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公开(公告)号：US08846817B2
公开(公告)日：2014-09-30
申请号：US13294926
申请日：2011-11-11
申请人： Dorie J. Yontz , Brian D. Mullen , Cora M. Leibig , Marc D. Rodwogin , Vivek Badarinarayana , Feng Jing , Friederike T. Stollmaier
发明人： Dorie J. Yontz , Brian D. Mullen , Cora M. Leibig , Marc D. Rodwogin , Vivek Badarinarayana , Feng Jing , Friederike T. Stollmaier
IPC分类号： C08F8/12 , C08F218/10 , B01J20/26 , C08F224/00 , B01J20/30 , C08F220/16 , B01J20/28 , C08F226/10 , C08F220/06
CPC分类号： B01J20/3042 , B01J20/264 , B01J20/267 , B01J20/2803 , B01J2220/46 , B01J2220/68 , C08F8/44 , C08F220/06 , C08F220/16 , C08F224/00 , C08F226/10 , C08F2800/10
摘要： An ionic polymer of formula VI wherein each b=0 or 1; X is hydrogen, 1/z of a metal ion of charge z, a protonated nitrogen base, or a tetrasubstituted organic ammonium compound; the molar ratio of q:r:s:t=(100-0.1):(0-99.9):(0-50):(0-30); R1, R2 and R3 are hydrogen or C1-4 alkyl; R4, R5, R6 and R7 are hydrogen, C1-4 alkyl or F, wherein F is a functional group that imparts a property to polymer VI, at least one and no more than two of R4, R5, R6 and R7 are F and F is the same or different; G is a single bond or a C1-30 hydrocarbyl group; and for each instance of t when t is not zero, c=0-5 and d=0-5, provided that c+d=1-5, and wherein q, r and s as present in c are independent of any other value of q, r and s.
摘要翻译： 式VI的离子聚合物，其中每个b = 0或1; X是氢，电荷z的金属离子的1 / z，质子化的氮碱或四取代的有机铵化合物; q：r：s：t =（100-0.1）：（0-99.9）：（0-50）：（0-30）的摩尔比; R1，R2和R3是氢或C1-4烷基; R4，R5，R6和R7是氢，C1-4烷基或F，其中F是赋予聚合物VI性质的官能团，R 4，R 5，R 6和R 7中的至少一个不超过两个是F， F相同或不同; G是单键或C1-30烃基; 并且对于t的每个实例，当t不为零时，c = 0-5和d = 0-5，条件是c + d = 1-5，并且其中存在于c中的q，r和s独立于任何其它 q，r和s的值。
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公开(公告)号：US20120118832A1
公开(公告)日：2012-05-17
申请号：US13294926
申请日：2011-11-11
申请人： Dorie J. Yontz , Brian D. Mullen , Cora M. Leibig , Marc D. Rodwogin , Vivek Badarinarayana , Feng Jing , Friederike T. Stollmaier
发明人： Dorie J. Yontz , Brian D. Mullen , Cora M. Leibig , Marc D. Rodwogin , Vivek Badarinarayana , Feng Jing , Friederike T. Stollmaier
IPC分类号： B01D21/01 , B01J20/26 , C09K3/00 , C08F218/10 , C08F8/44
CPC分类号： B01J20/3042 , B01J20/264 , B01J20/267 , B01J20/2803 , B01J2220/46 , B01J2220/68 , C08F8/44 , C08F220/06 , C08F220/16 , C08F224/00 , C08F226/10 , C08F2800/10
摘要： An ionic polymer of formula VI wherein each b=0 or 1; X is hydrogen, 1/z of a metal ion of charge z, a protonated nitrogen base, or a tetrasubstituted organic ammonium compound; the molar ratio of q:r:s:t=(100-0.1):(0-99.9):(0-50):(0-30); R1, R2 and R3 are hydrogen or C1-4 alkyl; R4, R5, R6 and R7 are hydrogen, C1-4 alkyl or F, wherein F is a functional group that imparts a property to polymer VI, at least one and no more than two of R4, R5, R6 and R7 are F and F is the same or different; G is a single bond or a C1-30 hydrocarbyl group; and for each instance of t when t is not zero, c=0-5 and d=0-5, provided that c+d=1-5, and wherein q, r and s as present in c are independent of any other value of q, r and s.
