Process for the treatment of organic amine compositions
    1.
    发明授权
    Process for the treatment of organic amine compositions 失效
    用于处理有机胺组合物的方法

    公开(公告)号:US4381223A

    公开(公告)日:1983-04-26

    申请号:US307223

    申请日:1981-09-30

    摘要: This invention provides for the separation of an amine composition undergoing processing at high temperatures and pressures which amine composition contains volatile components and less volatile components where the volatile components are desirable for further processing and/or utilization and the less volatile components are less desirable for further processing and/or utilization. The separation serves to divide the amine composition into two streams, one which is enriched in the volatile components and the other which is enriched in the less volatile components.

    摘要翻译: 本发明提供了在高温和高压下进行加工的胺组合物的分离,该胺组合物含有挥发性组分和较不易挥发的组分,其中挥发性组分对于进一步处理和/或利用是理想的,并且较不易挥发的组分对于进一步的 处理和/或利用。 该分离用于将胺组合物分成两股,其中富含挥发性组分的物质和富含较不易挥发组分的另一种。

    Continuous process for preparing alkanolamines
    2.
    发明授权
    Continuous process for preparing alkanolamines 失效
    链烷醇胺的连续工艺

    公开(公告)号:US4847418A

    公开(公告)日:1989-07-11

    申请号:US196802

    申请日:1988-05-16

    IPC分类号: C07C213/04

    CPC分类号: C07C213/04

    摘要: A continuous process is provided for preparing alkanolamines having a high yield of monoalkanolamine, which comprises continuously reacting a flowing stream of a homogeneous mixture of an alkylene oxide having from two to four carbon atoms and ammonia in a molar ratio of ammonia to alkylene oxide within the range from about 15:1 to about 50:1 at temperatures above the critical temperature of the mixture and at pressures above the critical pressure of the mixture and maintaining the mixture in a single phase having a density of at least 15 lbs./cu.ft. for the time necessary to form an alkanolamine product mixture containing at least about 65% by weight monoalkanolamine.

    摘要翻译: 提供了一种制备具有高产率的单链烷醇胺的链烷醇胺的连续方法,其包括将具有2至4个碳原子的烯化氧的均匀混合物的流动流与氨与氧化烯的摩尔比连续反应 在高于混合物的临界温度的温度下在约15:1至约50:1的范围内,并且在高于混合物的临界压力的压力下,将混合物保持在密度为至少15lbs./cu的单相中。 英尺 在形成含有至少约65重量%的单链烷醇胺的链烷醇胺产物混合物所需的时间。

    Process for preparing alkanolamines
    3.
    发明授权
    Process for preparing alkanolamines 失效
    烷醇胺的制备方法

    公开(公告)号:US4845296A

    公开(公告)日:1989-07-04

    申请号:US195395

    申请日:1988-05-12

    IPC分类号: C07C213/04

    CPC分类号: C07C213/04

    摘要: A process is provided for preparing alkanolamines having a high yield of monoalkanolamine which comprises reacting in a reaction mixture an alkylene oxide having from two to four carbon atoms with ammonia in a molar ratio of ammonia to alkylene oxide within the range from about 15.1 to about 50.1 at temperatures above the critical temperature of the reaction mixture and at pressures above the critical pressure of the reaction mixture and high enough to maintain the reaction mixture at sufficiently high fluid densities.

    摘要翻译: 提供了一种制备具有高产率的单烷醇胺的链烷醇胺的方法,其包括在反应混合物中使具有2至4个碳原子的环氧烷与氨与氧化烯的摩尔比在约15.1至约50.1的范围内反应 在高于反应混合物的临界温度的温度和高于反应混合物的临界压力的压力下,并且足够高以将反应混合物保持在足够高的流体密度。

    Process for ionic liquid catalyst regeneration
    6.
    发明授权
    Process for ionic liquid catalyst regeneration 有权
    离子液体催化剂再生方法

    公开(公告)号:US07732364B2

    公开(公告)日:2010-06-08

    申请号:US12003578

    申请日:2007-12-28

    IPC分类号: B01J38/10

    摘要: A regeneration process for re-activating an ionic liquid catalyst, which is useful in a variety of reactions, especially alkylation reactions, and which has been deactivated by conjunct polymers. The process includes a reaction step and a solvent extraction step. The process comprises (a) providing the ionic liquid catalyst, wherein at least a portion of the ionic liquid catalyst is bound to conjunct polymers; and (b) reacting the ionic liquid catalyst with aluminum metal to free the conjunct polymers from the ionic liquid catalyst in a stirred reactor or a fixed reactor. The conjunct polymer is then separated from the catalyst phase by solvent extraction in a stirred extraction or packed column.

    摘要翻译: 用于重新活化离子液体催化剂的再生方法,其可用于各种反应,特别是烷基化反应,并且已经通过结合聚合物失活。 该方法包括反应步骤和溶剂萃取步骤。 该方法包括(a)提供离子液体催化剂,其中至少一部分离子液体催化剂与结合聚合物结合; 和(b)使离子液体催化剂与铝金属反应,以在搅拌反应器或固定反应器中从离子液体催化剂中释放结合的聚合物。 然后在搅拌的萃取或填充柱中通过溶剂萃取将结合的聚合物与催化剂相分离。