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    Bismide-ether compounds, compositions thereof, and method of producing same
    2.
    发明授权
    Bismide-ether compounds, compositions thereof, and method of producing same 失效
    二苯醚类化合物及其组合物及其制备方法

    公开(公告)号：US4296219A

    公开(公告)日：1981-10-20

    申请号：US5233

    申请日：1979-01-22

    申请人： Akio Takahashi ,  Yutaka Itoh ,  Motoyo Wajima ,  Hirosada Morishita ,  Akio Nishikawa

    发明人： Akio Takahashi ,  Yutaka Itoh ,  Motoyo Wajima ,  Hirosada Morishita ,  Akio Nishikawa

    IPC分类号： C07D207/44 ,  C07D207/448 ,  C08G73/12

    CPC分类号： C07D207/448 ,  C08G73/121

    摘要： A bisimide-ether compound having the general formula is obtained by reacting an ethylenically unsaturated dicarboxylic acid anhydride, a diamine compound and a phenolic compound having in the molecule at least two hydroxyl groups, or by reacting a prepolymer of the anhydride and diamine compound with the phenolic compound: ##STR1## wherein R.sub.1 is a group containing at least two carbon atoms, R.sub.2 is a group containing at least two carbon atoms, R'.sub.2 is a group containing at least two carbon atoms and a carbon-carbon double bond, R.sub.3 is an aromatic group, the nitrogen atoms of the imide rings being directly connected to different carbon atoms of the group R.sub.1, the carbonyl groups of the imide rings being directly connected to different carbon atoms of the group R.sub.2 or R'.sub.2, the oxygen atoms between the groups R.sub.2 and R.sub.3 being directly connected to an aromatic nucleus of the group R.sub.3, and n is an integer of zero, one or more than 1.

    摘要翻译： 通过使烯键式不饱和二羧酸酐，二胺化合物和分子中至少两个羟基的酚类化合物反应，或者使酸酐与二胺化合物的预聚物与 酚类化合物：其中R1是含有至少两个碳原子的基团，R2是含有至少两个碳原子的基团，R'2是含有至少两个碳原子的基团和碳 - 碳双键，R3 是芳族基团，酰亚胺环的氮原子直接连接到基团R1的不同碳原子上，酰亚胺环的羰基直接连接到基团R 2或R'2的不同碳原子上，氧原子 在基团R 2和R 3直接连接到基团R 3的芳香环上，且n是0，1或1以上的整数。

    Thermosetting resin composition comprising dicyanamide and polyvalent imide
    4.
    发明授权
    Thermosetting resin composition comprising dicyanamide and polyvalent imide 失效
    包含二氰胺和多价酰亚胺的热固性树脂组合物

    公开(公告)号：US4482703A

    公开(公告)日：1984-11-13

    申请号：US435766

    申请日：1982-10-20

    申请人： Akio Takahashi ,  Takeshi Shimazaki ,  Motoyo Wajima ,  Hirosada Morishita

    发明人： Akio Takahashi ,  Takeshi Shimazaki ,  Motoyo Wajima ,  Hirosada Morishita

    IPC分类号： C08G73/00 ,  C08G73/06 ,  C08G73/12 ,  C09D179/08 ,  C08G73/10

    CPC分类号： C08G73/12

    摘要： A thermosetting resin composition comprises (A) at least one dicyanamide compound and (B) at least one polyvalent imide having one or more unsaturated bonds and, if necessary (C) at least one polymerizable compound of epoxy compounds, phenolic compounds and triallyl isocyanurate compounds. A thermosetting prepolymer can be obtained by subjecting the composition to a preliminary reaction with heating to the B stage and this prepolymer can give a cured product having excellent heat resistance of class C and flexibility. An exemplary composition containing 60 parts by wt. of 4,4'-dicyanomidodiphenylmethane and 40 parts by wt. of N,N'-4,4'-diphenylmethane bismaleimide dissolved in methyl Cellosolve is reacted at 70.degree. to 110.degree. C. for about 40 minutes to obtain a prepolymer soluble in methyl ethyl ketone. This prepolymer when admixed with 2-ethyl-4-methyl-imidazole and after removal of the methyl cellusolve will form an insoluble and infusible cured product upon heating at temperatures on the order of 170.degree. to 200.degree. C. for about 80 minutes. The resin composition when admixed with a solvent, is useful for impregnation and when used as a powder, it is useful as a molding resin.

