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    Hydroxy-functional poly(amide ethers) as thermoplastic barrier resins
    1.
    发明授权
    Hydroxy-functional poly(amide ethers) as thermoplastic barrier resins 失效
    羟基官能团（酰胺类）作为热塑性树脂树脂

    公开(公告)号：US5143998A

    公开(公告)日：1992-09-01

    申请号：US759288

    申请日：1991-09-13

    申请人： David J. Brennan ,  Anthony P. Haag ,  Jerry E. White

    发明人： David J. Brennan ,  Anthony P. Haag ,  Jerry E. White

    IPC分类号： C08G59/62 ,  C08G69/40

    CPC分类号： C08G59/621 ,  C08G69/40

    摘要： Hydroxy-functional poly(amide-ethers) are fabricated into articles such as rigid containers and flexible films exhibiting high barrier to oxygen transmission in both dry and moist environments. For example, a polymer prepared by reacting the diglycidyl ether of 4,4'-isopropylidene bisphenol with .alpha.,.alpha.'-bis(4-hydroxybenzamido)-1,3-xylene exhibits especially high barrier.

    摘要翻译： 羟基官能的聚（酰胺 - 醚）被制成制品，例如刚性容器和在干燥和潮湿的环境中对透氧具有高阻隔性的柔性膜。 例如，通过使4,4'-异亚丙基双酚的二缩水甘油醚与α，α'-双（4-羟基苯甲酰氨基）-1,3-二甲苯反应而制备的聚合物显示出特别高的阻隔性。

    Amide and hydroxymethyl functionalized polyethers as thermoplastic barrier resins
    2.
    发明授权
    Amide and hydroxymethyl functionalized polyethers as thermoplastic barrier resins 失效
    酰胺和羟甲基官能化聚醚作为热塑性阻隔树脂

    公开(公告)号：US5115075A

    公开(公告)日：1992-05-19

    申请号：US520689

    申请日：1990-05-08

    申请人： David J. Brennan ,  Jerry E. White ,  Anthony P. Haag ,  Shari L. Kram

    发明人： David J. Brennan ,  Jerry E. White ,  Anthony P. Haag ,  Shari L. Kram

    IPC分类号： C07C235/34 ,  C07D303/24 ,  C08G59/62

    CPC分类号： C08G59/621 ,  C07C235/34 ,  C07D303/24

    摘要： Polyethers having improved barrier to oxygen are normally solid, thermoplastic polyethers having aromatic ether repeating units in their backbones and pendent hydroxyl moieties and pendent amido, N-substituted amido and/or hydroxyalkyl moieties. Such polyethers are prepared by reacting diglycidyl ethers of dihydric aromatic compounds such as diglycidyl ether of bisphenol A with dihydric phenols having pendent amido, N-substituted amido and/or hydroxyalkyl moieties such as 2,2-bis(4-hydroxyphenyl)acetamide and 3,5-dihydroxybenzamide.

    摘要翻译： 具有改善的对氧的屏障的聚醚通常是固体，其主链中具有芳族醚重复单元的热塑性聚醚和侧挂的羟基部分以及侧链酰胺基，N-取代的酰胺基和/或羟烷基部分。 这样的聚醚通过使二羟基芳族化合物的二缩水甘油醚如双酚A的二缩水甘油醚与具有侧枝酰氨基的二元酚，N-取代的酰氨基和/或羟烷基部分如2,2-双（4-羟基苯基）乙酰胺和3 ，5-二羟基苯甲酰胺。

    Amide and hydroxymethyl functionalized polyethers as thermoplastic barrier resins
    3.
    发明授权
    Amide and hydroxymethyl functionalized polyethers as thermoplastic barrier resins 失效
    酰胺和羟甲基官能化聚醚作为热塑性阻隔树脂

    公开(公告)号：US5218075A

    公开(公告)日：1993-06-08

    申请号：US836626

    申请日：1992-02-13

    申请人： David J. Brennan ,  Jerry E. White ,  Anthony P. Haag ,  Shari L. Kram

    发明人： David J. Brennan ,  Jerry E. White ,  Anthony P. Haag ,  Shari L. Kram

    IPC分类号： C07C235/34 ,  C07D303/24 ,  C08G59/62

    CPC分类号： C07D303/24 ,  C07C235/34 ,  C08G59/621

    摘要： Polyethers having improved barrier to oxygen are normally solid, thermoplastic polyethers having aromatic ether repeating units in their backbones and pendent hydroxyl moieties and pendent amido, N-substituted amido and/or hydroxyalkyl moieties. Such polyethers are prepared by reacting diglycidyl ethers of dihydric aromatic compounds such as the diglycidyl ether of bisphenol A with dihydric phenols having pendent amido, N-substituted amido and/or hydroxyalkyl moieties such as 2,2-bis(4-hydroxyphenyl)acetamide and 3,5-dihydroxybenzamide.

