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    Phosphorus-containing compounds useful for making halogen-free, ignition-resistant polymers
    1.
    发明授权
    Phosphorus-containing compounds useful for making halogen-free, ignition-resistant polymers 有权
    含磷化合物可用于制备无卤素，耐点火聚合物

    公开(公告)号：US09388297B2

    公开(公告)日：2016-07-12

    申请号：US14110939

    申请日：2012-05-01

    申请人： Anteneh Z. Worku ,  Michael J. Mullins

    发明人： Anteneh Z. Worku ,  Michael J. Mullins

    IPC分类号： C08K5/5313 ,  C07F9/6571 ,  C08K5/527 ,  C08K5/5393 ,  C09J11/06 ,  C08K5/00

    CPC分类号： C08K5/51 ,  C07F9/28 ,  C07F9/657172 ,  C07F9/657181 ,  C08J5/24 ,  C08J2363/04 ,  C08K5/0066 ,  C08K5/527 ,  C08K5/5313 ,  C08K5/5393 ,  C09D163/04 ,  C09J11/06 ,  C09J163/04 ,  H05K1/0353

    摘要： A process for making a phosphorus-containing compound is disclosed. The process comprises contacting a compound of formula (A) wherein RA and RB are selected from optionally substituted aryl, aryloxy, alkyl and alkoxy groups or can be combined to form cyclic structures; and RC is methyl, ethyl, isopropyl, n-butyl, i-butyl, t-butyl, phenyl or benzyl; and a compound of formula (B) wherein R1-R4 are selected from optionally substituted aryl, aryloxy, alkyl and alkoxy groups. The phosphorus-containing compound can then be used as a flame retardants for polymers, especially for epoxy, polyurethane, thermosetting resins and thermoplastic polymers. Such flame retardant-containing polymers can be used to make protective coating formulations and ignition-resistant fabricated articles, such as electrical laminates, polyurethane foams, and various molded and/or foamed thermoplastic products.

    摘要翻译： 公开了一种制备含磷化合物的方法。 该方法包括使其中RA和RB选自任选取代的芳基，芳氧基，烷基和烷氧基的式（A）化合物或可以组合形成环状结构; 乙基，异丙基，正丁基，异丁基，叔丁基，苯基或苄基; 和式（B）的化合物，其中R 1 -R 4选自任选取代的芳基，芳氧基，烷基和烷氧基。 然后可以将含磷化合物用作聚合物的阻燃剂，特别是用于环氧树脂，聚氨酯，热固性树脂和热塑性聚合物。 这种含阻燃剂的聚合物可用于制备保护性涂料配方和耐点火制造品，例如电层压材料，聚氨酯泡沫以及各种模制和/或发泡热塑性产品。

    PHOSPHORUS-CONTAINING COMPOUNDS USEFUL FOR MAKING HALOGEN-FREE, IGNITION-RESISTANT POLYMERS
    2.
    发明申请
    PHOSPHORUS-CONTAINING COMPOUNDS USEFUL FOR MAKING HALOGEN-FREE, IGNITION-RESISTANT POLYMERS 有权
    用于制备无卤素，耐点火聚合物的含磷化合物有用

    公开(公告)号：US20140249253A1

    公开(公告)日：2014-09-04

    申请号：US14110939

    申请日：2012-05-01

    申请人： Anteneh Z. Worku ,  Michael J. Mullins

    发明人： Anteneh Z. Worku ,  Michael J. Mullins

    IPC分类号： C08K5/5313 ,  C09J11/06

    CPC分类号： C08K5/51 ,  C07F9/28 ,  C07F9/657172 ,  C07F9/657181 ,  C08J5/24 ,  C08J2363/04 ,  C08K5/0066 ,  C08K5/527 ,  C08K5/5313 ,  C08K5/5393 ,  C09D163/04 ,  C09J11/06 ,  C09J163/04 ,  H05K1/0353

    摘要： A process for making a phosphorus-containing compound is disclosed. The process comprises contacting a compound of formula (A) wherein RA and RB are selected from optionally substituted aryl, aryloxy, alkyl and alkoxy groups or can be combined to form cyclic structures; and RC is methyl, ethyl, isopropyl, n-butyl, i-butyl, t-butyl, phenyl or benzyl; and a compound of formula (B) wherein R1-R4 are selected from optionally substituted aryl, aryloxy, alkyl and alkoxy groups. The phosphorus-containing compound can then be used as a flame retardants for polymers, especially for epoxy, polyurethane, thermosetting resins and thermoplastic polymers. Such flame retardant-containing polymers can be used to make protective coating formulations and ignition-resistant fabricated articles, such as electrical laminates, polyurethane foams, and various molded and/or foamed thermoplastic products.

