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公开(公告)号：US08828288B2
公开(公告)日：2014-09-09
申请号：US13484322
申请日：2012-05-31
申请人： Qi Liao , Walter A. Scrivens , Philip T. Wilson , Darin L. Dotson , Hao Zhou
发明人： Qi Liao , Walter A. Scrivens , Philip T. Wilson , Darin L. Dotson , Hao Zhou
IPC分类号： B29C35/16
CPC分类号： C08K3/346 , C04B33/04 , C04B38/0045 , C04B2111/2046 , C04B2111/52 , C04B2235/349 , C04B2235/5454 , C04B2235/606 , C08J3/075 , C08J9/008 , C08J9/28 , C08J2201/0484 , C08J2305/00 , C08J2305/12 , C08J2329/04 , C08J2361/28 , C08J2389/00 , C08J2405/12 , C08K5/053 , C08L5/12 , C08L29/04 , Y10T442/2861 , C04B38/0054 , C04B38/0605
摘要： Disclosed are porous, low density nanoclay composites that exhibit highly homogeneous microcellular morphology and methods for forming the nanocomposites. The nanocomposites include a three-dimensional matrix having a non-lamellar, generally isotropic cellular structure with little or no macroscopic pores. The nanocomposites also include a gel that may be a noncovalently cross-linked, thermoreversible gel. The nanocomposites may include a binder and/or fibrous reinforcement materials. The nanocomposites may be formed according to a freeze-drying process in which ice crystal growth is controlled to prevent formation of macroscopic pores in the composite materials.
摘要翻译： 公开了多孔，低密度纳米粘土复合材料，其表现出高度均匀的微孔形态和形成纳米复合材料的方法。 纳米复合材料包括具有非层状，通常各向同性的细胞结构，具有很少或不具有宏观孔的三维基质。 纳米复合材料还包括可以是非共价交联的热可逆凝胶的凝胶。 纳米复合材料可以包括粘合剂和/或纤维增强材料。 可以根据冷冻干燥方法形成纳米复合材料，其中控制冰晶生长以防止在复合材料中形成宏观孔。
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公开(公告)号：US20120077015A1
公开(公告)日：2012-03-29
申请号：US12893030
申请日：2010-09-29
申请人： Hao Zhou , Walter A. Scrivens
发明人： Hao Zhou , Walter A. Scrivens
CPC分类号： B32B5/26 , B29C48/05 , B29C48/08 , B29C48/21 , Y10T428/249949 , Y10T428/249952
摘要： A nano-composite article containing a nanofiber layer and a supporting layer. The nanofiber layer has a first outer boundary adjacent the supporting layer, a second outer boundary on the side of the nanofiber layer opposite the supporting layer and an inner boundary located at the mid-point between the first outer boundary and the second outer boundary and parallel to the first outer boundary. The nanofiber layer contains a matrix and a plurality of nanofibers, where at least 70% of the nanofibers are bonded to other nanofibers. The supporting layer contains a thermoplastic polymer. The concentration of nanofibers is substantially uniform in the nanofiber layer from the inner boundary to the first boundary layer.
摘要翻译： 一种含纳米纤维层和支撑层的纳米复合制品。 纳米纤维层具有与支撑层相邻的第一外边界，在与支撑层相对的纳米纤维层侧的第二外边界和位于第一外边界和第二外边界之间的中点处的内边界，并且平行 到第一个外边界。 纳米纤维层包含基质和多个纳米纤维，其中至少70％的纳米纤维结合到其他纳米纤维上。 支撑层含有热塑性聚合物。 纳米纤维层从内边界到第一边界层的纳米纤维的浓度基本一致。
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公开(公告)号：US6121332A
公开(公告)日：2000-09-19
申请号：US322754
申请日：1999-05-28
CPC分类号： A61K8/498 , A61K8/042 , A61K8/345 , A61Q15/00 , A61K2800/262 , Y10S514/944
摘要： This invention relates to gelled compositions formed through the introduction of specific solvents to compositions comprising 2,4-O-(3,4-dimethylbenzylidene)-D-sorbitol. Such compositions provide excellent gelling for any number of potential applications, particularly where translucent gels are desired. In general, these compositions are formed by introducing heated solvents to the specific monobenzylidene sorbitol present in its solid form. The monobenzylidene sorbitol is preferably added in very low amounts to the target solvents in order to generate the desired gelling effect. A method of producing such gelled compositions is also provided.