    摘要翻译： 热固性树脂组合物包含（A）至少一种二氰酰胺化合物和（B）至少一种具有一个或多个不饱和键的多价酰亚胺，并且如果需要（C）至少一种环氧化合物的可聚合化合物，酚类化合物和三烯丙基异氰脲酸酯化合物 。 通过将加热至B阶段的组合物进行预反应，可以获得热固性预聚物，该预聚物可以得到具有优异的C级耐热性和柔软性的固化产物。 含有60重量份的示例性组合物 的4,4'-二氰基二苯基甲烷和40重量份。 溶解在甲基溶纤剂中的N，N'- 4,4'-二苯基甲烷双马来酰亚胺在70〜110℃下反应约40分钟，得到可溶于甲基乙基酮的预聚物。 当与2-乙基-4-甲基 - 咪唑混合并且除去甲基溶液后，该预聚物将在约170℃至200℃的温度下加热约80分钟时形成不溶性和不可渗透的固化产物。 当与溶剂混合时，树脂组合物可用于浸渍，并且当用作粉末时，其可用作模制树脂。

    Heat-resistant resin from aromatic cyanamide compound and aromatic amine compound
    7.
    发明授权
    Heat-resistant resin from aromatic cyanamide compound and aromatic amine compound 失效
    芳香族氰胺化合物和芳香胺化合物的耐热树脂

    公开(公告)号：US4486583A

    公开(公告)日：1984-12-04

    申请号：US525700

    申请日：1983-08-23

    申请人： Akio Takahashi ,  Masahiro Ono ,  Ritsuro Tada ,  Motoyo Wajima ,  Hirosada Morishita

    发明人： Akio Takahashi ,  Masahiro Ono ,  Ritsuro Tada ,  Motoyo Wajima ,  Hirosada Morishita

    IPC分类号： C08G73/00 ,  B32B27/04 ,  C08G73/06 ,  C08L79/04 ,  C08G73/08

    CPC分类号： C08G73/0644 ,  Y10T428/31504

    摘要： A polymer which has excellent heat resistance and mechanical properties which is useful as a molding material, contains the structural units having the following formulae [I] and [II]: ##STR1## wherein A and B each represents an at least divalent organic group having at least one aromatic ring such as a diphenyl ring; and m and n each represents a number of at least 1. The polymer is used in the form of a solution or varnish as an impregnating, laminating, bonding or film-forming coating or prepreg-forming varnish. A resin composition for forming the polymer contains an aromatic cyanamide compound and an aromatic amine which are reacted to form a prepolymer which, upon heating, is converted into a cured polymer having the structural units of formulae [I] and [II].

    摘要翻译： 具有优异的耐热性和机械性能的聚合物可用作成型材料，含有具有下式[I]和[II]的结构单元：即具有异质单胺环的聚合物单元 （即，具有正常三聚氰胺环的聚合物单元）其中A和B各自表示至少具有至少一个芳环的二价有机基团，例如二苯基环; m和n各自表示至少为1的数量。聚合物以溶液或清漆的形式用作浸渍，层压，粘合或成膜涂层或预浸料形成清漆。 用于形成聚合物的树脂组合物含有芳香族氰酰胺化合物和芳族胺，它们反应形成预聚物，其在加热时转化为具有式[I]和[II]结构单元的固化聚合物。

    Process for preparing thermosetting prepolymer from mixture of polyfunctional maleimide and bis-maleimide
    10.
    发明授权
    Process for preparing thermosetting prepolymer from mixture of polyfunctional maleimide and bis-maleimide 失效
    由多官能马来酰亚胺和双马来酰亚胺的混合物制备热固性预聚物的方法

    公开(公告)号：US4283522A

    公开(公告)日：1981-08-11

    申请号：US71518

    申请日：1979-08-31

    申请人： Akio Takahashi ,  Yutaka Itoh ,  Motoyo Wajima ,  Hirosada Morishita ,  Kenji Tsukanishi

    发明人： Akio Takahashi ,  Yutaka Itoh ,  Motoyo Wajima ,  Hirosada Morishita ,  Kenji Tsukanishi

    IPC分类号： C08G73/12 ,  C08J5/24 ,  C08G69/26 ,  C08G73/10

    CPC分类号： C08G73/121

    摘要： A process for preparing a thermosetting maleimide type prepolymer which comprises heating (A) a polyfunctional maleimide compound derived from a polyamine prepared from aniline and formalin, (B) a bis-maleimide and (C) a diamine. The thermosetting maleimide type prepolymer prepared according to the process of the present invention is excellent in solubility in low boiling point solvents such as acetone, methyl ethyl ketone and methyl cellosolve, which are available at low cost. Accordingly, the prepolymer is advantageously used especially for the production of laminated boards having excellent heat resisting properties.

    摘要翻译： 一种制备热固性马来酰亚胺型预聚物的方法，其包括加热（A）由苯胺和福尔马林制备的多胺衍生的多官能马来酰亚胺化合物，（B）双马来酰亚胺和（C）二胺。 根据本发明的方法制备的热固性马来酰亚胺型预聚物在低沸点溶剂如丙酮，甲基乙基酮和甲基溶纤剂中的溶解性优异，可以低成本获得。 因此，预聚物有利地用于生产具有优异的耐热性能的层压板。