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    Process for producing alkali pulp
    1.
    发明授权
    Process for producing alkali pulp 失效
    碱浆生产工艺

    公开(公告)号：US4274913A

    公开(公告)日：1981-06-23

    申请号：US41505

    申请日：1979-05-22

    申请人： Makoto Kikuiri ,  Yoshimi Nakashio ,  Yasue Arai ,  Toshio Hidaka

    发明人： Makoto Kikuiri ,  Yoshimi Nakashio ,  Yasue Arai ,  Toshio Hidaka

    IPC分类号： D21C3/02 ,  D21C3/24 ,  D21C3/26 ,  D21C7/08

    CPC分类号： D21C7/08 ,  D21C3/263

    摘要： A process for producing alkali pulp by using a single, cylindrical pressurized reaction vessel having therein a liquor-inpregnating zone, a cooking zone, a washing zone, and a diluting zone in that order, and having a motor-driven scraping or agitating device and a pulp discharging outlet in the end portion of the diluting zone. Alkaline aqueous medium containing dissolved oxygen therein is introduced into the diluting zone. A part of the introduced alkaline aqueous medium countercurrently contacts cooked cellulosic materials transferred from the washing zone to the diluting zone to proceed with oxygen-alkali delignification, and is finally discharged out of the vessel from the end portion of the cooking zone. The remainder of the introduced alkaline aqueous medium contacts the cooked cellulosic materials in the diluting zone in a scraping or agitating manner by means of the motor-driven scraping or agitating device to proceed with oxygen-alkali delignification, and finally serves as diluting liquor to be discharged out of the vessel accompanying the resulting pulp.

    摘要翻译： 一种通过使用其中具有浸渍浸渍区，蒸煮区，洗涤区和稀释区的单个圆柱形加压反应容器来生产碱浆的方法，并且具有马达驱动的刮擦或搅拌装置和 在稀释区的端部的纸浆排出口。 将含有溶解氧的碱性水性介质引入稀释区。 引入的碱性水性介质的一部分与从洗涤区转移到稀释区的煮熟的纤维素材料逆流接触，进行氧碱脱木质素，最后从烹调区的端部排出容器。 引入的碱性水性介质的其余部分通过马达驱动的刮擦或搅拌装置以刮擦或搅拌方式与稀释区中的熟化纤维素材料接触，进行氧碱脱木质素，最后作为稀释液体 从伴随所产生的纸浆的容器中排出。

    Process for producing chroman compound
    2.
    发明授权
    Process for producing chroman compound 失效
    苯并二氢吡喃化合物的制备方法

    公开(公告)号：US07615650B2

    公开(公告)日：2009-11-10

    申请号：US10587545

    申请日：2005-01-28

    申请人： Kazuo Tanaka ,  Youichi Kyuuko ,  Toshio Hidaka

    发明人： Kazuo Tanaka ,  Youichi Kyuuko ,  Toshio Hidaka

    IPC分类号： C07D311/66

    CPC分类号： C07D311/66 ,  C07D311/62

    摘要： The invention provides a process for producing a chroman compound represented by formula (1), characterized in that the process includes allowing a phenol, an unsaturated compound, and a formaldehyde to react in the absence of catalyst and in the presence of water in an amount by mole 1 to 10 times that of the phenol.According to the present invention, a high-purity chroman compound can be produced in the absence of catalyst and under mild conditions. In addition, the invention provides an industrial means for producing the compound, without using a large amount of an acid or a base serving as a reaction promoter or a catalyst, which would otherwise cause side reactions, apparatus corrosion, etc.

    摘要翻译： 本发明提供一种制备由式（1）表示的苯并二氢吡喃化合物的方法，其特征在于该方法包括使苯酚，不饱和化合物和甲醛在不存在催化剂的情况下和在水存在下反应， 为摩尔比的1〜10倍。 根据本发明，可以在不存在催化剂的条件下，在温和的条件下生产高纯度色满化合物。 此外，本发明提供了一种用于生产化合物的工业方法，而不使用大量的酸或作为反应促进剂或催化剂的碱，否则会引起副反应，装置腐蚀等。

