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公开(公告)号：US07638581B2
公开(公告)日：2009-12-29
申请号：US11305978
申请日：2005-12-19
申请人： Naiyong Jing , Tatsuo Fukushi , Chuntao Cao , Lan H. Liu , Thomas P. Klun , William D. Coggio , Vivian W. Jones
发明人： Naiyong Jing , Tatsuo Fukushi , Chuntao Cao , Lan H. Liu , Thomas P. Klun , William D. Coggio , Vivian W. Jones
IPC分类号： C08L27/12
CPC分类号： C08J3/005 , C08J7/047 , C08J2327/12 , C08J2427/00 , C08L27/12 , C08L27/16 , C08L27/18 , C08L2205/02 , C09D127/12 , C09D127/16 , C09D127/18 , C08L2666/04
摘要： A fluoropolymer coating composition contains a homogeneous mixture of crystalline submicron fluoropolymer particles dispersed in a solvent-borne solution of less crystalline or amorphous fluororesin. The composition may be prepared by blending a latex containing crystalline submicron fluoropolymer particles with a latex containing less crystalline or amorphous fluororesin particles, coagulating and drying the blended latices, and dissolving the dried blend in a solvent for the fluororesin particles. Quasi-homogenous compositions may be prepared by blending dry crystalline submicron fluoropolymer particles with a) dry less crystalline or amorphous fluororesin particles and a solvent for the fluororesin particles, or b) a solvent-borne solution of less crystalline or amorphous fluororesin. Rubbing the disclosed coatings can provide a thin, continuous or nearly continuous fluoropolymer surface layer atop a less crystalline or amorphous fluororesin binder containing crystalline submicron fluoropolymer particles.
摘要翻译： 氟聚合物涂料组合物含有分散在不太结晶或无定形氟树脂的溶剂型溶液中的结晶亚微米含氟聚合物颗粒的均匀混合物。 该组合物可以通过将含有结晶亚微米含氟聚合物颗粒的胶乳与含有较少结晶或无定形氟树脂颗粒的胶乳混合来制备，将混合的胶乳凝结并干燥，并将干燥的共混物溶解在氟树脂颗粒的溶剂中。 准均匀组合物可以通过将干结晶亚微米含氟聚合物颗粒与a）干结晶或无定形氟树脂颗粒和用于氟树脂颗粒的溶剂混合来制备，或b）不太结晶或无定形氟树脂的溶剂型溶液。 摩擦所公开的涂层可以在含有结晶亚微米含氟聚合物颗粒的较少结晶或无定形氟树脂粘合剂的顶部提供薄的，连续的或几乎连续的含氟聚合物表面层。
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2.发明授权Low refractive index fluoropolymer coating compositions for use in antireflective polymer films 有权用于抗反射聚合物膜的低折射率含氟聚合物涂料组合物公开(公告)号：US07323514B2
公开(公告)日：2008-01-29
申请号：US11026640
申请日：2004-12-30
申请人： Naiyong Jing , Chuntao Cao , Tatsuo Fukushi , Timothy J. Tatge , William D. Coggio , Christopher B. Walker, Jr. , Thomas P. Klun , William J. Schultz , Zai-Ming Qiu
发明人： Naiyong Jing , Chuntao Cao , Tatsuo Fukushi , Timothy J. Tatge , William D. Coggio , Christopher B. Walker, Jr. , Thomas P. Klun , William J. Schultz , Zai-Ming Qiu
IPC分类号： C08F259/00
CPC分类号： G02B1/111 , Y10T428/24942 , Y10T428/3154 , Y10T428/31663
摘要： An economic, optically transmissive, stain and ink repellent, durable low refractive index fluoropolymer composition for use in an antireflection film or coupled to an optical display. In one aspect of the invention, the composition is formed from the reaction product of a fluoropolymer or reactive fluoropolymer, an amino silane ester coupling agent or ester equivalent, a multi-olefinic crosslinker, and optional surface modified inorganic particles or sol gel precursors.