摘要翻译： 式VI的离子聚合物，其中每个b = 0或1; X是氢，电荷z的金属离子的1 / z，质子化的氮碱或四取代的有机铵化合物; q：r：s：t =（100-0.1）：（0-99.9）：（0-50）：（0-30）的摩尔比; R1，R2和R3是氢或C1-4烷基; R4，R5，R6和R7是氢，C1-4烷基或F，其中F是赋予聚合物VI性质的官能团，R 4，R 5，R 6和R 7中的至少一个不超过两个是F， F相同或不同; G是单键或C1-30烃基; 并且对于t的每个实例，当t不为零时，c = 0-5和d = 0-5，条件是c + d = 1-5，并且其中存在于c中的q，r和s独立于任何其它 q，r和s的值。
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3.发明申请公开(公告)号：US20120121911A1
公开(公告)日：2012-05-17
申请号：US13294854
申请日：2011-11-11
IPC分类号： B32B27/36 , C07D317/30 , C08J9/35 , C08K5/156 , C08G63/16 , C08G14/02 , C08G18/32 , C09K3/00 , C09D163/00 , C09D175/06 , C08G64/00 , B05D7/24 , B05D3/00 , B32B27/28 , C07D407/12
CPC分类号： C08K5/1565 , C07D317/02 , C07D317/14 , C07D317/30 , C08G2/32 , C08G18/3218 , C08G63/668 , C08G63/672 , C08G63/91 , C08G64/0208 , C08G64/42 , C08G2101/0025 , C08L59/00 , C08L67/00 , C09D159/00 , C09D167/00 , Y02P20/582 , Y10T428/31507 , Y10T428/31786
摘要： Disclosed herein is a polyhydroxy ketal adduct obtained by the esterification of a hydrocarbon polyol by at least 1.5 equivalents of a ketocarboxy to produce an intermediate ketocarboxylic ester. The intermediate polyketocarboxylic ester is then ketalized to produce the polyhydroxyketal adduct, which can be used to provide a polymeric composition.
摘要翻译： 本文公开了通过烃多元醇通过至少1.5当量的酮羧基酯化以产生中间体酮羧酸酯而获得的多羟基缩酮加合物。 然后中间体多酮羧酸酯被缩醛化以产生可用于提供聚合物组合物的多羟基缩酮加合物。
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4.发明授权公开(公告)号：US09187598B2
公开(公告)日：2015-11-17
申请号：US13294854
申请日：2011-11-11
IPC分类号： C08G63/91 , C07D317/02 , C07D317/14 , C07D317/30 , C08G2/32 , C08G63/668 , C08G64/02 , C08G64/42 , C08L59/00 , C09D159/00 , C09D167/00 , C08G18/32 , C08L67/00 , C08G101/00
CPC分类号： C08K5/1565 , C07D317/02 , C07D317/14 , C07D317/30 , C08G2/32 , C08G18/3218 , C08G63/668 , C08G63/672 , C08G63/91 , C08G64/0208 , C08G64/42 , C08G2101/0025 , C08L59/00 , C08L67/00 , C09D159/00 , C09D167/00 , Y02P20/582 , Y10T428/31507 , Y10T428/31786
摘要： Disclosed herein is a polyhydroxy ketal adduct obtained by the esterification of a hydrocarbon polyol by at least 1.5 equivalents of a ketocarboxy to produce an intermediate ketocarboxylic ester. The intermediate polyketocarboxylic ester is then ketalized to produce the polyhydroxyketal adduct, which can be used to provide a polymeric composition.