    摘要翻译： 具有改善的对氧的屏障的聚醚通常是固体，其主链中具有芳族醚重复单元的热塑性聚醚和侧挂的羟基部分以及侧链酰胺基，N-取代的酰胺基和/或羟烷基部分。 这样的聚醚通过使二羟基芳族化合物的二缩水甘油醚如双酚A的二缩水甘油醚与具有侧酰氨基的二元酚，N-取代的酰氨基和/或羟烷基部分如2,2-双（4-羟基苯基）乙酰胺和 3,5-二羟基苯甲酰胺。

    Process for the preparation of thermoplastic poly(hydroxy ethers)
    4.
    发明授权
    Process for the preparation of thermoplastic poly(hydroxy ethers) 失效
    制备热塑性聚（羟基醚）的方法

    公开(公告)号：US5401814A

    公开(公告)日：1995-03-28

    申请号：US135712

    申请日：1993-10-13

    申请人： Joseph A. Schomaker ,  Jerry E. White ,  Anthony P. Haag ,  Ha Q. Pham

    发明人： Joseph A. Schomaker ,  Jerry E. White ,  Anthony P. Haag ,  Ha Q. Pham

    IPC分类号： C08G59/62 ,  C08G59/68 ,  C08G65/28

    CPC分类号： C08G59/688 ,  C08G59/621

    摘要： Poly(hydroxy ethers) are prepared by reacting a dihydric phenol with a diepoxide in the presence of a catalyst selected from the group consisting of bis(trihydrocarbylphosphoranylidene)ammonium salt, bis[tris(dihydrocarbylamino)phosphoranylidene]ammonium salt, and tetrakis[tris(dihydrocarbylamino)phosphoranylideneamino]phosphonium salt. The reaction between the dihydric phenol and the diepoxide is conducted in an ether or hydroxy ether solvent at a temperature sufficiently high to produce a poly(hydroxy ether). Polymers prepared by the new process are more highly branched than those produced by known methods.

    摘要翻译： 聚（羟基醚）通过二选苯酚与二环氧化物在选自双（三烃基亚正膦基）铵盐，双[三（二烃基氨基）亚正膦基]铵盐和四[三 二烃基氨基）正膦亚基氨基]鏻盐。 二羟基酚和二环氧化物之间的反应在足够高的温度下在醚或羟基醚溶剂中进行以产生聚（羟基醚）。 通过新方法制备的聚合物比通过已知方法制备的聚合物分枝得多。

    Hydroxy-phenoxyether polymer thermoplastic composites
    7.
    发明授权
    Hydroxy-phenoxyether polymer thermoplastic composites 失效
    羟基 - 苯氧基醚聚合物热塑性复合材料

    公开(公告)号：US6011111A

    公开(公告)日：2000-01-04

    申请号：US138300

    申请日：1993-10-18

    申请人： David J. Brennan ,  Jerry E. White ,  Daryl R. Calhoun

    发明人： David J. Brennan ,  Jerry E. White ,  Daryl R. Calhoun

    IPC分类号： C08K7/04 ,  C08K3/40 ,  C08K3/04

    CPC分类号： C08K7/04

    摘要： A thermoplastic composite is prepared by applying a hydroxy-phenoxyether polymer onto the surface of reinforcing fibers or by the in-situ polymerization of mixtures of diepoxides and difunctional species in the presence of reinforcing fibers. The composites can be molded into shaped articles useful for structural materials and parts by conventional thermoforming or other fabrication techniques.

