摘要:
A method and apparatus for sorting and performing redundant analysis of particles in an aerosol is disclosed. Redundant analysis reduces the possibility of false positive analyses, which is advantageous in the art. The apparatus may comprise an aerosol concentrator, an optical particle analyzer, an electrosprayer and a charged particle analyzer. A method according to the invention may comprise delivering a concentrated aerosol stream to an optical particle analyzer; analyzing each particle of interest and selectively triggering an electrosprayer to electrospray each particle of interest; adding a charge to the particle, which is then moved by electrostatic forces to a charged particle analyzer; and performing a second, redundant analysis of each charged particle collected on the charged particle analyzer to confirm the identity of the particle of interest. The apparatus and method may also be adapted to perform redundant analysis of disguised particles that are coated to disguise their payload.
摘要:
The Reactive Bed Plasma is a novel air purification and material processingevice which may efficiently treat both toxic chemicals and hazardous aerosols. The Reactive Bed Plasma device embodies an active alternating current discharge plasma permeating a dielectric packed bed. Advantages of this device include an increased power efficiency by the elimination of dielectric barriers (characteristic of ozonizer devices); a selectively increased residence time of contaminants in the active plasma zones through interaction with the packing material (analogous to chromotographic separations); also a reduced size and power consumption while maintaining high processing efficiency. Further advantages include greatly increased operating lifetime without failure due to electrical arcing (problematic with ozonizers) or poisoning of the packing surfaces (problematic with adsorbents and catalysts); an achievement of a high processing efficiency at low temperature; a control over plasma air by-product formation; and the promotion of chemical and physical reactions simultaneously in a single device heretofore requiring several vastly different devices (promoting photoionoization, catalytic oxidation, plasma-induced decomposition, combustion, electrostatic precipitation, or plasma etching processes).
摘要:
A method and apparatus for sorting and performing redundant analysis of particles in an aerosol is disclosed. Redundant analysis reduces the possibility of false positive analyses, which is advantageous in the art. The apparatus may comprise an aerosol concentrator, an optical particle analyzer, an electrosprayer and a charged particle analyzer. A method according to the invention may comprise delivering a concentrated aerosol stream to an optical particle analyzer; analyzing each particle of interest and selectively triggering an electrosprayer to electrospray each particle of interest; adding a charge to the particle, which is then moved by electrostatic forces to a charged particle analyzer; and performing a second, redundant analysis of each charged particle collected on the charged particle analyzer to confirm the identity of the particle of interest. The apparatus and method may also be adapted to perform redundant analysis of disguised particles that are coated to disguise their payload.
摘要:
A separation plate (10) includes a first surface and an opposing second surface. Plural pairs of a nozzle (14) and a virtual impactor (16) are provided on the first surface. Each nozzle tapers from an inlet end (14a) to an outlet end (14b). Each virtual impactor comprises a pair of generally fin-shaped projections (24). Each fin-shaped projection includes an inner wall (26) and a convex outer wall (28). The inner walls of the fin-shaped projections of a virtual impactor face each other to define a minor flow passage (30) therebetween. The convex outer walls of the fin-shaped projections of a virtual impactor cooperatively present a convex surface including a virtual impact void therethrough. The virtual impact void defines an inlet end of the minor flow passage. A virtual impactor body (33) is provided between adjacent virtual impactors (16). When a particle-laden fluid stream (23) is caused to flow through the nozzles and advance to the virtual impactors, a major portion of the fluid containing a minor portion of particles flows around the virtual impactors, is blocked by the virtual impactor bodies, and redirected from the first surface through a suitable major flow outlet. A minor portion of the fluid containing a major portion of particles enters the virtual impact voids, advances through the minor flow passages, and exits therefrom, where it can be collected, analyzed, or processed further in any other manner.
摘要:
The invention is a microcomponent sheet architecture wherein macroscale unit processes are performed by microscale components. The sheet architecture may be a single laminate with a plurality of separate microcomponent sections or the sheet architecture may be a plurality of laminates with one or more microcomponent sections on each laminate. Each microcomponent or plurality of like microcomponents perform at least one chemical process unit operation. A first laminate having a plurality of like first microcomponents is combined with at least a second laminate having a plurality of like second microcomponents thereby combining at least two unit operations to achieve a system operation.
摘要:
Fluids are atomized using a miniaturized electrostatic microinjector. The microinjectors are capable of producing uniform droplets in several spray modes, and metering and dispersing very small volume fluids. The atomizer is useful in carburetion systems for internal combustion engines, to prepare samples for analytical methods such as MALDI, for fluid filtration and separation, and in other applications.
摘要:
A separation plate (10) includes a first surface (10a) and an opposing second surface. A plurality of teardrop-shaped virtual impactor projections (12) are provided on the first surface, preferably in a plurality of rows (13a, 13b, 13c). Each projection includes a convex leading profile (18) facing a fluid stream (16), and two concave side surfaces (19) that are positioned to define a tapered downstream portion. The convex leading profile may include a concave portion (20). The concave portion defines a virtual impact void therethrough. The virtual impact void defines a terminal end of a passageway that extends through the separation plate to communicate with the second surface. When particle-laden fluid is caused to flow along the first surface, a major portion of the fluid containing a minor portion of particles flows around the teardrop-shaped virtual impactor projections along the first surface. A minor portion of the fluid containing a major portion of particles is collected near the convex leading profiles of the projections, and enters the concave portions and the virtual impact voids of the projections. The minor portion of the fluid then travels through the passageways to the second surface of the separation plate, where it can be collected, analyzed, or processed further.
摘要:
A micro-machined virtual impactor device to permit the separation, collection and concentration of a significant portion of environmental particulates having a diameter of less than ten microns and its method of operation. The device includes a plurality of projections, each having a virtual impact surface that defines an aperture in a stagnant zone of fluid flow. A major portion of the particulate material is concentrated into a minor portion of the fluid which is processed through the aperture, where it is collected for subsequent analysis.
摘要:
A nanofluid contact potential difference cell comprises a cathode with a lower work function and an anode with a higher work function separated by a nanometer-scale spaced inter-electrode gap containing a nanofluid with intermediate work function nanoparticle clusters. The cathode comprises a refractory layer and a thin film of electrosprayed dipole nanoparticle clusters partially covering a surface of the refractory layer. A thermal power source, placed in good thermal contact with the cathode, drives an electrical current through an electrical circuit connecting the cathode and anode with an external electrical load in between. A switch is configured to intermittently connect the anode and the cathode to maintain non-equilibrium between a first current from the cathode to the anode and a second current from the anode to the cathode.
摘要:
A virtual impactor device having reduced fouling includes injection ports within the separation zone to redirect particles that otherwise tend to impact the walls of the separation zone and produce fouling. The virtual impactor device preferably also includes an acceleration zone having concave and convex sections, which reduces fouling in that area. The virtual impactor device can be combined with various downstream components such as collectors, atomizers and various analytical devices.