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    Attrition resistant molecular sieve catalyst
    7.
    发明申请
    Attrition resistant molecular sieve catalyst 有权
    耐磨分子筛催化剂

    公开(公告)号：US20070100187A1

    公开(公告)日：2007-05-03

    申请号：US11588552

    申请日：2006-10-27

    申请人： Yun-feng Chang

    发明人： Yun-feng Chang

    IPC分类号： B01J29/06 ,  B01J27/00 ,  B01J27/182 ,  C07C1/00

    CPC分类号： B01J29/06 ,  B01J29/83 ,  B01J29/85 ,  B01J35/002 ,  B01J37/0045 ,  B01J37/04 ,  B01J2229/42 ,  C07C1/20 ,  C07C2529/83 ,  C07C2529/84 ,  C07C2529/85 ,  C07C11/02

    摘要： This invention provides a process for making an attrition resistant molecular sieve catalyst composition. The formation of highly attrition resistant catalyst particles is accomplished by initially mixing together catalyst components to form a slurry at a relatively low viscosity and high solids content. Preferably, a slurry having characteristics of high solids content and low viscosity is achieved using a rotor-stator mixer. Once the desired slurry characteristics are obtained, the slurry is dried, preferably by spray drying and calcining, to form a highly attrition resistant catalyst.

    摘要翻译： 本发明提供了制造耐磨分子筛催化剂组合物的方法。 通过最初将催化剂组分混合在一起，以相对较低的粘度和高的固体含量形成浆料来实现高耐磨性催化剂颗粒的形成。 优选地，使用转子 - 定子混合器实现具有高固体含量和低粘度特性的浆料。 一旦获得所需的浆料特性，将浆料干燥，优选通过喷雾干燥和煅烧来形成高耐磨性的催化剂。

    Method of formulating a molecular sieve catalyst composition by controlling component addition
    9.
    发明授权
    Method of formulating a molecular sieve catalyst composition by controlling component addition 有权
    通过控制组分添加剂配制分子筛催化剂组合物的方法

    公开(公告)号：US07772337B2

    公开(公告)日：2010-08-10

    申请号：US11859227

    申请日：2007-09-21

    申请人： Yun-feng Chang ,  Stephen N. Vaughn

    发明人： Yun-feng Chang ,  Stephen N. Vaughn

    IPC分类号： C08F4/00

    CPC分类号： C08F10/00 ,  B01J29/84 ,  B01J29/85 ,  B01J35/002 ,  B01J37/0036 ,  B01J37/0045 ,  B01J2229/42 ,  C07C1/20 ,  C07C2521/04 ,  C07C2521/16 ,  C07C2529/83 ,  C07C2529/85 ,  C08F210/16 ,  Y02P20/52 ,  Y02P30/42 ,  C07C11/02 ,  C07C11/06 ,  C07C11/04 ,  C08F210/06 ,  C08F2/00

    摘要： This invention provides a method of making a molecular sieve catalyst composition comprising the steps of: a) combining molecular sieve crystals with binder and liquid to form a binder-sieve mixture; b) combining the binder-sieve mixture with matrix material to form a binder-sieve-matrix mixture; c) mixing the binder-sieve-matrix mixture under conditions sufficient to form a slurry having a solids content of at least 40 wt %, based on total weight of the slurry; d) progressing the mixing until slurry viscosity decreases without significant additional dilution of the slurry, so that the slurry solids content does not significantly decrease; and e) drying the decreased viscosity slurry to produce a dried molecular sieve catalyst composition having an attrition rate index of not greater than 1 wt %/hr. The aforementioned catalyst compositions can be used in processes for making olefin product from oxygenate feedstock, which olefin products can be further used for making (co)polymer products.

    摘要翻译： 本发明提供一种制备分子筛催化剂组合物的方法，其包括以下步骤：a）将分子筛结晶与粘合剂和液体结合以形成粘合剂 - 筛混合物; b）将粘合剂 - 筛混合物与基质材料组合以形成粘合剂 - 筛 - 基质混合物; c）在足以形成基于浆料总重量的至少40重量％的固体含量的浆料的条件下混合粘合剂 - 筛子 - 基质混合物; d）进行混合直到浆液粘度降低而不显着额外稀释浆料，使得浆料固体含量不显着降低; 和e）干燥粘度降低的浆料以产生具有不大于1重量％/小时的磨耗率指数的干燥分子筛催化剂组合物。 上述催化剂组合物可用于从含氧化合物原料制备烯烃产物的方法中，该烯烃产物可以进一步用于制备（共）聚合物产物。

    Methods addressing aging in flocculated molecular sieve catalysts for hydrocarbon conversion processes
    10.
    发明授权
    Methods addressing aging in flocculated molecular sieve catalysts for hydrocarbon conversion processes 有权
    解决用于烃转化过程的絮凝分子筛催化剂中的老化的方法

    公开(公告)号：US07732537B2

    公开(公告)日：2010-06-08

    申请号：US12021918

    申请日：2008-01-29

    申请人： Yun-feng Chang ,  Luc R. M. Martens ,  Machteld Maria Mertens ,  Stephen N. Vaughn

    发明人： Yun-feng Chang ,  Luc R. M. Martens ,  Machteld Maria Mertens ,  Stephen N. Vaughn

    IPC分类号： C08F2/00 ,  B01J29/06 ,  C08F10/00

    CPC分类号： C08F10/00 ,  B01J29/06 ,  B01J29/7015 ,  B01J29/84 ,  B01J29/85 ,  B01J37/0045 ,  B01J2229/40 ,  B01J2229/42 ,  C07C1/20 ,  C07C2529/85 ,  Y02P20/52 ,  Y02P30/42 ,  C07C11/06 ,  C07C11/04 ,  C08F4/16 ,  C08F4/12

    摘要： One aspect of the invention relates to a method for formulating a molecular sieve catalyst composition, the method comprising the steps of: (a) providing a synthesized molecular sieve having been recovered in the presence of a flocculant; (b) thermally treating the synthesized molecular sieve at a temperature from about 50° C. to about 250° C. and under other conditions sufficient to form a thermally treated synthesized molecular sieve having a first LOI less than 26% and a first micropore surface area; (c) aging the thermally treated synthesized molecular sieve for at least one year; (d) analyzing the aged, thermally treated molecular sieve to determine a second micropore surface area, wherein the second micropore surface area is 3% or less lower than the first micropore surface area; and (e) combining the aged, thermally treated synthesized molecular sieve, a binder, and optionally a matrix material to produce an aged, formulated molecular sieve catalyst composition.

    摘要翻译： 本发明的一个方面涉及一种配制分子筛催化剂组合物的方法，该方法包括以下步骤：（a）提供在絮凝剂存在下回收的合成分子筛; （b）在约50℃至约250℃的温度和在足以形成具有第一LOI小于26％的热处理合成分子筛的其它条件下热处理合成的分子筛和第一微孔表面 区; （c）将经热处理的合成分子筛老化至少一年; （d）分析老化的热处理分子筛以确定第二微孔表面积，其中第二微孔表面积比第一微孔表面积低3％或更低; 和（e）将老化的热处理合成分子筛，粘合剂和任选的基质材料组合以制备老化的配制分子筛催化剂组合物。