from the first regions and extend at least partially in a layered shape along the crystal plane. The regions are alternately repeated, and a compositional distribution exists in a direction orthogonal to the crystal plane. In the first region, the concentration of Na is higher, the concentration of K is lower, the concentration of Nb is lower, and the concentration of Ta is higher than the second region, and in the second region, the concentration of Na is lower, the concentration of K is higher, the concentration of Nb is higher, and the concentration of Ta is lower than the first region.
摘要翻译： 一种晶体取向陶瓷，其包括第一区域，其中晶核保留并且包含预定浓度范围的特定元素并且沿着晶面至少部分地以层状形式延伸，并且在第一区域中含有特定元素的第二区域 与第一区域不同的浓度范围，并且至少部分地沿着晶面延伸成层叠形状。 这些区域交替重复，并且在与晶面正交的方向上存在组成分布。 在第一区域，Na的浓度较高，K浓度较低，Nb浓度较低，Ta浓度高于第二区域，第二区域的Na浓度较低 ，K浓度较高，Nb浓度较高，Ta浓度低于第一区域。
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公开(公告)号：US07528539B2
公开(公告)日：2009-05-05
申请号：US11145004
申请日：2005-06-02
申请人： Iwao Ohwada , Kei Sato , Nobuyuki Kobayashi , Shohei Yokoyama
发明人： Iwao Ohwada , Kei Sato , Nobuyuki Kobayashi , Shohei Yokoyama
IPC分类号： H01J1/46
摘要： An electron emitter includes an emitter layer formed of a dielectric material, an upper electrode, and a lower electrode. A drive voltage is applied between the upper electrode and the lower electrode, for emitting electrons. The upper electrode is formed of scale-like conductive particles on the upper surface of the emitter layer and has a plurality of opening portions. The surfaces of overhanging portions of the opening portions that face the emitter layer are apart from the emitter layer. The overhanging portions each have such a cross-sectional shape as to be acutely pointed toward the inner edge of the opening portion, or the tip end of the overhanging portion, so that lines of electric force concentrate at the inner edge.
摘要翻译： 电子发射器包括由电介质材料，上电极和下电极形成的发射极层。 在上电极和下电极之间施加驱动电压以发射电子。 上电极由发射极层的上表面上的鳞状导电粒子形成，具有多个开口部。 面向发射极层的开口部分的突出部分的表面与发射极层分开。 突出部分各自具有尖锐地指向开口部分的内边缘或突出部分的尖端的横截面形状，使得电力线集中在内边缘处。
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8.发明授权公开(公告)号：US08795898B2
公开(公告)日：2014-08-05
申请号：US12644394
申请日：2009-12-22
CPC分类号： H01M10/0525 , H01M4/131 , H01M4/485 , H01M2004/021
摘要： An object of the present invention is to provide a lithium secondary battery which has improved capacity, durability, and the other characteristic as compared with conventional lithium secondary batteries. A plate-like particle or a film for a lithium secondary battery cathode active material has a layered rock salt structure. The lithium ion gateway plane is oriented in parallel with a plate surface, which is a surface orthogonal to a thickness direction of the particle and thus exposed at the plate surface, a plurality of layers are stacked together in the thickness direction, and while the layers have the same crystal axis in the thickness direction, as for the plate surface direction perpendicular to the thickness direction, the layers have different crystal axes.
摘要翻译： 本发明的目的是提供一种与常规锂二次电池相比具有改善的容量，耐久性和其它特性的锂二次电池。 锂二次电池正极活性物质的板状粒子或膜具有层状岩盐结构。 锂离子网关平面与平板表面平行，板表面是与颗粒的厚度方向正交的表面，因此在板表面露出，多个层在厚度方向上堆叠在一起，而层 在厚度方向上具有相同的晶轴，对于与厚度方向垂直的板表面方向，这些层具有不同的晶轴。
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9.发明申请公开(公告)号：US20100159329A1
公开(公告)日：2010-06-24
申请号：US12644369
申请日：2009-12-22
CPC分类号： H01M4/485 , H01M4/131 , H01M10/0525 , H01M2004/021 , Y10T428/25 , Y10T428/2982
摘要： An object of the present invention is to improve the characteristics such as cell capacity, by raising the exposure of a crystal plane (a plane other than the (003) plane: e.g., (101) plane and (104) plane), through which lithium ions are favorably intercalated and deintercalated, to an electrolyte. A plate-like particle or a film for a lithium secondary battery cathode active material has a layered rock salt structure. A plane other than the (003) plane is oriented in parallel with the plate surface (a surface orthogonal to a thickness direction) and step-like structures are two-dimensionally formed along the plate surface.
摘要翻译： 本发明的目的是通过提高晶面（除（003）面以外的平面（例如（101）面和（104）面）来提高诸如电池容量的特性，通过该平面 锂离子有利地插入和脱嵌到电解质中。 锂二次电池正极活性物质的板状粒子或膜具有层状岩盐结构。 除了（003）面以外的平面与板表面（与厚度方向正交的表面）平行取向，并且沿着板表面二维地形成阶梯状结构。
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公开(公告)号：US20100119800A1
公开(公告)日：2010-05-13
申请号：US12612034
申请日：2009-11-04
CPC分类号： C04B35/475 , C04B35/495 , C04B35/62218 , C04B2235/3201 , C04B2235/3203 , C04B2235/3255 , C04B2235/3291 , C04B2235/3298 , C04B2235/5445 , C04B2235/6025 , C04B2235/6562 , C04B2235/6587 , C04B2235/77 , C04B2235/787 , C04B2235/79 , C04B2235/9623 , H01L41/1873 , H01L41/43
摘要： A ceramic sheet 20 is produced by a method in which inorganic particles including, as a main component, an oxide represented by general formula ABO3 and containing a volatile component are mixed such that the A/B ratio is 1.05 or more, the inorganic particles are formed into a self-supported planar shaped body with a thickness of 30 μm or less, and the shaped body is fired, without an inactive layer or with an inactive layer which does not substantially react with the shaped body and is disposed adjacent to the shaped body, at a temperature-rising rate of 30° C./min or more in a temperature range which is equal to or higher than a temperature at which the volatile component is volatilized.
摘要翻译： 通过以下方法制造陶瓷片20：将无机粒子作为主要成分，由通式ABO3表示的含有挥发性成分的氧化物混合，使得A / B比为1.05以上，无机粒子为 形成厚度为30μm以下的自支撑平面状体，并且成形体被烧制而没有无活性层或不与成形体基本上反应的不活泼层，并且与成形体 在等于或高于挥发性组分挥发的温度的温度范围内以30℃/分钟以上的升温速度进行。
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