摘要翻译： 用于抗反射膜或耦合到光学显示器的经济，光学透射，防污和防油墨，耐用的低折射率含氟聚合物组合物。 在本发明的一个方面，组合物由含氟聚合物或反应性含氟聚合物，氨基硅烷酯偶联剂或酯当量的反应产物，多烯属交联剂和任选的表面改性的无机颗粒或溶胶凝胶前体形成。
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3.发明授权Low refractive index fluoropolymer compositions having improved coating and durability properties 有权具有改进的涂层和耐久性的低折射率含氟聚合物组合物公开(公告)号：US07473462B2
公开(公告)日：2009-01-06
申请号：US11972034
申请日：2008-01-10
申请人： William D. Coggio , Thomas P. Klun , George G. I. Moore , Naiyong Jing , Chuntao Cao , Sharon Wang , Patricia M. Savu , Lan H. Liu , Joan M. Noyola
发明人： William D. Coggio , Thomas P. Klun , George G. I. Moore , Naiyong Jing , Chuntao Cao , Sharon Wang , Patricia M. Savu , Lan H. Liu , Joan M. Noyola
CPC分类号： C08F14/18 , C08F259/08 , C08F283/00 , C08L51/003 , C09D151/003 , G02B1/111 , Y10T428/24942 , Y10T428/259 , Y10T428/3154 , Y10T428/31544 , Y10T428/31935 , C08F2/00 , C08L2666/02
摘要： A low refractive index composition that forms a low refractive index layer on an optical display is formed having a co-crosslinked interpenetrating polymer network of a fluoropolymer phase and an acrylate phase. The fluoropolymer phase is preferably formed from fluoropolymers based on THV or FKM and having either a degree of unsaturation and/or containing a reactive cure site monomer in its polymer backbone. The acrylate phase includes a multifunctional acrylate crosslinker, and more preferably includes a perfluoropolyether acrylate crosslinker. The formed low refractive index layer has improved interfacial adhesion to other layers or substrates contained in the optical display. Further, the mechanical strength and scratch resistance of the either of above low refractive index compositions can be further enhanced through the incorporation of surface functionalized inorganic particle into the formed layer.
摘要翻译： 形成在光学显示器上形成低折射率层的低折射率组合物，其具有含氟聚合物相和丙烯酸酯相的共交联互穿聚合物网络。 含氟聚合物相优选由基于THV或FKM的含氟聚合物形成，并且在其聚合物主链中具有不饱和度和/或含有反应性固化位点单体。 丙烯酸酯相包括多官能丙烯酸酯交联剂，更优选包括全氟聚醚丙烯酸酯交联剂。 所形成的低折射率层具有改善的与光学显示器中包含的其它层或基底的界面粘合性。 此外，通过将表面官能化的无机颗粒并入成形层，可以进一步提高上述低折射率组合物中的任一种的机械强度和耐划伤性。
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4.发明申请LOW REFRACTIVE INDEX COMPOSITION COMPRISING FLUOROPOLYETHER URETHANE COMPOUND 有权包含氟聚乙二醇脲化合物的低折射率指数组合物公开(公告)号：US20070287093A1
公开(公告)日：2007-12-13
申请号：US11427665
申请日：2006-06-29
申请人： Naiyong Jing , Thomas P. Klun , Chuntao Cao , William D. Coggio , Zai-Ming Qiu
发明人： Naiyong Jing , Thomas P. Klun , Chuntao Cao , William D. Coggio , Zai-Ming Qiu
IPC分类号： G03C1/00
CPC分类号： G03F7/091 , G03F7/0046 , G03F7/027 , G03F7/038 , G03F7/0388 , Y10T428/24942 , Y10T428/3154 , Y10T428/31971
摘要： Antireflective films and low refractive index compositions are described. The low refractive index layer comprises the reaction product of a composition comprising at least one free-radically polymerizable material having a high fluorine content, and at least one free-radically polymerizable fluoropolyether urethane material.