    METHOD OF PRODUCING S-(-)-6-HYDROXY-2,5,7,8-TETRAMETHYLCHROMANE-2-CARBOXYLIC ACID AND PRODUCT OBTAINED BY THE METHOD
    5.
    发明申请
    METHOD OF PRODUCING S-(-)-6-HYDROXY-2,5,7,8-TETRAMETHYLCHROMANE-2-CARBOXYLIC ACID AND PRODUCT OBTAINED BY THE METHOD 失效
    生产S - （ - ） - 6-羟基-2,5,7,8-四甲基-2-羟基-2-羧酸的方法及其方法

    公开(公告)号：US20100063305A1

    公开(公告)日：2010-03-11

    申请号：US12312125

    申请日：2007-10-25

    申请人： Akifumi Iida ,  Youichi Kyuuko ,  Toshio Hidaka

    发明人： Akifumi Iida ,  Youichi Kyuuko ,  Toshio Hidaka

    IPC分类号： C07D311/04

    CPC分类号： C07D311/66 ,  C07B53/00

    摘要： The present invention provides an industrially available method for efficiently producing high-purity S-(−)-6-hydroxy-2,5,7,8-tetramethylchromane-2-carboxylic acid excellent in solid-liquid separability from an S-(−)-6-hydroxy-2,5,7,8-tetramethylchromane-2-carboxylic acid ester, and also provides products obtained by the method.Under a temperature condition of 50-80° C. in an aqueous solvent, (A) an S-(−)-6-hydroxy-2,5,7,8-tetramethylchromane-2-carboxylic acid ester represented by the general formula (1) is hydrolyzed under a basic condition for 1-3 hours; then (B) the insoluble matters contained in the reaction solution resulting from the hydrolysis are removed; and (C) an acid is added to the resulting solution to effect crystallization; provided that R in the general formula (1) represents an alkyl or aryl group.

    摘要翻译： 本发明提供了一种工业上可行的方法，用于有效地生产出具有优异的S - （ - ） - （ - ） - 羟基-2,4,5,6,7,8-四甲基苯并二氢吡喃-2-羧酸的高纯度S - （ - ） - ）-6-羟基-2,5,7,8-四氢苯并二氢吡喃-2-羧酸酯，并且还提供通过该方法获得的产物。 在水性溶剂中在50-80℃的温度条件下，（A）由通式（A）表示的S - （ - ） - 6-羟基-2,5,7,8-四氢苯并二氢吡喃-2-羧酸酯 （1）在碱性条件下水解1-3小时; 然后（B）去除由水解产生的反应溶液中所含的不溶物; 和（C）向所得溶液中加入酸以进行结晶; 条件是通式（1）中的R表示烷基或芳基。

    Fluorine compound and fluorinating agent comprising the compound
    6.
    发明申请
    Fluorine compound and fluorinating agent comprising the compound 失效
    氟化合物和包含该化合物的氟化剂

    公开(公告)号：US20060089513A1

    公开(公告)日：2006-04-27

    申请号：US11297408

    申请日：2005-12-09

    申请人： Toshio Hidaka ,  Norio Fushimi ,  Takafumi Yoshimura ,  Takeshi Kawai

    发明人： Toshio Hidaka ,  Norio Fushimi ,  Takafumi Yoshimura ,  Takeshi Kawai

    IPC分类号： C07C211/27

    CPC分类号： C07F9/54 ,  C07B39/00 ,  C07C17/16 ,  C07C17/18 ,  C07C211/29 ,  C07C251/30 ,  C07C271/20 ,  C07F9/5004 ,  Y02P20/582

    摘要： A fluorine compound represented by Formula (1) is provided. The above fluorine compound is effective for introducing a fluorine atom into a compound having an active group such as an oxygen-containing functional group, and it can be used for uses of surface treatment, cleaning and coating. Further, after the fluorination reaction, the above compound is recovered and can be reused as a starting material for producing the above fluorine compound, and it is useful for various fluorination processes. (wherein X represents a nitrogen or phosphorus atom; R0, R1, and R2 represent hydrogen, an alkyl group or aryl group which may have a substituent, and they each may be the same or different; and R0, R1, and R2 may be combined with each other to form a ring).

