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公开(公告)号：US11807704B2
公开(公告)日：2023-11-07
申请号：US16954083
申请日：2018-12-13
发明人： Yuan-Yong Yan , Zengquan Qin , Koichi Saito , Rita E. Cook
CPC分类号： C08F36/06 , C08K3/04 , C08K3/36 , C08K5/20 , C08K5/3412 , C08K5/55 , B60C1/0016 , C08F2810/40
摘要： Disclosed herein are a functionalized diene monomer-containing polymer containing first and second functionalizing groups, processes for preparing the functionalized polymer, and rubber compositions containing the functionalized polymer. The functionalized polymer contains polymer chains comprises of at least one conjugated diene monomer optionally in combination with at least one vinyl aromatic monomer wherein each polymer chain is functionalized at its chain end with at least the first functionalizing group and is coupled via the first functionalizing group to the second functionalizing group.
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2.发明授权公开(公告)号：US11168160B2
公开(公告)日：2021-11-09
申请号：US16863458
申请日：2020-04-30
IPC分类号： C08F36/06 , C08K3/04 , C08K3/06 , C08L47/00 , C08L21/00 , C08F4/52 , C08L9/00 , C08L7/02 , C08L15/02 , C08L19/00
摘要： Embodiments of 1,4-polybutadiene rubber compositions useful at low temperatures are provided, wherein the 1,4-polybutadiene incorporated therein comprises a cis content of at least 85 to about 92%, a vinyl content of at about 1% to about 5%, and a trans content of about 3 to about 12%, and wherein the 1,4-polybutadiene has an enthalpy of melting ΔHm of about 5 to about 25 J/g° C. as measured via differential scanning calorimetry (DSC).
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公开(公告)号：US11028195B2
公开(公告)日：2021-06-08
申请号：US16297689
申请日：2019-03-10
IPC分类号： C08F36/06 , C08F36/04 , C08F212/14 , C08F290/06 , C08F290/14 , C08F297/02 , C08F297/04 , C08L53/02 , C08K3/013 , C08C19/44 , C07D339/08 , C08F236/10
摘要： Vulcanizates with desirable properties can be obtained from compounds incorporating polymers that include hydroxyl group-containing aryl functionalities. The functionalities can be incorporated by using any or all of appropriate initiators, monomers and terminating compounds. Such polymers exhibit excellent interactivity with both conventional and non-conventional fillers.
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4.发明授权公开(公告)号：US10457765B2
公开(公告)日：2019-10-29
申请号：US15315011
申请日：2015-05-26
发明人： Zengquan Qin , Joshua P. Abell
IPC分类号： C08F236/06 , C08F4/52 , C08F4/54 , C08F4/6392 , C07F7/10 , C08F297/06 , C08L9/00 , C07F17/00
摘要： Metallic complexes having indenyl ligands can be used as an ingredient of a catalyst system. The catalyst system can be used in polymerizations of ethylenically unsaturated hydrocarbon monomers that include both olefins and polyenes. Embodiments of the catalyst system can provide interpolymers that include polyene mer and from 40 to 75 mole percent ethylene mer, with a plurality of the ethylene mer being randomly distributed. The catalyst system also can be used in solution polymerizations conducted in C5-C12 alkanes, yielding interpolymers that include at least 10 mole percent ethylene mer.
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公开(公告)号：US20190233557A1
公开(公告)日：2019-08-01
申请号：US16297689
申请日：2019-03-10
IPC分类号： C08F36/06 , C08F297/02 , C08C19/44 , C07D339/08 , C08K3/013 , C08L53/02 , C08F297/04 , C08F290/14 , C08F290/06 , C08F212/14 , C08F36/04
CPC分类号： C08F36/06 , C07D339/08 , C08C19/44 , C08F36/04 , C08F212/14 , C08F236/10 , C08F290/06 , C08F290/14 , C08F297/02 , C08F297/04 , C08K3/013 , C08L53/02 , Y02P20/55 , C08F4/48 , C08L2666/02 , C08L15/00
摘要： Vulcanizates with desirable properties can be obtained from compounds incorporating polymers that include hydroxyl group-containing aryl functionalities. The functionalities can be incorporated by using any or all of appropriate initiators, monomers and terminating compounds. Such polymers exhibit excellent interactivity with both conventional and non-conventional fillers.