摘要翻译： 本发明涉及通过将特定溶剂引入到包含2,4-O-（3,4-二甲基亚苄基）-D-山梨糖醇的组合物中而形成的凝胶组合物。 这样的组合物为任何数量的潜在应用提供优异的胶凝，特别是在需要半透明凝胶的情况下。 通常，这些组合物通过将加热的溶剂引入其固体形式存在的特定单亚苄基山梨糖醇中而形成。 优选将单亚苄基山梨糖醇以非常低的量加入到目标溶剂中以产生所需的胶凝效果。 还提供了生产这种凝胶组合物的方法。
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公开(公告)号：US20120076972A1
公开(公告)日：2012-03-29
申请号：US12893035
申请日：2010-09-29
申请人： Hao Zhou , Walter A. Scrivens
发明人： Hao Zhou , Walter A. Scrivens
CPC分类号： B82Y30/00 , B29C48/04 , B29C48/05 , B29C48/21 , B29C48/919 , B29K2313/00 , B29K2913/00 , B32B5/022 , B32B5/26 , D04H1/559 , D04H1/64 , Y10T428/23914
摘要： A nanofiber non-woven composite containing a nanofiber non-woven layer and a textile layer. The nanofiber non-woven layer has a first side and a second side and a plurality of nanofibers. At least 70% of the nanofibers are bonded to other nanofibers. The textile layer has a textile layer thickness and is located on the first side of the nanofiber non-woven layer. At least a portion of the nanofibers of the nanofiber non-woven layer are penetrated at least partially into the textile layer thickness.
摘要翻译： 一种含有纳米纤维无纺布层和织物层的纳米纤维无纺布复合材料。 纳米纤维无纺布层具有第一面和第二面以及多个纳米纤维。 至少70％的纳米纤维结合到其他纳米纤维上。 纺织层具有织物层厚度，并且位于纳米纤维无纺布层的第一面上。 纳米纤维无纺层的纳米纤维的至少一部分至少部分地渗入织物层的厚度。
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公开(公告)号：US20120074612A1
公开(公告)日：2012-03-29
申请号：US12893041
申请日：2010-09-29
申请人： Walter A. Scrivens , Hao Zhou
发明人： Walter A. Scrivens , Hao Zhou
IPC分类号： B29C51/04
CPC分类号： D04H1/413 , B29C47/0004 , B29C47/0014 , D01D5/082 , D04H1/541 , D04H1/544 , D04H1/549 , D04H1/55 , D04H3/005
摘要： A process for forming a nanofiber non-woven includes mixing a first and second thermoplastic polymer and a plurality of particles, then subjecting the mixture to elongational forces when the first and second polymers are in a softened condition forming nanofibers of the first polymer. Next, the mixture is brought to a condition where the temperature is below the softening temperature of the first polymer forming a first intermediate. The first intermediate is consolidated forming the second intermediate where at least 70% of the nanofibers are fused to other nanofibers. Next, at least a portion of the second polymer is removed and at least 50% of the particles are positioned adjacent a surface of the nanofibers.
摘要翻译： 形成纳米纤维无纺布的方法包括混合第一和第二热塑性聚合物和多个颗粒，然后当第一和第二聚合物处于形成第一聚合物的纳米纤维的软化状态时，对混合物进行拉伸力。 接下来，使混合物达到温度低于形成第一中间体的第一聚合物的软化温度的条件。 将第一中间体固结形成第二中间体，其中至少70％的纳米纤维与其它纳米纤维融合。 接下来，除去至少一部分第二聚合物，并且至少50％的颗粒位于纳米纤维的表面附近。
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公开(公告)号：US07262236B2
公开(公告)日：2007-08-28
申请号：US10831920
申请日：2004-04-26
申请人： Chunping Xie , Jiang Li , Lee Rieth , Jason Alan Smith , John D. Anderson , Shane M. Waybright , Brian M. Burkhart , Walter A. Scrivens
发明人： Chunping Xie , Jiang Li , Lee Rieth , Jason Alan Smith , John D. Anderson , Shane M. Waybright , Brian M. Burkhart , Walter A. Scrivens
IPC分类号： C08K5/15 , C07D323/04
CPC分类号： C07D319/06 , C07D493/04 , C08K5/0083 , C08K5/1575
摘要： An acetal-based composition useful as a nucleating, gelling, thickening or clarifying agent is disclosed. The composition may be synthesized or provided in many different forms, including multicarbon diacetals formed from carbohydrates. Once synthesized, the compound may be employed as an additive in a plastic composition, such as (for example) a polypropylene copolymer. One structure of such an acetal-based composition is provided by the formula: wherein: n is 0, 1 or 2; Ar1 and Ar2 are independently selected from substituted or unsubstituted aryl-containing groups; and R is selected from the group consisting of: alkenyls, alkyls, alkoxy, hydroxyl alkyls, and alkyl-halides.
