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    Self-assembled monolayer and method of making
    3.
    发明授权
    Self-assembled monolayer and method of making 有权
    自组装单层和制作方法

    公开(公告)号：US06733835B2

    公开(公告)日：2004-05-11

    申请号：US10347040

    申请日：2003-01-17

    申请人： Glen E. Fryxell ,  Thomas S. Zemanian ,  Jun Liu ,  Yongsoon Shin

    发明人： Glen E. Fryxell ,  Thomas S. Zemanian ,  Jun Liu ,  Yongsoon Shin

    IPC分类号： B05D300

    CPC分类号： B01J35/002 ,  B01J29/0308 ,  B01J29/06 ,  B01J29/70 ,  B01J29/7007 ,  B01J29/80 ,  B01J31/0274 ,  B01J37/00 ,  B01J2229/12 ,  B01J2229/32 ,  B82Y30/00 ,  B82Y40/00 ,  Y10T428/249955 ,  Y10T428/249956 ,  Y10T428/249969 ,  Y10T428/261 ,  Y10T428/2995 ,  Y10T428/2996 ,  Y10T428/31663

    摘要： According to the present invention, the previously known functional material having a self-assembled monolayer on a substrate has a plurality of assembly molecules each with an assembly atom with a plurality of bonding sites (four sites when silicon is the assembly molecule) wherein a bonding fraction (or fraction) of fully bonded assembly atoms (the plurality of bonding sites bonded to an oxygen atom) has a maximum when made by liquid solution deposition, for example a maximum of 40% when silicon is the assembly molecule, and maximum surface density of assembly molecules was 5 silanes per square nanometer. Note that bonding fraction and surface population are independent parameters. The method of the present invention is an improvement to the known method for making a siloxane layer on a substrate, wherein instead of a liquid phase solution chemistry, the improvement is a supercritical phase chemistry. The present invention has the advantages of greater fraction of oxygen bonds, greater surface density of assembly molecules and reduced time for reaction of about 5 minutes to about 24 hours.

    摘要翻译： 根据本发明，在衬底上具有自组装单层的先前已知的功能材料具有多个组装分子，每个组装分子具有多个结合位置的组装原子（当硅是组装分子时的四个位置），其中键合 完全结合的组装原子（多个与氧原子结合的键合位置）的分数（或分数）在通过液体溶液沉积制备时具有最大值，例如当硅是组装分子时最大为40％，最大表面密度 的组装分子是每平方毫米5硅烷。 注意，结合分数和表面总体数是独立的参数。 本发明的方法是对已知的在基材上制备硅氧烷层的方法的改进，其中代替液相溶液化学，改进是超临界相化学。 本发明具有氧键分数更高，组装分子表面密度更大，反应时间缩短约5分钟至约24小时的优点。

    Self-assembled monolayer and method of making
    10.
    发明授权
    Self-assembled monolayer and method of making 失效
    自组装单层和制作方法

    公开(公告)号：US06846554B2

    公开(公告)日：2005-01-25

    申请号：US10347042

    申请日：2003-01-17

    申请人： Glen E. Fryxell ,  Thomas S. Zemanian ,  Jun Liu ,  Yongsoon Shin

    发明人： Glen E. Fryxell ,  Thomas S. Zemanian ,  Jun Liu ,  Yongsoon Shin

    IPC分类号： B01J29/03 ,  B01J29/06 ,  B01J29/70 ,  B01J29/80 ,  B01J31/02 ,  B01J35/00 ,  B01J37/00 ,  B32B3/06

    CPC分类号： B01J35/002 ,  B01J29/0308 ,  B01J29/06 ,  B01J29/70 ,  B01J29/7007 ,  B01J29/80 ,  B01J31/0274 ,  B01J37/00 ,  B01J2229/12 ,  B01J2229/32 ,  B82Y30/00 ,  B82Y40/00 ,  Y10T428/249955 ,  Y10T428/249956 ,  Y10T428/249969 ,  Y10T428/261 ,  Y10T428/2995 ,  Y10T428/2996 ,  Y10T428/31663

    摘要： According to the present invention, the previously known functional material having a self-assembled monolayer on a substrate has a plurality of assembly molecules each with an assembly atom with a plurality of bonding sites (four sites when silicon is the assembly molecule) wherein a bonding fraction (or fraction) of fully bonded assembly atoms (the plurality of bonding sites bonded to an oxygen atom) has a maximum when made by liquid solution deposition, for example a maximum of 40% when silicon is the assembly molecule, and maximum surface density of assembly molecules was 5 silanes per square nanometer. Note that bonding fraction and surface population are independent parameters. The method of the present invention is an improvement to the known method for making a siloxane layer on a substrate, wherein instead of a liquid phase solution chemistry, the improvement is a supercritical phase chemistry. The present invention has the advantages of greater fraction of oxygen bonds, greater surface density of assembly molecules and reduced time for reaction of about 5 minutes to about 24 hours.

    摘要翻译： 根据本发明，在基板上具有自组装单层的先前已知的功能材料具有多个组装分子，每个组装分子具有多个结合位置的组装原子（当硅是组装分子时的四个位置），其中键合 完全结合的组装原子（多个与氧原子结合的键合位置）的分数（或分数）在通过液体溶液沉积制备时具有最大值，例如当硅是组装分子时最大为40％，最大表面密度 的组装分子是每平方毫米5硅烷。 注意，结合分数和表面总体数是独立的参数。 本发明的方法是对已知的在基材上制备硅氧烷层的方法的改进，其中代替液相溶液化学，改进是超临界相化学。 本发明具有氧键分数更高，组装分子表面密度更大，反应时间缩短约5分钟至约24小时的优点。