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    Process to produce biofuels from biomass
    4.
    发明授权
    Process to produce biofuels from biomass 有权
    从生物质生产生物燃料的过程

    公开(公告)号：US09394485B2

    公开(公告)日：2016-07-19

    申请号：US13332281

    申请日：2011-12-20

    申请人： Joseph Broun Powell ,  Juben Nemchand Chheda

    发明人： Joseph Broun Powell ,  Juben Nemchand Chheda

    IPC分类号： C10G3/00 ,  C10L1/00

    CPC分类号： C10G3/00 ,  C10G3/42 ,  C10G2300/1014 ,  C10G2300/202 ,  C10G2300/4081 ,  C10L1/00 ,  Y02E50/13 ,  Y02P30/20 ,  Y02T50/678

    摘要： A method to produce biofuels from biomass is provide by contacting the biomass with an aqueous media to form an extracted biomass, separating at least a portion of an aqueous liquor from the extracted biomass thereby providing the aqueous liquor stream comprising soluble carbohydrates; contacting the aqueous liquor stream with a purification substrate effective to remove sulfur compounds and nitrogen compounds thereby producing a treated carbohydrate stream having less than 35% of the sulfur content and less than 35% of the nitrogen content of the untreated aqueous liquor feed, based on the untreated aqueous liquor stream, then contacting the treated carbohydrate stream with an aqueous phase reforming catalyst to form a plurality of oxygenated intermediates; and processing at least a portion of the oxygenated intermediates to form a liquid fuel.

    摘要翻译： 通过使生物质与水性介质接触以形成提取的生物质，从提取的生物质中分离出至少一部分含水液体，从而提供包含可溶性碳水化合物的含水液体物流，从而提供从生物质生产生物燃料的方法; 使含水液体流与净化底物接触，有效地除去硫化合物和氮化合物，从而基于未处理的含水液体进料的少于35％的硫含量和少于35％的氮含量的处理的碳水化合物流，基于 未处理的含水液体物流，然后使经处理的碳水化合物流与水相重整催化剂接触以形成多个含氧中间体; 以及处理所述氧化中间体的至少一部分以形成液体燃料。

    Process to produce biofuels from biomass
    6.
    发明授权
    Process to produce biofuels from biomass 有权
    从生物质生产生物燃料的过程

    公开(公告)号：US09102879B2

    公开(公告)日：2015-08-11

    申请号：US13331065

    申请日：2011-12-20

    申请人： Joseph Broun Powell ,  Juben Nemchand Chheda

    发明人： Joseph Broun Powell ,  Juben Nemchand Chheda

    IPC分类号： C07C1/00 ,  C10G3/00 ,  C10L1/04

    CPC分类号： C10G3/00 ,  C10G3/42 ,  C10G2300/1014 ,  C10G2300/202 ,  C10G2300/4081 ,  C10G2300/44 ,  C10L1/04 ,  Y02P30/20

    摘要： Biomass is contacted with an aqueous media to form an extracted biomass. An aqueous liquor separated from the extracted biomass is treated with a purification substrate to form a treated carbohydrate stream having less than 35% of the sulfur content and less than 35% of the nitrogen content, based on the untreated aqueous liquor stream, prior to contact with an aqueous phase reforming catalyst to form oxygenated intermediates that can be further processed to form a liquid fuel. An extracted biomass solids stream is also separated from the extracted biomass which is contacted with a first digestive solvent and then a second digestive solvent to form a solubilized pulp. This solublilized pulp may be combined with the aqueous liquor stream or combined to an aqueous reforming reaction system or recycled to the aqueous media to be processed further for an effective process to produce the liquid fuel.

    摘要翻译： 生物质与水性介质接触以形成提取的生物质。 用提取的生物质分离的含水液体用净化底物处理，以在接触之前基于未处理的含水液体流形成具有少于35％的硫含量和小于氮含量的35％的经处理的碳水化合物流 与水相重整催化剂形成氧化中间体，其可进一步加工以形成液体燃料。 提取的生物质固体物流也与提取的生物质分离，其与第一消化溶剂接触，然后与第二消化溶剂接触以形成溶解的纸浆。 这种溶解的纸浆可以与含水液体流合并或与水性重整反应体系结合或再循环到水性介质中以进一步进行处理以产生液体燃料。