摘要翻译： 本文公开了通过烃多元醇通过至少1.5当量的酮羧基酯化以产生中间体酮羧酸酯而获得的多羟基缩酮加合物。 然后中间体多酮羧酸酯被缩醛化以产生可用于提供聚合物组合物的多羟基缩酮加合物。
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公开(公告)号：US20120118201A1
公开(公告)日：2012-05-17
申请号：US13294690
申请日：2011-11-11
IPC分类号： C08K5/1565 , C08L67/04 , C08L27/06 , C08L23/00 , C08L69/00 , C08L79/08 , C08L25/06 , C08L77/00 , C08L1/02 , C08L81/04 , C08L81/06 , C07D407/12 , C08L83/04
CPC分类号： C07D407/12 , C08K5/1565 , C08L59/02 , C08L77/00 , C08L79/08 , Y02P20/582 , C08L27/06
摘要： Disclosed herein is a polyketal adduct obtained by forming an ester between a hydrocarbon polyol and a ketocarboxylic acid to produce an intermediate polyketocarboxylic ester. The intermediate polyketocarboxylic ester can be purified via crystallization to achieve purities of greater than 99.0% and then ketalized to produce the polyketal adduct, which can be used in polymer compositions. The polyketal adduct I is obtained at high purity and at high yield.
摘要翻译： 本文公开了通过在烃多元醇和酮羧酸之间形成酯以产生中间体多酮羧酸酯而获得的聚缩酮加成物。 可以通过结晶纯化中间体多酮羧酸酯以实现大于99.0％的纯度，然后缩醛化以产生可用于聚合物组合物中的聚缩酮加合物。 以高纯度和高收率获得聚缩酮加成物I.
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公开(公告)号：US09212176B2
公开(公告)日：2015-12-15
申请号：US13294690
申请日：2011-11-11
申请人： Brian D. Mullen , Marc D. Scholten , Tara J. Mullen , Cora M. Leibig , Vivek Badarinarayana , Matthew J. Tjosaas
发明人： Brian D. Mullen , Marc D. Scholten , Tara J. Mullen , Cora M. Leibig , Vivek Badarinarayana , Matthew J. Tjosaas
IPC分类号： C07D407/12 , C08K5/1565 , C08L79/08 , C08L77/00 , C08L59/02
CPC分类号： C07D407/12 , C08K5/1565 , C08L59/02 , C08L77/00 , C08L79/08 , Y02P20/582 , C08L27/06
摘要： Disclosed herein is a polyketal adduct obtained by forming an ester between a hydrocarbon polyol and a ketocarboxylic acid to produce an intermediate polyketocarboxylic ester. The intermediate polyketocarboxylic ester can be purified via crystallization to achieve purities of greater than 99.0% and then ketalized to produce the polyketal adduct, which can be used in polymer compositions. The polyketal adduct I is obtained at high purity and at high yield.
摘要翻译： 本文公开了通过在烃多元醇和酮羧酸之间形成酯以产生中间体多酮羧酸酯而获得的聚缩酮加成物。 可以通过结晶纯化中间体多酮羧酸酯以实现大于99.0％的纯度，然后缩醛化以产生可用于聚合物组合物中的聚缩酮加合物。 以高纯度和高收率获得聚缩酮加成物I.
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7.发明授权Water reducible coating compositions including carboxy ester ketals, methods of manufacture, and uses thereof 有权包含羧酯缩酮的可水稀释涂料组合物，其制备方法及其应用公开(公告)号：US08728625B2
公开(公告)日：2014-05-20
申请号：US13276091
申请日：2011-10-18
CPC分类号： C09D167/00 , C08G18/0866 , C08K5/06 , C08K5/156 , C09D167/08 , C09D175/06 , Y10T428/31855 , C08K5/0041
摘要： A water-reducible coating composition includes a water-reducible polymer binder; water; and a ketal adduct of formula (1) as well as coated substrates and films formed from the compositions. The films are useful as paints, stains, and clear-coats.
