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    Production of highly conductive graphitic films from polymer films
    1.
    发明申请
    Production of highly conductive graphitic films from polymer films 审中-公开
    从聚合物薄膜生产高导电性石墨膜

    公开(公告)号：US20160059444A1

    公开(公告)日：2016-03-03

    申请号：US14121387

    申请日：2014-08-29

    申请人： Yanbo Wang ,  Bor Z. Jang ,  David Burton ,  Lucy Fu ,  Aruna Zhamu

    发明人： Yanbo Wang ,  Bor Z. Jang ,  David Burton ,  Lucy Fu ,  Aruna Zhamu

    IPC分类号： B29C35/02 ,  C01B31/04

    CPC分类号： C01B31/04 ,  C01B32/20 ,  C01P2006/10 ,  C01P2006/32 ,  C01P2006/40

    摘要： A one-step (direct graphitization) process for producing a graphitic film, comprising directly feeding a precursor polymer film, without going through a carbonization step, to a graphitization zone preset at a graphitization temperature no less than 2,200° C. for a period of residence time sufficient for converting the precursor polymer film to a porous graphitic film having a density from 0.1 g/cm3 to 1.5 g/cm3 and retreating the porous graphitic film from the graphitization zone. Preferably, the precursor polymer film is selected from the group consisting of polyimide, polyamide, phenolic resin, polyoxadiazole, polybenzoxazole, polybenzobisoxazole, polythiazole, polybenzothiazole, polybenzobisthiazole, poly(p-phenylene vinylene), polybenzimidazole, polybenzobisimidazole, polyacrylonitrile, and combinations thereof. Preferably, the precursor polymer film contains an amount of graphene sheets or expanded graphite flakes, preferably from 1% to 90% by weight, sufficient for promoting or accelerating graphitization.

    摘要翻译： 用于生产石墨膜的一步（直接石墨化）方法，包括直接将前体聚合物膜直接进料到不经过碳化步骤的石墨化区域，石墨化区域以石墨化温度不低于2200℃预设一段时间 将前体聚合物膜转化为密度为0.1g / cm 3至1.5g / cm 3的多孔石墨膜，并从石墨化区域中回收多孔石墨膜的足够的停留时间。 优选地，前体聚合物膜选自聚酰亚胺，聚酰胺，酚醛树脂，聚恶二唑，聚苯并恶唑，聚苯并双恶唑，聚噻唑，聚苯并噻唑，聚苯并二噻唑，聚（对亚苯基亚乙烯基），聚苯并咪唑，聚苯并双咪唑，聚丙烯腈及其组合。 优选地，前体聚合物膜含有足以促进或加速石墨化的量的石墨烯片或膨胀石墨片，优选为1重量％至90重量％。

    Process for producing highly oriented graphene films
    3.
    发明申请
    Process for producing highly oriented graphene films 有权
    生产高取向石墨烯薄膜的方法

    公开(公告)号：US20150218003A1

    公开(公告)日：2015-08-06

    申请号：US13999282

    申请日：2014-02-06

    申请人： Aruna Zhamu ,  Bor Z. Jang ,  Yanbo Wang ,  Lucy Fu

    发明人： Aruna Zhamu ,  Bor Z. Jang ,  Yanbo Wang ,  Lucy Fu

    IPC分类号： C01B31/04 ,  B29C39/38 ,  B29C43/00 ,  B29C39/00

    CPC分类号： C01B32/19 ,  B29K2105/0061 ,  B29L2007/008 ,  B32B37/24 ,  B32B38/0036 ,  B82Y30/00 ,  B82Y40/00 ,  C01B31/043 ,  C01B32/184 ,  C01B32/192 ,  C01B32/194 ,  C01B2204/04 ,  C01B2204/22 ,  C01B2204/24 ,  C01B2204/26 ,  C09K5/14

    摘要： A process for producing a highly oriented graphene film (HOGF), comprising: (a) preparing a graphene oxide (GO) dispersion having GO sheets dispersed in a fluid medium; (b) dispensing and depositing the dispersion onto a surface of a supporting substrate to form a layer of GO, wherein the dispensing and depositing procedure includes subjecting the dispersion to an orientation-inducing stress; (c) removing the fluid medium to form a dried layer of GO having an inter-plane spacing d002 of 0.4 nm to 1.2 nm; (d) slicing the dried layer of GO into multiple pieces of dried GO and stacking at least two pieces of dried GO to form a mass of multiple pieces of GO; and (f) heat treating the mass under an optional first compressive stress to produce the HOGF at a first heat treatment temperature higher than 100° C. to an extent that an inter-plane spacing d002 is decreased to a value less than 0.4 nm.