    Biomass conversion systems having a fluid circulation loop containing backflushable filters for control of cellulosic fines and methods for use thereof
    7.
    发明授权
    Biomass conversion systems having a fluid circulation loop containing backflushable filters for control of cellulosic fines and methods for use thereof 有权
    具有流体循环回路的生物质转化系统，其包含用于控制纤维素细粉的可反吹过滤器及其使用方法

    公开(公告)号：US08846993B2

    公开(公告)日：2014-09-30

    申请号：US13332309

    申请日：2011-12-20

    申请人： Joseph Broun Powell

    发明人： Joseph Broun Powell

    IPC分类号： C07C1/00

    CPC分类号： C10G1/06 ,  B01D29/56 ,  B01J8/00 ,  C10G1/002 ,  C10G1/065 ,  C10G3/00 ,  C10G3/42 ,  C10G2300/1014 ,  C10L1/02 ,  Y02P30/20

    摘要： Digestion of cellulosic biomass to produce a hydrolysate may be accompanied by the formation of cellulosic fines which may be damaging to system components. Biomass conversion systems that may address the issue of cellulosic fines may comprise a fluid circulation loop comprising: a hydrothermal digestion unit; a solids separation unit that is in fluid communication with an outlet of the hydrothermal digestion unit; where the solids separation unit comprises a plurality of filters and the filters are in fluid communication with the fluid circulation loop in both a forward and a reverse flow direction; and a catalytic reduction reactor unit that is in fluid communication with an outlet of the solids separation unit and an inlet of the hydrothermal digestion unit; where at least one of the plurality of filters is in fluid communication with an inlet of the catalytic reduction reactor unit.

    摘要翻译： 消化纤维素生物质以产生水解产物可伴随着可能损害系统组分的纤维素细粉的形成。 可能解决纤维素细粒问题的生物质转化系统可以包括流体循环回路，包括：水热消解单元; 固体分离单元，其与所述水热消解单元的出口流体连通; 其中固体分离单元包括多个过滤器，并且过滤器在正向和反向流动方向上与流体循环回路流体连通; 以及催化还原反应器单元，其与所述固体分离单元的出口和所述水热消解单元的入口流体连通; 其中所述多个过滤器中的至少一个与所述催化还原反应器单元的入口流体连通。

    Reduction of the viscosity of reactive heavy byproducts during the production of 1,3-propanediol
    10.
    发明授权
    Reduction of the viscosity of reactive heavy byproducts during the production of 1,3-propanediol 失效
    在1,3-丙二醇生产过程中降低反应性重副产物的粘度

    公开(公告)号：US07276634B2

    公开(公告)日：2007-10-02

    申请号：US10676682

    申请日：2003-10-01

    申请人： John Frederick Knifton ,  Talmadge Gail James ,  Paul Richard Weider ,  Joseph Broun Powell ,  Edward Lewis Nielsen ,  Glenn Charles Komplin

    发明人： John Frederick Knifton ,  Talmadge Gail James ,  Paul Richard Weider ,  Joseph Broun Powell ,  Edward Lewis Nielsen ,  Glenn Charles Komplin

    IPC分类号： C07C27/10

    CPC分类号： C07C45/58 ,  C07C29/141 ,  C07C31/205

    摘要： The present invention is an improvement upon the process for the production of 1,3-propanediol wherein an aqueous solution of 3-hydroxy propanal is formed, catalyst, if any, used in said formation is removed from the solution, sodium hydroxide is added to the solution to neutralize any acid therein such that the pH is at least about 5, the neutralized aqueous solution is subjected to hydrogenation to produce a crude 1,3-propanediol mixture which is distilled to produce 1,3-propanediol, water, and reactive heavy components. The improvement on this process comprises replacing the sodium hydroxide with a hydroxide selected from the group consisting of ammonium hydroxide, alkali metal hydroxides other than sodium hydroxide, and alkaline earth metal hydroxides to reduce the viscosity of the reactive heavy components.

    摘要翻译： 本发明是对生产1,3-丙二醇的方法的改进，其中形成3-羟基丙醛的水溶液，从该溶液中除去所述地层中使用的催化剂（如果有的话），将氢氧化钠加入 中和其中的任何酸使其pH至少约为5的溶液，中和的水溶液进行氢化以产生粗制的1,3-丙二醇混合物，其被蒸馏以产生1,3-丙二醇，水和反应性 重组件。 该方法的改进包括用选自氢氧化铵，氢氧化钠以外的碱金属氢氧化物和碱土金属氢氧化物的氢氧化物代替氢氧化钠，以降低反应性重组分的粘度。