摘要翻译： 描述了抗反射膜和低折射率组合物。 低折射率层包括含有至少一种具有高氟含量的至少一种可自由基聚合的材料和至少一种可自由基聚合的氟聚醚聚氨酯材料的组合物的反应产物。
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5.发明授权Low refractive index composition comprising fluoropolyether urethane compound 有权包含含氟聚醚氨基甲酸酯化合物的低折射率组合物公开(公告)号：US07575847B2
公开(公告)日：2009-08-18
申请号：US11427665
申请日：2006-06-29
申请人： Naiyong Jing , Thomas P. Klun , Chuntao Cao , William D. Coggio , Zai-Ming Qiu
发明人： Naiyong Jing , Thomas P. Klun , Chuntao Cao , William D. Coggio , Zai-Ming Qiu
CPC分类号： G03F7/091 , G03F7/0046 , G03F7/027 , G03F7/038 , G03F7/0388 , Y10T428/24942 , Y10T428/3154 , Y10T428/31971
摘要： Antireflective films and low refractive index compositions are described. The low refractive index layer comprises the reaction product of a composition comprising at least one free-radically polymerizable material having a high fluorine content, and at least one free-radically polymerizable fluoropolyether urethane material.
摘要翻译： 描述了抗反射膜和低折射率组合物。 低折射率层包括含有至少一种具有高氟含量的至少一种可自由基聚合的材料和至少一种可自由基聚合的氟聚醚聚氨酯材料的组合物的反应产物。
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6.发明授权Fluoropolymer coating compositions with multifunctional fluoroalkyl crosslinkers for anti-reflective polymer films 失效具有用于抗反射聚合物膜的多功能氟代烷基交联剂的含氟聚合物涂料组合物公开(公告)号：US07351471B2
公开(公告)日：2008-04-01
申请号：US11026754
申请日：2004-12-30
申请人： Naiyong Jing , Chuntao Cao , Tatsuo Fukushi , Timothy J. Tatge , Christopher B. Walker, Jr. , Thomas P. Klun , William J. Schultz , Zai-Ming Qiu
发明人： Naiyong Jing , Chuntao Cao , Tatsuo Fukushi , Timothy J. Tatge , Christopher B. Walker, Jr. , Thomas P. Klun , William J. Schultz , Zai-Ming Qiu
CPC分类号： G02B1/111 , A63B37/0004 , Y10T428/269
摘要： An economic, optically transmissive, stain and ink repellent, durable low refractive index fluoropolymer composition for use in an antireflection film or coupled to an optical display. In one aspect of the invention, the composition is formed from the reaction product of a fluoropolymer and a fluoroalkyl containing multi-olefinic crosslinker. In another aspect of the invention, the composition further includes surface modified inorganic nanoparticles.
摘要翻译： 用于抗反射膜或耦合到光学显示器的经济，光学透射，防污和防油墨，耐用的低折射率含氟聚合物组合物。 在本发明的一个方面，组合物是由含氟聚合物和含氟烷基的多烯烃交联剂的反应产物形成的。 在本发明的另一方面，组合物还包括表面改性的无机纳米颗粒。
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7.发明授权Perfluoropolyether urethane additives having (meth)acryl groups and hard coats 有权具有（甲基）丙烯酸基团和硬涂层的全氟聚醚氨基甲酸酯添加剂公开(公告)号：US08147966B2
公开(公告)日：2012-04-03
申请号：US12718481
申请日：2010-03-05
申请人： Thomas P. Klun , Naiyong Jing , Richard J. Pokorny , Zai-Ming Qiu , Mark J. Pellerite , William D. Coggio , Christopher B. Walker, Jr.
发明人： Thomas P. Klun , Naiyong Jing , Richard J. Pokorny , Zai-Ming Qiu , Mark J. Pellerite , William D. Coggio , Christopher B. Walker, Jr.
IPC分类号： B32B27/40
CPC分类号： C07C235/08 , C08G18/3802 , C08G18/3825 , C08G18/672 , C08G18/673 , C08G18/792 , C08G18/8175 , C09D175/16 , G02B1/105 , G02B1/14 , Y10T428/265 , Y10T428/3154 , Y10T428/31551 , C08G18/50
摘要： Fluorocarbon- and urethane-(meth)acryl-containing additives and hardcoats. The hardcoats are particularly useful as a surface layer on an optical device.