摘要翻译： 水可稀释的涂料组合物包括水可稀释的聚合物粘合剂; 水; 和式（1）的缩酮加合物以及由组合物形成的涂覆的基底和薄膜。 这些电影可用作油漆，污渍和清漆。
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公开(公告)号：US20120128614A1
公开(公告)日：2012-05-24
申请号：US13322948
申请日：2010-05-28
CPC分类号： C11D3/2093 , A61K8/4973 , A61K8/498 , A61Q1/14 , A61Q5/02 , A61Q19/10 , C11D3/2096 , C11D3/43 , C11D17/0017
摘要： A cleaning composition can comprise aqueous, nonaqueous liquid, or solid formulations The formulations can contain a surfactant and a solvent The solvent has been shown to have utility in promoting removal, solubilizing or cleaning undesirable soil residues from a number of substrates The solvent materials can be used as a component of an aqueous solution, can be combined in a solid or powdered formulation as an encapsulated solvent or can be combined in a solid or powdered formulation as a solvent absorbed on a solid earner The aqueous formulations can be made in the form of a concentrate The cleaner can be combined with water to form an active cleaning solution that can be applied in a variety of cleaning processes The cleaner can contain additional ingredients including surfactants, builders, sequestrates, bleaches, biocides, to be found in cleaners of general and specific applications Personal care cleaning products are also described.
摘要翻译： 清洁组合物可以包含水性，非水性液体或固体制剂。制剂可以含有表面活性剂和溶剂。已经显示溶剂可用于促进从许多底物中去除，增溶或清洁不期望的土壤残留物溶剂材料可以是 用作水溶液的组分，可以作为包封的溶剂组合在固体或粉末制剂中，或者可以作为吸收在固体载体上的溶剂结合在固体或粉末制剂中。水性制剂可以以 浓缩物清洁剂可以与水结合形成可用于各种清洁过程的主动清洁溶液清洁剂可以含有其他成分，包括表面活性剂，助洗剂，螯合剂，漂白剂，杀生物剂，可用于一般清洁剂和 具体应用也描述了个人护理清洁产品。
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公开(公告)号：US10316009B2
公开(公告)日：2019-06-11
申请号：US15754060
申请日：2016-08-19
申请人： GFBIOCHEMICALS LIMITED , Brian D. Mullen , Cora M. Leibig , Roger Schoonover , Kevin Jon Bechtold
IPC分类号： C07D307/50 , C07D307/48 , C07D307/54 , C07C59/185
摘要： The invention relates generally to the preparation of hydroxymethyl furfural derivatives such as 5-carboxymethyl furfural derivatives, ethers such as 5-alkoxymethyl furfural derivatives, 5-hydroxymethyl furfural, levulinic acid, levulinic acid esters, and/or formic acid, formic acid esters from sugar.
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公开(公告)号：US08507718B2
公开(公告)日：2013-08-13
申请号：US13294751
申请日：2011-11-11
申请人： Brian D. Mullen , Cora M. Leibig , Leo E. Manzer
发明人： Brian D. Mullen , Cora M. Leibig , Leo E. Manzer
IPC分类号： C07C69/716 , C07C51/36
CPC分类号： C07C69/738 , C07C51/09 , C07C51/493 , C07C67/08 , C07C67/52 , C07C69/716 , Y02P20/582 , C07C59/185
摘要： Ketocarboxylic acids such as levulinic acid can be efficiently purified in high yield by esterification with a hydrocarbon polyol to the corresponding polyketocarboxylic ester, which can be readily purified, for example recrystallized. After purification, the ketocarboxylic ester can be hydrolyzed to provide pure ketocarboxylic acid, or a salt thereof, after removal of the esterifying hydrocarbon polyol, or used for other synthetic transformations. Advantageously, the polyketocarboxylic esters, ketocarboxylic acids, and salts thereof produced by this method are obtained in high purity.
摘要翻译： 酮羧酸如乙酰丙酸可以通过用烃多元醇与相应的聚酮羧酸酯酯化而以高收率有效地纯化，其可以容易地纯化，例如重结晶。 纯化后，在除去酯化烃多元醇之后，可以将酮羧酸酯水解以提供纯酮羧酸或其盐，或用于其它合成转化。 有利地，以高纯度获得通过该方法制备的多酮羧酸酯，酮羧酸及其盐。
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