    摘要翻译： 一种制备高取向石墨烯膜（HOGF）的方法，包括：（a）制备分散在流体介质中的GO片的氧化石墨烯（GO）分散体; （b）将分散体分配并沉积到支撑基底的表面上以形成一层GO，其中分配和沉积步骤包括使分散体经受定向诱导应力; （c）去除流体介质以形成具有0.4nm至1.2nm的平面间距d002的GO干燥层; （d）将干燥的GO层切成多个干燥的GO，并堆叠至少两片干燥的GO以形成多个GO块; 和（f）在任选的第一压缩应力下热处理所述物质，以在高于100℃的第一热处理温度下产生HOGF，使得平面间距d002减小到小于0.4nm的值。

    Process for producing highly oriented graphene films
    4.
    发明授权
    Process for producing highly oriented graphene films 有权
    生产高取向石墨烯薄膜的方法

    公开(公告)号：US09580325B2

    公开(公告)日：2017-02-28

    申请号：US13999282

    申请日：2014-02-06

    申请人： Aruna Zhamu ,  Bor Z Jang ,  Yanbo Wang ,  Lucy Fu

    发明人： Aruna Zhamu ,  Bor Z Jang ,  Yanbo Wang ,  Lucy Fu

    IPC分类号： B82Y30/00 ,  B82Y40/00 ,  C01B31/04 ,  B32B37/24 ,  B32B38/00 ,  B29K105/00 ,  B29L7/00

    CPC分类号： C01B32/19 ,  B29K2105/0061 ,  B29L2007/008 ,  B32B37/24 ,  B32B38/0036 ,  B82Y30/00 ,  B82Y40/00 ,  C01B31/043 ,  C01B32/184 ,  C01B32/192 ,  C01B32/194 ,  C01B2204/04 ,  C01B2204/22 ,  C01B2204/24 ,  C01B2204/26 ,  C09K5/14

    摘要： A process for producing a highly oriented graphene film (HOGF), comprising: (a) preparing a graphene oxide (GO) dispersion having GO sheets dispersed in a fluid medium; (b) dispensing and depositing the dispersion onto a surface of a supporting substrate to form a layer of GO, wherein the dispensing and depositing procedure includes subjecting the dispersion to an orientation-inducing stress; (c) removing the fluid medium to form a dried layer of GO having an inter-plane spacing d002 of 0.4 nm to 1.2 nm; (d) slicing the dried layer of GO into multiple pieces of dried GO and stacking at least two pieces of dried GO to form a mass of multiple pieces of GO; and (f) heat treating the mass under an optional first compressive stress to produce the HOGF at a first heat treatment temperature higher than 100° C. to an extent that an inter-plane spacing d002 is decreased to a value less than 0.4 nm.

    摘要翻译： 一种制备高取向石墨烯膜（HOGF）的方法，包括：（a）制备分散在流体介质中的GO片的氧化石墨烯（GO）分散体; （b）将分散体分配并沉积到支撑基底的表面上以形成一层GO，其中分配和沉积步骤包括使分散体经受定向诱导应力; （c）去除流体介质以形成具有0.4nm至1.2nm的平面间距d002的GO干燥层; （d）将干燥的GO层切成多个干燥的GO，并堆叠至少两片干燥的GO以形成多个GO块; 和（f）在任选的第一压缩应力下热处理所述物质，以在高于100℃的第一热处理温度下产生HOGF，使得平面间距d002减小到小于0.4nm的值。

    Highly oriented graphene structures and process for producing same
    5.
    发明申请
    Highly oriented graphene structures and process for producing same 有权
    高取向石墨烯结构及其制造方法

    公开(公告)号：US20150217538A1

    公开(公告)日：2015-08-06

    申请号：US13999283

    申请日：2014-02-06

    申请人： Aruna Zhamu ,  Bor Z. Jang ,  Yanbo Wang ,  Lucy Fu

    发明人： Aruna Zhamu ,  Bor Z. Jang ,  Yanbo Wang ,  Lucy Fu

    IPC分类号： B32B9/04 ,  B32B38/00 ,  B32B37/24

    CPC分类号： B32B9/04 ,  B32B5/00 ,  B82Y30/00 ,  B82Y40/00 ,  C01B32/182 ,  C01B32/23 ,  C01P2006/10 ,  C01P2006/32 ,  C01P2006/40 ,  C04B35/52 ,  C04B35/645 ,  C04B2235/5292 ,  C04B2235/604 ,  C04B2235/723 ,  C04B2235/787 ,  Y10T156/1075

    摘要： A process for producing a bulk highly oriented graphene structure, comprising: (a) preparing a graphene oxide dispersion having graphene oxide (GO) sheets dispersed in a fluid medium; (b) dispensing and depositing the dispersion onto a surface of a supporting substrate to form a layer of GO, wherein the dispensing and depositing procedure includes subjecting the dispersion to an orientation-inducing stress; (c) removing the fluid medium to form a dried layer of GO having an inter-plane spacing d002 of 0.4 nm to 1.2 nm; (d) slicing the dried layer of GO into multiple pieces of dried GO and stacking at least two pieces of dried GO to form a mass of multiple pieces of GO; and (f) heat treating the mass under an optional first compressive stress to produce the highly oriented graphene structure at a first heat treatment temperature higher than 100° C. to an extent that an inter-plane spacing d002 is decreased to a value less than 0.4 nm.