    摘要翻译： 提供由式（1）表示的氟化合物。 上述氟化合物有效地将氟原子引入具有活性基团的化合物如含氧官能团，并且其可用于表面处理，清洁和涂覆的用途。 此外，在氟化反应之后，回收上述化合物，可以重复使用作为制备上述氟化合物的原料，可用于各种氟化处理。 （其中X表示氮或磷原子; R 0，R 1，R 2和R 2表示氢，烷基或芳基， 可以具有取代基，并且它们各自可以相同或不同;并且R 0，R 1和R 2可以与 彼此形成一个戒指）。

    Catalysts for producing methylamines
    7.
    发明授权
    Catalysts for producing methylamines 有权
    用于生产甲胺的催化剂

    公开(公告)号：US06294633B1

    公开(公告)日：2001-09-25

    申请号：US09630559

    申请日：2000-08-02

    申请人： Toshio Hidaka ,  Katsumi Higuchi

    发明人： Toshio Hidaka ,  Katsumi Higuchi

    IPC分类号： C07C20916

    CPC分类号： C07C209/16 ,  B01J29/18 ,  B01J35/023 ,  C07C211/04

    摘要： Catalysts for producing methylamines are provided, which comprise mordenite, as the essential component, of spherical fine particles having a crystal diameter of not more than 0.5 &mgr;m. When the catalysts are used for the production of dimethylamine from methanol and ammonia or through a disproportionation of methylamines, they exhibit a high dimethylamine productivity with the formation of few amount of trimethylamine whose demand is very small. The process can be operated for a long period of time without decrease in the catalyst activity.

    摘要翻译： 提供了用于生产甲胺的催化剂，其包含丝光沸石作为必需组分的具有不超过0.5μm的晶体直径的球形细颗粒。 当催化剂用于从甲醇和氨生产二甲胺或通过甲胺歧化生成二甲胺时，它们表现出高的二甲胺生产率，形成的需求量很少的三甲胺数量很少。 该方法可以长时间运行而催化剂活性不降低。

    Method for producing 2-oxazoline analogue or 1,3-oxazine analogue
    10.
    发明授权
    Method for producing 2-oxazoline analogue or 1,3-oxazine analogue 失效
    2-恶唑啉类似物或1,3-恶嗪类似物的制备方法

    公开(公告)号：US08063205B2

    公开(公告)日：2011-11-22

    申请号：US12065347

    申请日：2006-08-30

    申请人： Shoji Hara ,  Tsuyoshi Fukuhara ,  Toshio Hidaka

    发明人： Shoji Hara ,  Tsuyoshi Fukuhara ,  Toshio Hidaka

    IPC分类号： C07D263/12 ,  C07D263/16 ,  C07D263/56 ,  C07D265/08 ,  C07D277/10 ,  C07D279/06

    CPC分类号： C07D263/12 ,  C07D263/16 ,  C07D263/56 ,  C07D265/08 ,  C07D277/10

    摘要： The present invention is a method for producing a 2-oxazoline analogue or a 1,3-oxazine analogue represented by the following general formula (3) by reacting a 1,2-aminoalcohol compound or a 1,2-aminothiol compound with an α,α-dihaloamine compound.(In the formula, n represents 0 or 1, and R represents an oxygen atom or a sulfur atom. R1, R2 and R3 each represents an atom or a group shown in Group 1 to Group 3, and R0 represents an atom or a group shown in Group 2 or Group 3. Two or more of R1, R2 and R3 may be bonded to each other to form a ring.Group 1: a hydrogen atom, a halogen atom, a nitro group, a cyano group, a formyl group, a carboxyl group, a sulfonyl group, a sulfinoyl group or a sulfenyl group;Group 2: an alkyl group, which may have an arbitrary substituent, an aryl group or an aralkyl group; andGroup 3: an alkyl-substituted, aryl-substituted or aralkyl-substituted oxy group, a carbonyl group, an oxycarbonyl group, a carbonyloxy group, a thio group, a sulfonyl group, a sulfinoyl group or a sulfenyl group)

    摘要翻译： 本发明是通过使1,2-氨基醇化合物或1,2-氨基硫醇化合物与α反应生成2-恶唑啉类似物或由以下通式（3）表示的1,3-恶嗪类似物的方法， ，α-二卤代胺化合物。 （式中，n表示0或1，R表示氧原子或硫原子，R1，R2和R3各自表示1〜3族所示的原子或基团，R0表示原子或基团） 第1组：氢原子，卤素原子，硝基，氰基，甲酰基等。另外，R 1，R 2，R 3可以相互结合形成环。 ，羧基，磺酰基，亚磺酰基或亚磺酰基;第2族：可以具有任意取代基的烷基，芳基或芳烷基;第3族：烷基取代的芳基 - 取代或芳烷基取代的氧基，羰基，氧羰基，羰氧基，硫基，磺酰基，亚磺酰基或亚磺酰基）