    摘要翻译： 公开了一种制备含磷化合物的方法。 该方法包括使其中RA和RB选自任选取代的芳基，芳氧基，烷基和烷氧基的式（A）化合物或可以组合形成环状结构; 乙基，异丙基，正丁基，异丁基，叔丁基，苯基或苄基; 和式（B）的化合物，其中R 1 -R 4选自任选取代的芳基，芳氧基，烷基和烷氧基。 然后可以将含磷化合物用作聚合物的阻燃剂，特别是用于环氧树脂，聚氨酯，热固性树脂和热塑性聚合物。 这种含阻燃剂的聚合物可用于制备保护性涂料配方和耐点火制造品，例如电层压材料，聚氨酯泡沫以及各种模制和/或发泡热塑性产品。

    Compositions having phosphorus-containing compounds
    4.
    发明授权
    Compositions having phosphorus-containing compounds 有权
    具有含磷化合物的组合物

    公开(公告)号：US09267030B2

    公开(公告)日：2016-02-23

    申请号：US13575617

    申请日：2011-01-26

    申请人： Kamesh Vyakaranam ,  Mark B. Wilson ,  Endre Szuromi ,  Michael J. Mullins

    发明人： Kamesh Vyakaranam ,  Mark B. Wilson ,  Endre Szuromi ,  Michael J. Mullins

    IPC分类号： H01B3/40 ,  C08L63/04 ,  C08G59/40

    CPC分类号： C08L63/04 ,  C08G59/4014

    摘要： Embodiments of the present disclosure provide a composition that includes a phosphorous-containing compound, a cyanate ester, an epoxy resin, and a maleimide. For the various embodiments, a viscosity of the composition increases less than 100% as measured by Gardner Bubble Viscosity a temperature of 23° C. in at least 3 days. For the various embodiments, the composition of the present disclosure can also include an aprotic solvent, such as a ketone. Embodiments of the present disclosure further include a composition that includes the phosphorous-containing compound, the cyanate ester, and the aprotic solvent. For the various embodiments, the composition can also include the epoxy resin and the maleimide. For the various embodiments, the composition does not include an aliphatic alcohol.

    摘要翻译： 本公开的实施方案提供了包含含磷化合物，氰酸酯，环氧树脂和马来酰亚胺的组合物。 对于各种实施方案，组合物的粘度增加小于100％，如通过Gardner Bubble Viscosity在至少3天内23℃的温度测量的。 对于各种实施方案，本公开的组合物还可以包括非质子溶剂，例如酮。 本公开的实施方案还包括包含含磷化合物，氰酸酯和非质子传递溶剂的组合物。 对于各种实施方案，组合物还可以包括环氧树脂和马来酰亚胺。 对于各种实施方案，组合物不包括脂族醇。

    COMPOSITIONS HAVING PHOSPHORUS-CONTAINING COMPOUNDS
    5.
    发明申请
    COMPOSITIONS HAVING PHOSPHORUS-CONTAINING COMPOUNDS 有权
    含有含磷化合物的组合物

    公开(公告)号：US20130005857A1

    公开(公告)日：2013-01-03

    申请号：US13575617

    申请日：2011-01-26

    申请人： Kamesh Vyakaranam ,  Mark B. Wilson ,  Endre Szuromi ,  Michael J. Mullins

    发明人： Kamesh Vyakaranam ,  Mark B. Wilson ,  Endre Szuromi ,  Michael J. Mullins

    IPC分类号： C08L63/04 ,  C09K3/00

    CPC分类号： C08L63/04 ,  C08G59/4014

    摘要： Embodiments of the present disclosure provide a composition that includes a phosphorous-containing compound, a cyanate ester, an epoxy resin, and a maleimide. For the various embodiments, a viscosity of the composition increases less than 100% as measured by Gardner Bubble Viscosity a temperature of 23° C. in at least 3 days. For the various embodiments, the composition of the present disclosure can also include an aprotic solvent, such as a ketone. Embodiments of the present disclosure further include a composition that includes the phosphorous-containing compound, the cyanate ester, and the aprotic solvent. For the various embodiments, the composition can also include the epoxy resin and the maleimide. For the various embodiments, the composition does not include an aliphatic alcohol.

    摘要翻译： 本公开的实施方案提供了包含含磷化合物，氰酸酯，环氧树脂和马来酰亚胺的组合物。 对于各种实施方案，组合物的粘度增加小于100％，如通过Gardner Bubble Viscosity在至少3天内23℃的温度测量的。 对于各种实施方案，本公开的组合物还可以包括非质子溶剂，例如酮。 本公开的实施方案还包括包含含磷化合物，氰酸酯和非质子传递溶剂的组合物。 对于各种实施方案，组合物还可以包括环氧树脂和马来酰亚胺。 对于各种实施方案，组合物不包括脂族醇。

    METAL STABILIZERS FOR EPOXY RESINS AND ADVANCEMENT PROCESS
    7.
    发明申请
    METAL STABILIZERS FOR EPOXY RESINS AND ADVANCEMENT PROCESS 审中-公开
    金属稳定剂用于环氧树脂和高级过程