    摘要翻译： 一种用于制造块体高取向石墨烯结构的方法，包括：（a）制备分散在流体介质中的具有氧化石墨烯（GO）片的石墨烯氧化物分散体; （b）将分散体分配并沉积到支撑基底的表面上以形成一层GO，其中分配和沉积步骤包括使分散体经受定向诱导应力; （c）去除流体介质以形成具有0.4nm至1.2nm的平面间距d002的GO干燥层; （d）将干燥的GO层切成多个干燥的GO，并堆叠至少两片干燥的GO以形成多个GO块; 和（f）在任选的第一压缩应力下热处理所述材料，以在高于100℃的第一热处理温度下产生高度取向的石墨烯结构，使得平面间距d002减小到小于 0.4nm。

    Lithium secondary batteries containing non-flammable quasi-solid electrolyte
    7.
    发明授权
    Lithium secondary batteries containing non-flammable quasi-solid electrolyte 有权
    锂二次电池含有不易燃的准固体电解质

    公开(公告)号：US09368831B2

    公开(公告)日：2016-06-14

    申请号：US13986814

    申请日：2013-06-10

    申请人： Hui He ,  Bor Z Jang ,  Yanbo Wang ,  Aruna Zhamu

    发明人： Hui He ,  Bor Z Jang ,  Yanbo Wang ,  Aruna Zhamu

    IPC分类号： H01M10/056 ,  H01M10/052 ,  H01M10/0569 ,  H01M4/136 ,  H01M4/58 ,  H01M10/0525 ,  H01M10/0568 ,  H01M12/08 ,  H01M4/02

    CPC分类号： H01M10/052 ,  H01M4/136 ,  H01M4/5825 ,  H01M10/0525 ,  H01M10/0568 ,  H01M10/0569 ,  H01M12/08 ,  H01M2004/028 ,  H01M2300/0028 ,  Y02E60/122 ,  Y02E60/128 ,  Y02T10/7011

    摘要： A rechargeable lithium cell comprising a cathode having a cathode active material, an anode having an anode active material, a porous separator electronically separating the anode and the cathode, a non-flammable quasi-solid electrolyte in contact with the cathode and the anode, wherein the electrolyte contains a lithium salt dissolved in a first organic liquid solvent with a concentration sufficiently high so that the electrolyte exhibits a vapor pressure less than 0.01 kPa when measured at 20° C., a flash point at least 20 degrees Celsius higher than the flash point of the first organic liquid solvent alone, a flash point higher than 150° C., or no flash point. This battery cell is non-flammable and safe, has a long cycle life, high capacity, and high energy density.

    摘要翻译： 一种可再充电锂电池，包括具有阴极活性材料的阴极，具有阳极活性材料的阳极，电子分离阳极和阴极的多孔隔板，与阴极和阳极接触的不可燃的准固体电解质，其中 电解质含有溶解在浓度足够高的第一有机液体溶剂中的锂盐，使得当在20℃下测量时，电解质的蒸汽压力低于0.01kPa，闪点高于闪光灯的至少20摄氏度 第一有机液体溶剂点，闪点高于150℃，或无闪点。 该电池不易燃，安全，循环寿命长，容量大，能量密度高。

    Surface-mediated cell-driven power tools and methods of operating same
    8.
    发明授权
    Surface-mediated cell-driven power tools and methods of operating same 有权
    表面介导的电池驱动电动工具及其操作方法

    公开(公告)号：US09085076B2

    公开(公告)日：2015-07-21

    申请号：US13385350

    申请日：2012-02-16

    申请人： Aruna Zhamu ,  Guorong Chen ,  Wei Xiong ,  Bor Z. Jang ,  Yanbo Wang ,  Qing Fang

    发明人： Aruna Zhamu ,  Guorong Chen ,  Wei Xiong ,  Bor Z. Jang ,  Yanbo Wang ,  Qing Fang

    IPC分类号： B25F5/00 ,  H01M4/00 ,  H01G11/50 ,  H01M10/0525 ,  H01M16/00 ,  H01M4/133 ,  H01M10/46 ,  H01M6/50 ,  H01M12/00 ,  H01M14/00 ,  H02M3/158 ,  H01G11/06