    摘要翻译： 通过在增强纤维的表面上施加羟基 - 苯氧基醚聚合物或通过在增强纤维的存在下二环氧化物和双官能物质的混合物的原位聚合来制备热塑性复合材料。 复合材料可以通过常规热成型或其他制造技术模制成用于结构材料和部件的成型制品。

    Bisbenzocyclobutene thermosetting compounds and process for preparing the same
    10.
    发明授权
    Bisbenzocyclobutene thermosetting compounds and process for preparing the same 失效
    双苯并环丁烯热固性化合物及其制备方法

    公开(公告)号：US5391650A

    公开(公告)日：1995-02-21

    申请号：US998495

    申请日：1992-12-30

    申请人： David J. Brennan ,  Jerry E. White ,  Daniel M. Scheck ,  Robert A. Kirchhoff ,  Charles Z. Hotz

    发明人： David J. Brennan ,  Jerry E. White ,  Daniel M. Scheck ,  Robert A. Kirchhoff ,  Charles Z. Hotz

    IPC分类号： C07C43/23 ,  C07C69/00 ,  C07C69/76 ,  C07C69/80 ,  C07C69/92 ,  C07C215/18 ,  C07C217/34 ,  C07C233/25 ,  C07C235/50 ,  C07C311/17 ,  C07C317/22 ,  C07C323/12 ,  C07D295/092 ,  C08G59/14 ,  C08G59/24 ,  C08G59/32 ,  C08G61/00 ,  C08G61/12 ,  C08G59/04

    CPC分类号： C07D295/088 ,  C07C215/18 ,  C07C217/34 ,  C07C233/25 ,  C07C235/50 ,  C07C311/17 ,  C07C317/22 ,  C07C323/12 ,  C07C43/23 ,  C07C69/16 ,  C07C69/76 ,  C07C69/80 ,  C07C69/92 ,  C08G59/1438 ,  C08G59/24 ,  C08G59/3218 ,  C08G61/00 ,  C08G61/12 ,  C07C2102/06 ,  C07C2103/18

    摘要： A compound having at least one 2-hydroxy-1,3-propylidene, 2-acetoxy-1,3-propylidene, or 2-alkoxy-1,3-propylidene moiety between two benzocyclobutene end moieties is prepared by (a) contacting a diepoxide species with a benzocyclobutene species containing a functionality capable of reacting with an epoxy group, (b) contacting an epoxy-containing benzocyclobutene species with a species containing two functionalities capable of reacting with an epoxy group, (c) contacting an epoxy-containing benzocyclobutene species with a benzocyclobutene species containing a functionality capable of reacting with an epoxy group, (d) contacting epichlorohydrin with benzocyclobutene species capable of reacting with an epoxy group, or (e) contacting epihalohydrin with benzocyclobutene species and difunctional species, wherein both species contain functionalities capable of reacting with epoxy groups. Each benzocyclobutene moiety is attached to the 2-hydroxy-1,3-propylidene moiety at the six-membered ring through oxygen or sulfur atoms, carboxyl, N-alkylimino, or 1,3-dioxyphenylene units. The unit linking the two benzocyclobutene moieties optionally contains aromatic moieties. The polymers prepared from the compounds are suitable for use in composites, coatings, adhesives, and binders. The polymers have outstanding processability and are mainly non-crystalline materials with low melt viscosities prior to the onset of curing.

    摘要翻译： 通过以下步骤制备在两个苯并环丁烯末端部分之间具有至少一个2-羟基-1,3-亚丙基，2-乙酰氧基-1,3-亚丙基或2-烷氧基-1,3-亚丙基部分的化合物：（a） 具有能够与环氧基反应的官能团的苯并环丁烯物质的二环氧化物物质，（b）使含环氧基的苯并环丁烯物质与能够与环氧基反应的两种官能团的物质接触，（c）使含环氧基的苯并环丁烯 具有能够与环氧基反应的官能团的苯并环丁烯物质的物质，（d）将表氯醇与能够与环氧基反应的苯并环丁烯物质接触，或（e）使表卤代醇与苯并环丁烯物质和双官能物质接触，其中两种物质都含有官能团 能够与环氧基反应。 每个苯并环丁烯部分通过氧或硫原子连接到六元环上的2-羟基-1,3-亚丙基部分，羧基，N-烷基亚氨基或1,3-二氧代亚苯基单元。 连接两个苯并环丁烯部分的单元任选地含有芳族部分。 由化合物制备的聚合物适用于复合材料，涂料，粘合剂和粘合剂。 聚合物具有优异的可加工性，并且主要是在固化开始之前具有低熔融粘度的非结晶材料。