    公开(公告)号：US20110218273A1

    公开(公告)日：2011-09-08

    申请号：US13127745

    申请日：2009-12-15

    申请人： Raymond J. Thibault ,  Michael J. Mullins

    发明人： Raymond J. Thibault ,  Michael J. Mullins

    IPC分类号： C08L63/00 ,  C09D163/00

    CPC分类号： C08L63/00 ,  C08G59/4028 ,  C08G59/621 ,  C08K5/0091 ,  C08K2201/019

    摘要： A process comprising: contacting a) an epoxy resin; b) a compound selected from the group consisting of a phenol-containing compound, an isocyanate-containing compound, and mixtures thereof and c) a stabilizer comprising a metal-containing compound, said metal-containing compound comprising a metal selected from the Group 11-13 metals and combinations thereof; in the presence of a catalyst in an advancement reaction zone under advancement reaction conditions to produce an advancement reaction product is disclosed.

    摘要翻译： 一种方法，包括：a）环氧树脂; b）选自含苯酚的化合物，含异氰酸酯的化合物及其混合物的化合物，和c）包含含金属化合物的稳定剂，所述含金属化合物包含选自第11组的金属 -13金属及其组合; 在促进反应条件下在催化剂存在下，在提前反应条件下，制备提前反应产物。

    Rheology modification of low density polyethylene
    10.
    发明授权
    Rheology modification of low density polyethylene 有权
    低密度聚乙烯的流变改性

    公开(公告)号：US06521306B1

    公开(公告)日：2003-02-18

    申请号：US09129163

    申请日：1998-08-05

    申请人： Wendy D. Hoenig ,  Teresa Karjala ,  Li-Min Tau ,  Clark H. Cummins ,  Michael J. Mullins ,  H. Craig Silvis ,  Thoi H. Ho

    发明人： Wendy D. Hoenig ,  Teresa Karjala ,  Li-Min Tau ,  Clark H. Cummins ,  Michael J. Mullins ,  H. Craig Silvis ,  Thoi H. Ho

    IPC分类号： B29D2200

    CPC分类号： C08L23/02 ,  C08G81/02 ,  C08K5/43 ,  C08L23/04 ,  C08L23/06 ,  C08L23/08 ,  C08L23/0815 ,  C08L23/0838 ,  C08L23/0853 ,  C08L23/16 ,  C08L2205/22 ,  C08L2312/00 ,  C08L2314/06 ,  Y10T428/1334 ,  Y10T428/1352 ,  Y10T428/1386 ,  Y10T428/139 ,  Y10T428/31913 ,  Y10T428/31917 ,  C08L2666/04

    摘要： The invention includes a process of preparing a coupled polymer characterized by heating an admixture containing (1) at least one ethylene polymer or blend of ethylene polymers having a density of at least about 0.89 g/mL and less than about 0.935 g/mL and a comonomer content between about 0.5 and 50 weight percent of an alpha olefin having greater than 2 and less than 20 carbon atoms per molecule and (2) a coupling amount of at least one poly(sulfonyl azide) to at least the decomposition temperature of the poly(sulfonyl azide) for a period sufficient for decomposition of at least about 80 weight percent of the poly(sulfonyl azide) and sufficient to result in a coupled polymer. The amount of poly(sulfonyl azide) is preferably from about 0.01 to about 5 weight percent of polymers in the admixture. The invention also includes any composition which is the product of any of the processes of the invention and articles made from those compositions, particularly any film of any composition of the invention. Additionally the invention includes a use of any composition of the invention in a process of blowing, casting or calendaring a film. More particularly the invention includes articles of compositions of the invention which are trash bags, agricultural films, construction films, or geomembranes, grocery sacks, sealant layers, tie layers, produce bags, garment bags, shipping sacks, medical films, stretch films, shrink films, agricultural films, greenhouse films, construction films, or stretch hooders.

    摘要翻译： 本发明包括一种制备偶联聚合物的方法，其特征在于加热含有（1）至少一种乙烯聚合物或密度为至少约0.89g / mL且小于约0.935g / mL的乙烯聚合物的共混物的混合物， 共聚单体含量为约0.5至50重量％的每分子具有大于2个且小于20个碳原子的α-烯烃，和（2）至少一个聚（磺酰基叠氮化物）的偶联量至少达到聚 （磺酰基叠氮化物）足以分解至少约80重量％的聚（磺酰基叠氮化物）并足够导致偶联聚合物的时间。 聚（磺酰基叠氮化物）的量优选为混合物中约0.01至约5重量％的聚合物。 本发明还包括任何组合物，其是本发明任何方法的产物和由这些组合物制成的制品，特别是本发明任何组合物的任何薄膜。 此外，本发明包括在吹塑，浇铸或压延膜的方法中使用本发明的任何组合物。 更具体地，本发明包括本发明的制品，其为垃圾袋，农用膜，建筑膜或土工膜，杂货袋，密封剂层，连接层，生产袋，服装袋，运输袋，医疗膜，拉伸膜，收缩 电影，农膜，温室膜，建筑膜或拉伸罩。