摘要翻译： 含氟碳酸酯和氨基甲酸酯（甲基）丙烯酸的添加剂和硬涂层。 硬涂层作为光学装置上的表面层是特别有用的。
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8.发明申请PERFLUOROPOLYETHER URETHANE ADDITIVES HAVING (METH)ACRYL GROUPS AND HARD COATS 有权具有（甲基）丙烯酸树脂组合物和硬质涂料的全氟聚醚添加剂公开(公告)号：US20100160595A1
公开(公告)日：2010-06-24
申请号：US12718481
申请日：2010-03-05
申请人： Thomas P. Klun , Naiyong Jing , Richard J. Pokorny , Zai-Ming Qiu , Mark J. Pellerite , William D. Coggio , Christopher B. Walker, JR.
发明人： Thomas P. Klun , Naiyong Jing , Richard J. Pokorny , Zai-Ming Qiu , Mark J. Pellerite , William D. Coggio , Christopher B. Walker, JR.
CPC分类号： C07C235/08 , C08G18/3802 , C08G18/3825 , C08G18/672 , C08G18/673 , C08G18/792 , C08G18/8175 , C09D175/16 , G02B1/105 , G02B1/14 , Y10T428/265 , Y10T428/3154 , Y10T428/31551 , C08G18/50
摘要： Fluorocarbon- and urethane-(meth)acryl-containing additives and hardcoats. The hardcoats are particularly useful as a surface layer on an optical device.
摘要翻译： 含氟碳酸酯和氨基甲酸酯（甲基）丙烯酸的添加剂和硬涂层。 硬涂层作为光学装置上的表面层是特别有用的。
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公开(公告)号：US08476398B2
公开(公告)日：2013-07-02
申请号：US13396669
申请日：2012-02-15
申请人： Thomas P. Klun , Naiyong Jing , Richard J. Pokorny , Zai-Ming Qiu , Mark J. Pellerite , William D. Coggio , Christopher B. Walker, Jr.
发明人： Thomas P. Klun , Naiyong Jing , Richard J. Pokorny , Zai-Ming Qiu , Mark J. Pellerite , William D. Coggio , Christopher B. Walker, Jr.
CPC分类号： C07C235/08 , C08G18/3802 , C08G18/3825 , C08G18/672 , C08G18/673 , C08G18/792 , C08G18/8175 , C09D175/16 , G02B1/105 , G02B1/14 , Y10T428/265 , Y10T428/3154 , Y10T428/31551 , C08G18/50
摘要： Fluorocarbon- and urethane-(meth)acryl-containing additives and hardcoats. The hardcoats are particularly useful as a surface layer on an optical device.
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公开(公告)号：US07332217B2
公开(公告)日：2008-02-19
申请号：US11756662
申请日：2007-06-01
申请人： William D. Coggio , Thomas P. Klun , Mark J. Pellerite , George G. I. Moore , Cheryl L. S. Elsbernd , Sharon Wang , Richard S. Buckanin , Christopher B. Walker, Jr. , Naiyong Jing , Zai-Ming Qiu
发明人： William D. Coggio , Thomas P. Klun , Mark J. Pellerite , George G. I. Moore , Cheryl L. S. Elsbernd , Sharon Wang , Richard S. Buckanin , Christopher B. Walker, Jr. , Naiyong Jing , Zai-Ming Qiu
CPC分类号： B32B33/00 , B32B27/18 , B32B27/28 , B32B2307/21 , B32B2307/40 , B32B2457/20 , B32B2457/204 , C08F220/22 , C08F220/24 , Y10T428/10 , Y10T428/1059 , Y10T428/25 , Y10T428/263 , Y10T428/265 , Y10T428/2848 , Y10T428/3154 , Y10T428/31935
摘要： The invention relates to articles such as protective films and displays having a fluorochemical surface layer comprising an antistatic agent and the reaction products of at least one fluoropolyether (meth)acryl compound and at least 50 wt-% of non-fluorinated crosslinking agent(s).
摘要翻译： 本发明涉及诸如保护膜和显示器的制品，其具有包含抗静电剂的含氟表面层和至少一种含氟聚醚（甲基）丙烯酸化合物和至少50重量％的非氟化交联剂的反应产物， 。
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