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公开(公告)号：US09868801B2
公开(公告)日：2018-01-16
申请号：US15165552
申请日：2016-05-26
发明人： Zengquan Qin , Kevin M. McCauley , Steven Luo
IPC分类号： C08F36/06 , C08F136/06 , C08F4/54
CPC分类号： C08F136/06 , C08F4/545 , C08F36/06 , C08F4/52
摘要： Disclosed herein are solution polymerization processes for producing a high-cis polydiene. The processes include polymerizing at least one conjugated diene monomer in an organic solvent in the presence of at least one thiol compound and a lanthanide-based catalyst composition to produce a polydiene having a cis-1,4-linkage content of 90-99%. The at least one thiol compound is represented by the general formula R—S—H, where R is a hydrocarbyl group or a substituted hydrocarbyl group. The lanthanide-based catalyst composition comprises (a) a lanthanide compound, (b) an alkylating agent, and (c) a halogen source, where (c) may optionally be provided by (a), (b), or both (a) and (b). The molar ratio of the at least one thiol compound to the lanthanide compound used in the polymerization process ranges from 0.01:1 to 100:1. Improved solution polymerization processes regarding the same are also disclosed herein.
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公开(公告)号：US20170267798A1
公开(公告)日：2017-09-21
申请号：US15420482
申请日：2017-01-31
IPC分类号： C08F212/08 , C08C19/44 , C08K3/36 , C08L9/00 , C08L15/00
CPC分类号： C08F212/08 , C08C19/44 , C08K3/36 , C08L9/00 , C08L15/00
摘要： A method for providing a polymer having terminal functionality involves reacting a terminally active polymer with an α,β-ethylenically unsaturated compound that includes a group 2-13 element so as to provide a functionalized polymer. The resulting polymer exhibits enhanced interactivity with particulate fillers and can be used in the manufacture of vulcanizates.
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公开(公告)号：US20170114171A1
公开(公告)日：2017-04-27
申请号：US15315052
申请日：2015-05-25
发明人： Joshua P. Abell , Zengquan Qin
IPC分类号： C08F236/06 , C07F17/00
CPC分类号： C08F236/06 , B01J31/16 , C07F17/00 , C08F4/52 , C08F4/545 , C08F210/18 , C08F236/04 , C08F2420/04 , C08F2800/10 , C08L7/00 , C08L9/00 , C08L9/06
摘要： Metallic complexes having indenyl ligands can be used as an ingredient of a catalyst system. The catalyst system can be used in polymerizations of ethylenically unsaturated hydrocarbon monomers that include both olefins and polyenes. Embodiments of the catalyst system can provide interpolymers that include polyene mer and up to about 40 mole percent ethylene mer. The catalyst system also can be used in solution polymerizations conducted in C5-C12 alkanes.
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9.发明申请公开(公告)号：US20170114170A1
公开(公告)日：2017-04-27
申请号：US15315011
申请日：2015-05-26
发明人： Zengquan Qin , Joshua P. Abell
IPC分类号： C08F236/06 , C08L9/00 , C08F297/06
摘要： Metallic complexes having indenyl ligands can be used as an ingredient of a catalyst system. The catalyst system can be used in polymerizations of ethylenically unsaturated hydrocarbon monomers that include both olefins and polyenes. Embodiments of the catalyst system can provide interpolymers that include polyene mer and from 40 to 75 mole percent ethylene mer, with a plurality of the ethylene mer being randomly distributed. The catalyst system also can be used in solution polymerizations conducted in C5-C12 alkanes, yielding interpolymers that include at least 10 mole percent ethylene mer.
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公开(公告)号：US09422379B2
公开(公告)日：2016-08-23
申请号：US14319441
申请日：2014-06-30
IPC分类号： C08F36/04 , C08F136/06 , C08F236/06 , C08F4/70
CPC分类号： C08F136/06 , C08F36/04 , C08F236/06 , C08F4/7098
摘要： In general the present invention provides a process for forming conjugated diene polymer, the process comprising the step of polymerizing conjugated diene monomer in the presence of a catalytically effective amount of a catalyst composition formed by combining (a) a nickel-containing compound, (b) an alkylating agent, (c) a fluorine-containing compound, (d) a carboxylic acid, and (e) an alcohol.
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