    CPC分类号： B25F5/00 ,  H01G11/06 ,  H01G11/50 ,  H01M4/133 ,  H01M6/5033 ,  H01M10/0525 ,  H01M10/465 ,  H01M12/005 ,  H01M14/00 ,  H01M16/00 ,  H01M2220/30 ,  H02M3/1582 ,  Y02B70/1483 ,  Y02E60/122 ,  Y02E60/13 ,  Y02P70/54

    摘要： A portable power tool comprises an electric motor, actuator, or light-emitting hardware and a rechargeable power source connected to the electric motor, actuator, or light-emitting hardware, wherein the power source contains at least a surface-mediated cell (SMC). The power tools include, but are not limited to, impact driver, air compressor, alligator shear, angle grinder, band saw, belt sander, biscuit joiner, ceramic tile cutter tile saw, chainsaw, circular saw, concrete saw, cold saw, crusher, diamond blade, diamond tools, disc sander, drill, floor sander, grinding machine, heat gun, impact wrench, jackhammer, jointer, jigsaw, lathe, miter saw, nail gun, needle scaler, torque wrench, powder-actuated tools, power wrench, radial arm saw, random orbital sander, reciprocating saw, rotary reciprocating saw, rotary tool, sabre saw, sander, scroll saw, steel cut off saw, table saw, thickness planer, trimmer, wall chaser, wood router, or flashlight.

    摘要翻译： 便携式电动工具包括电动机，致动器或发光硬件以及连接到电动机，致动器或发光硬件的可再充电电源，其中电源至少包含表面介导的电池（SMC） 。 电动工具包括但不限于冲击驱动器，空气压缩机，鳄鱼剪，角磨机，带锯，皮带砂光机，饼干连接机，瓷砖切割机瓦锯，电锯，圆锯，混凝土锯，冷锯，破碎机 ，金刚石刀片，金刚石工具，圆盘砂光机，钻头，地板砂光机，磨床，热枪，冲击扳手，手提锤，接头，拼图，车床，斜切锯，指甲枪，针标机，扭矩扳手，粉末驱动工具，动力 扳手，径向手臂锯，随机轨道砂光机，往复锯，旋转往复锯，旋转工具，军刀锯，砂光机，卷锯，钢切割锯，台锯，厚度刨，修边机，壁挂机，木路由器或手电筒。

    Non-flammable quasi-solid electrolyte and non-lithium alkali metal or alkali-ion secondary batteries containing same
    9.
    发明授权
    Non-flammable quasi-solid electrolyte and non-lithium alkali metal or alkali-ion secondary batteries containing same 有权
    不易燃的准固体电解质和含有其的非锂碱金属或碱金属二次电池

    公开(公告)号：US09059481B2

    公开(公告)日：2015-06-16

    申请号：US13987764

    申请日：2013-08-30

    申请人： Hui He ,  Bor Z Jang ,  Yanbo Wang ,  Aruna Zhamu

    发明人： Hui He ,  Bor Z Jang ,  Yanbo Wang ,  Aruna Zhamu

    IPC分类号： H01M6/18 ,  H01M10/0568 ,  H01M10/05 ,  H01M4/40

    CPC分类号： H01M10/0568 ,  H01M4/40 ,  H01M4/405 ,  H01M4/587 ,  H01M10/05 ,  H01M10/054 ,  H01M10/0569

    摘要： A non-flammable quasi-solid electrolyte and a rechargeable non-lithium alkali metal cell containing this electrolyte. The electrolyte comprises an alkali metal salt dissolved in an organic liquid solvent with a concentration higher than 2.5 M (preferably >3.5 M) or a molecular ratio greater than 0.2 (preferably >0.3), wherein the alkali metal is selected from Na, K, a combination of Na and K, or a combination of Na and/or K with Li. The alkali metal salt concentration is sufficiently high so that the electrolyte exhibits a vapor pressure

    摘要翻译： 不可燃的准固体电解质和含有这种电解质的可再充电的非锂碱金属电池。 电解质包含溶解在浓度高于2.5M（优选> 3.5M）或分子比大于0.2（优选> 0.3））的有机液体溶剂中的碱金属盐，其中碱金属选自Na，K， Na和K的组合，或Na和/或K与Li的组合。 碱金属盐浓度足够高，使得当在20℃下测量时，电解质的蒸气压<0.01kPa，当单独测量时，有机溶剂的蒸气压的蒸汽压<60％，至少闪点 当单独测量时，有机液体溶剂的闪点高20摄氏度，闪点高于150℃，或无可检测的闪点。