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公开(公告)号:US20240287103A1
公开(公告)日:2024-08-29
申请号:US18583454
申请日:2024-02-21
发明人: Yuzo OKUMURA , Katsuya KONDO , Shuhei YAMADA , Atsushi RYOKAWA , Yuki FUKUI
IPC分类号: C07F7/10 , C09D5/00 , H01L21/304
CPC分类号: C07F7/10 , C09D5/00 , H01L21/304
摘要: The present invention is directed to a novel water-repellent protective film-forming agent and a novel water-repellent protective film-forming liquid chemical, each of which is for forming a water-repellent protective film on a silicon element-containing surface of a wafer, and a method of surface-treating a wafer with the use of the agent in liquid form or the liquid chemical. The water-repellent protective film-forming agent according to the present invention includes at least one kind of silicon compound selected from the group consisting of guanidine derivatives of the following general formula [1] and amidine derivatives of the following general formula [2].
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公开(公告)号:US20220020582A1
公开(公告)日:2022-01-20
申请号:US17295739
申请日:2019-10-21
发明人: Yuki FUKUI , Yuzo OKUMURA , Yoshiharu TERUI , Soichi KUMON
摘要: A bevel portion treatment agent composition of the present invention is a bevel portion treatment agent composition containing a silylating agent, which is used for treating a bevel portion of a wafer, in which a surface modification index Y and a surface modification index Z measured by a predetermined procedure have a characteristic of satisfying 0.5≤Y/Z≤1.0.
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公开(公告)号:US20210090881A1
公开(公告)日:2021-03-25
申请号:US16772024
申请日:2018-12-14
发明人: Yuki FUKUI , Yuzo OKUMURA , Yoshiharu TERUI , Soichi KUMON
摘要: According to the present disclosure, there are provided a surface treatment agent having the advantage that the raw material components can be dissolved in a short time during preparation of the surface treatment agent and capable of exerting a good water repellency imparting effect, and a method of manufacturing a surface-treated body with the use of the surface treatment agent. The surface treatment agent according to the present disclosure includes the following components: (I) at least one kind selected from the group consisting of silicon compounds represented by the following general formulas [1], [2] and [3]; (II) at least one kind selected from the group consisting of a nitrogen-containing heterocyclic compound represented by the following general formula [4], a nitrogen-containing heterocyclic compound represented by the following general formula [5], and imidazole; and (III) an organic solvent.
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公开(公告)号:US20200339850A1
公开(公告)日:2020-10-29
申请号:US16962159
申请日:2019-02-05
发明人: Yuzo OKUMURA , Katsuya KONDO , Shuhei YAMADA , Atsushi RYOKAWA , Yuki FUKUI
IPC分类号: C09K3/18 , H01L21/304 , H01L21/306
摘要: The present invention is directed to a liquid chemical for forming a water-repellent protective film on a silicon element-containing wafer surface, a method of preparing the liquid chemical and a method of manufacturing a surface-treated body with the use of the liquid chemical, wherein the liquid chemical includes the following components: (I) a silylation agent; (II) at least one kind of nitrogen-containing compound selected from the group consisting of those of the following general formulas [1] and [2]; and (III) an organic solvent.
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5.
公开(公告)号:US20230282473A1
公开(公告)日:2023-09-07
申请号:US17999361
申请日:2021-05-19
发明人: Yuzo OKUMURA , Yuki FUKUI , Saori SHIOTA , Yoshiharu TERUI , Soichi KUMON
IPC分类号: H01L21/02 , C09D183/08 , C09D7/20
CPC分类号: H01L21/0206 , C09D183/08 , C09D7/20
摘要: A surface treatment method for a semiconductor substrate of the present invention is a treatment method of treating a main surface of a semiconductor substrate that has, on the main surface of the substrate, a pattern formation region in which a pattern having a concave-convex structure with a pattern dimension of 30 nm or less is formed and a pattern non-formation region in which no pattern is formed, the method including a surface treatment step of bringing a surface treatment agent composition including a silylating agent into contact with the pattern formation region and the pattern non-formation region on the main surface of the semiconductor substrate, in which, with respect to a surface of the pattern non-formation region after the surface treatment step, an IPA contact angle with 2-propanol is 2° or more at a room temperature of 25° C. and/or a water contact angle with pure water is 50° or more at the room temperature of 25° C.