摘要翻译： 公开了可用作成核剂，胶凝剂，增稠剂或澄清剂的基于缩醛的组合物。 组合物可以以许多不同形式合成或提供，包括由碳水化合物形成的多碳二缩醛。 一旦合成，该化合物可以用作塑料组合物中的添加剂，例如（例如）聚丙烯共聚物。 这种基于缩醛的组合物的一种结构由下式提供：其中：n为0,1或2; Ar 1和Ar 2独立地选自取代或未取代的含芳基; 并且R选自：烯基，烷基，烷氧基，羟基烷基和烷基卤化物。
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公开(公告)号：US5731474A
公开(公告)日：1998-03-24
申请号：US792518
申请日：1997-01-31
IPC分类号： C07D317/20 , C07D317/22 , C07C43/307
CPC分类号： C07D317/22
摘要： A method of making acetals is provided by condensing an aromatic aldehyde and a polyhydric alcohol having five or more hydroxyl groups in the presence of an acid catalyst, a hydrophobic organic liquid medium and a processing agent selected from dihydric, trihydric and tetrahydric alcohols.
摘要翻译： 通过在酸催化剂，疏水性有机液体介质和选自二元，三元和四元醇的加工剂的存在下，使芳族醛和具有五个或更多个羟基的多元醇缩合来提供缩醛的方法。
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公开(公告)号：US5310532A
公开(公告)日：1994-05-10
申请号：US896193
申请日：1992-06-10
CPC分类号： B82Y30/00 , B82Y40/00 , C01B31/0206 , C01B31/0213 , Y10S423/39 , Y10S977/845
摘要： A low-cost and facile method of purifying fullerenes to obtain a preparation enriched in a fullerene of selected molecular weight using activated carbon involves adding a fullerene mixture to the top end of a column comprising activated carbon, passing a solvent in which the selected molecular weight fullerene is soluble through the column, and recovering a fraction enriched in the selected molecular weight fullerene from the bottom end of the column. In addition to activated carbon, the column may further comprise silica gel, diatomaceous earth, or other materials which aid in column packing and eluent flow.
摘要翻译： 使用活性炭纯化富勒烯以获得富含选定分子量的富勒烯的制剂的低成本和容易的方法包括将富勒烯混合物加入到包含活性炭的柱的顶端，通过其中所选择的分子量 富勒烯可通过塔溶解，并从塔的底端回收富集所选择的分子量富勒烯的馏分。 除了活性炭之外，该柱还可以包括硅胶，硅藻土或其它有助于柱填充和洗脱液流动的材料。
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公开(公告)号：US20120077405A1
公开(公告)日：2012-03-29
申请号：US12893046
申请日：2010-09-29
申请人： Hao Zhou , Walter A. Scrivens
发明人： Hao Zhou , Walter A. Scrivens
CPC分类号： D01D5/34 , D01D5/00 , D04H1/4391 , D04H3/016 , D04H3/018 , Y10T442/621 , Y10T442/622 , Y10T442/641
摘要： A core/shell nanofiber non-woven containing a plurality of core/shell nanofibers where at least 70% of the nanofibers are bonded to other nanofibers. The core of the nanofiber contains a core polymer and the shell of the nanofiber contains a shell polymer. At least a portion of the core polymer interpenetrates the shell of the nanofiber and at least a portion of the shell polymer interpenetrates the core of the nanofiber. The process for forming a core/shell nanofiber non-woven is also disclosed.
摘要翻译： 含有多个核/壳纳米纤维的核/壳纳米纤维无纺布，其中至少70％的纳米纤维结合到其他纳米纤维上。 纳米纤维的核心含有核心聚合物，纳米纤维的外壳含有壳聚合物。 核心聚合物的至少一部分互穿纳米纤维的外壳，并且壳聚合物的至少一部分互穿纳米纤维的核心。 还公开了形成核/壳纳米纤维无纺布的方法。
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10.发明授权Method of producing fluorinated and chlorinated benzaldehydes and compositions thereof 失效产生氟化和氯化苯甲醛的方法及其组合物公开(公告)号：US06300525B1
公开(公告)日：2001-10-09
申请号：US09653935
申请日：2000-09-01
IPC分类号： C07C4549
CPC分类号： C07D493/04 , C07C45/49 , C07C47/55
摘要： A process for the preparation of aromatic aldehydes containing fluorine, and more particularly, to a formylation process for fluorinated aromatic derivatives through the reaction of fluorinated benzenes with carbon monoxide and aluminum chloride at a relatively low pressure, a low temperature, and in the presence of at most a catalytic amount of an acid (such as aqueous hydrochloric acid) is herein disclosed. The resultant fluorinated benzaldehydes are useful as precursors to the formation of a number of different compounds, such as dyestuffs, flavorings, fragrances, herbicidal compounds, nucleating agents, polymer additives, and the like. The inventive method provides a very cost effective and safe procedure for producing such fluorinated benzaldehydes in very high yields.
摘要翻译： 一种制备含氟芳族醛的方法，更具体地说，涉及通过氟化苯与一氧化碳和氯化铝在较低压力，低温下和在 本文公开了至多催化量的酸（例如盐酸水溶液）。 得到的氟化苯甲醛可用作形成许多不同化合物的前体，例如染料，调味剂，香料，除草化合物，成核剂，聚合物添加剂等。 本发明的方法提供了以非常高的产率生产这种氟化苯甲醛的非常成本有效和安全的方法。
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