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公开(公告)号:US20190341246A1
公开(公告)日:2019-11-07
申请号:US16479330
申请日:2018-01-15
发明人: Yuzo OKUMURA , Yuki FUKUI , Hiroki FUKAZAWA , Soichi KUMON
IPC分类号: H01L21/02 , C09D7/62 , C09D7/20 , C09D127/06
摘要: According to the present invention, there is provided a water-repellent protective film-forming chemical liquid containing: a first solvent being at least one kind selected from the group consisting of an ether solvent and a hydrocarbon solvent; a second solvent being a glycol ether; a silylation agent represented by the following general formula [1]; and a base represented by the following general formula [2] and/or the following general formula [3], wherein the concentration of the second solvent in the chemical liquid is 1 to 30 mass %, wherein the concentration of the silylation agent in the chemical liquid is 2 to 15 mass %, wherein the concentration of the base in the chemical liquid is 0.05 to 2 mass %, and wherein the mass ratio of the silylation agent to the base is 4.5 or greater. (R1)a(H)bSi(OCOR2)4-a-b [1] (R3)c(H)dSi(X)4-c-d [2] [(R4)e(H)fSi]2NH [3]
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公开(公告)号:US20190074173A1
公开(公告)日:2019-03-07
申请号:US16084697
申请日:2017-03-07
发明人: Yuki FUKUI , Takashi SAIO , Atsushi RYOKAWA , Satoru NARIZUKA , Saori SHIOTA , Shota WATANABE , Shintaro SASAKI , Susumu IWASAKI
摘要: Disclosed are a water-repellent protective film forming agent for forming a water-repellent protective film on a silicon element-containing surface of a wafer and a water-repellent protective film forming liquid chemical in which the water-repellent protective film forming agent is dissolved in an organic solvent, characterized in that the water-repellent protective film forming agent consists of at least one kind of silicon compound selected from the group consisting of a sulfonimide derivative represented by the following general formula [1], a sulfonimide derivative represented by the following general formula [2] and a sulfonmethide derivative represented by the following general formula [3].
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公开(公告)号:US20230151163A1
公开(公告)日:2023-05-18
申请号:US17905978
申请日:2021-03-10
发明人: Yoshiharu TERUI , Soichi KUMON , Yuki FUKUI
CPC分类号: C08J5/18 , C08J3/09 , B01D7/00 , H01L21/02057
摘要: The sublimable film formation composition of the present invention includes a sublimable substance and a solvent in which a saturation solubility of the sublimable substance is more than 10% by mass.
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公开(公告)号:US20180308683A1
公开(公告)日:2018-10-25
申请号:US15753032
申请日:2016-08-10
发明人: Takashi SAIO , Yuzo OKUMURA , Yuki FUKUI , Hiroki FUKAZAWA , Tomohiro TAKATA , Soichi KUMON , Kazuyuki ABE , Shota WATANABE , Masayoshi IMACHI
CPC分类号: H01L21/02057 , B08B3/00 , C11D3/162 , H01L21/304 , H01L21/6704
摘要: To provide a water-repellent protective film-forming liquid chemical used in a process of cleaning a wafer by means of a cleaning machine whose liquid contact member contains a vinyl chloride resin. A liquid chemical is used, which includes an alkoxysilane represented by the following general formula [1]; at least one kind selected from the group consisting of a sulfonic acid represented by the following general formula [2], an anhydride of the sulfonic acid, a salt of the sulfonic acid and a sulfonic acid derivative represented by the following general formula [3]; and a diluent solvent containing at least one kind selected from the group consisting of a hydrocarbon, an ether and a thiol. (R1)aSi(H)b(OR2)4-a-b [1] R3—S(═O)2OH [2] R3—S(═O)2O—Si(H)3-c(R4)c [3]
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公开(公告)号:US20170287705A1
公开(公告)日:2017-10-05
申请号:US15512350
申请日:2015-09-11
发明人: Takashi SAIO , Yuzo OKUMURA , Yuki FUKUI , Soichi KUMON
IPC分类号: H01L21/02 , C07C309/03 , C07F7/08
CPC分类号: H01L21/02087 , C07C309/03 , C07F7/081 , H01L21/02057 , H01L21/0209 , H01L21/31138
摘要: Provided herein is a method for cleaning a wafer having a fine uneven surface pattern that at least partially contains a silicon element using a wafer cleaning device that includes a vinyl chloride resin as a liquid contacting member, the method including retaining a water-repellent protective film-forming chemical in at least a recessed portion of the uneven pattern to form a water-repellent protective film on a surface of the recessed portion, the water-repellent protective film-forming chemical containing: a monoalkoxysilane represented by the following general formula [1], (R1)aSi(H)3-a(OR2) [1]; a sulfonic acid represented by the following general formula [2], R3—S(═O)2OH [2]; and a diluting solvent, wherein the diluting solvent contains 80 to 100 mass % of alcohol with respect to the total 100 mass % of the diluting solvent.
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