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    Microbicidal and plant growth regulating compounds
    1.
    发明授权
    Microbicidal and plant growth regulating compounds 失效
    杀菌剂和植物生长调节化合物

    公开(公告)号：US4975459A

    公开(公告)日：1990-12-04

    申请号：US450127

    申请日：1989-12-13

    申请人： Raj J. Mehta ,  Colin Swithenbank ,  Zev Lidert ,  Margaret M. Bowers-Daines ,  David H. Young ,  Barry C. Lange

    发明人： Raj J. Mehta ,  Colin Swithenbank ,  Zev Lidert ,  Margaret M. Bowers-Daines ,  David H. Young ,  Barry C. Lange

    IPC分类号： C07D331/02 ,  A01N35/06 ,  A01N43/20 ,  A01N43/44 ,  C07C50/24 ,  C07C50/34 ,  C07C50/38 ,  C07C225/30 ,  C07C225/34 ,  C07C233/61 ,  C07D203/08 ,  C07D303/04 ,  C07D303/08 ,  C07D303/12 ,  C07D303/34 ,  C07D303/36 ,  C07D303/48

    CPC分类号： C07C50/34 ,  A01N35/06 ,  A01N43/20 ,  C07C225/30 ,  C07C225/34 ,  C07C233/61 ,  C07C50/24 ,  C07C50/38 ,  C07D303/36 ,  C07C2101/02 ,  C07C2103/24

    摘要： Process comprising the use as a microbicide or plant growth regulator of a compound of the formula ##STR1## wherein A, B, C and D is each independently selected from the group consisting of O,NR.sup.1, CR.sup.1 R.sup.1, CO, S,SO, and SO.sub.2, except for the A-C, C-A, B-D,D-B combinations: O--O, SO--SO, SO.sub.2 --SO.sub.2, S--O, S--NR.sup.2, SONR.sup.2, SO--CO, SO.sub.2 --CO, SO.sub.2 --SO;each group of the groups R.sup.1 is independently selected from the group consisting of H and (C.sub.1 -C.sub.4)alkyl;Y.sup.1 and Y.sup.2 may each be independently selected from the group consisting of H, (C.sub.1 -C.sub.4)alkyl, halogen, OR,SOR,SO.sub.2 R, SO.sub.3 R, CN, CO.sub.2 R, COR, CF.sub.3, NO.sub.2, NHCOR, and OCOR; or alternatively Y.sup.1 and Y.sup.2 and the carbons to which they are attached may comprise a cyclic structure selected from the group consisting of ##STR2## where R.sup.11 is aryl or (C.sub.1 -C.sub.4)alkylX.sup.1 to X.sup.8 is each independently selected from the group consisting of H, (C.sub.1 -C.sub.4)alkyl, halogen, OR, SOR, SO.sub.2 R, SO.sub.3 R, CN,CO.sub.2 R, COR, CF.sub.3, NO.sub.2, NHCOR, and OCOR: and furthermore optionally any pair or pairs of adjacent X's may be in the form of a divalent group attached across the adjacent X position;Z.sup.1 and Z.sup.2 is each independently selected from the group consisting of NR.sup.2, O, S, CR.sup.2 R.sup.2 where each of the groups R.sup.2 is independently selected from the group consisting of H and (C.sub.1 -C.sub.4)alkyl;each of the groups R.sup.3 is independently selected from the group consisting of CO.sub.2 R, COR, CN CF.sub.3, SOR, SO.sub.2 R, (C.sub.1 -C.sub.4)alkyl and H.

    摘要翻译： 其中A，B，C和D分别独立地选自O，NR 1，CR 1 R 1，CO，S，SO，以及其中A，B，C和D的化合物的杀微生物剂或植物生长调节剂 SO2，除了AC，CA，BD，DB组合：OO，SO-SO，SO2-SO2，SO，S-NR2，SONR2，SO-CO，SO2-CO，SO2-SO; 每个基团R 1独立地选自H和（C 1 -C 4）烷基; Y 1和Y 2可各自独立地选自H，（C 1 -C 4）烷基，卤素，OR，SOR，SO 2 R，SO 3 R，CN，CO 2 R，COR，CF 3，NO 2，NHCOR和OCOR; 或者Y1和Y2以及它们所连接的碳可以包含选自下列的环状结构：其中R11为芳基或（C1-C4）烷基X1至X8各自独立地选自 由H，（C 1 -C 4）烷基，卤素，OR，SOR，SO 2 R，SO 3 R，CN，CO 2 R，COR，CF 3，NO 2，NHCOR和OCOR组成的组： 为相邻X位置附近的二价基团的形式; Z 1和Z 2各自独立地选自NR 2，O，S，CR 2 R 2，其中每个基团R 2独立地选自H和（C 1 -C 4）烷基; 基团R3各自独立地选自CO 2 R，COR，CN CF 3，SOR，SO 2 R，（C 1 -C 4）烷基和H.

    Preparation and use of iodopropargyl esters of .alpha.-amino acid derivatives as antimicrobial agents
    3.
    发明授权
    Preparation and use of iodopropargyl esters of .alpha.-amino acid derivatives as antimicrobial agents 失效
    制备和使用α-氨基酸衍生物的碘代炔丙酯作为抗微生物剂

    公开(公告)号：US5252745A

    公开(公告)日：1993-10-12

    申请号：US704906

    申请日：1991-05-21

    申请人： Margaret M. Bowers-Daines ,  Barry C. Lange

    发明人： Margaret M. Bowers-Daines ,  Barry C. Lange

    IPC分类号： A01N37/44 ,  A01N37/46 ,  A01N47/10 ,  C07C229/08 ,  C07C233/49 ,  C07C271/22 ,  C07C229/00

    CPC分类号： A01N37/44 ,  A01N37/46 ,  A01N47/10 ,  C07C229/08 ,  C07C233/49 ,  C07C271/22 ,  Y02P20/55

    摘要： Antimicrobial compounds of the formula ##STR1## wherein R.sup.1 is selected from the group consisting of H, an amine protective group, and a moiety of the formula ##STR2## wherein R.sup.2, R.sup.5, and R.sup.6 are independently selected from H and an amine protective group;R.sup.3 and R.sup.4 are independently selected from H, lower alkyl, aryl, arylalkyl, CH.sub.2 OR, CH.sub.2 SR or CH(CH.sub.3)OR;R=H, propargyl lower alkyl, arylalkyl or aryl;wherein R.sup.1 and R.sup.2 or R.sup.5 and R.sup.6 can be joined to form a ring; and wherein when R.sup.1 and R.sup.2 or R.sup.5 and R.sup.6 are both H, the compound is either in free base form or in salt form.

    摘要翻译： 式（Ⅰ）的抗微生物化合物其中R 1选自H，胺保护基和式（II）的部分，其中R 2，R 5和R 6独立地选自 H和胺保护基; R3和R4独立地选自H，低级烷基，芳基，芳烷基，CH2OR，CH2SR或CH（CH3）OR; R = H，炔丙基低级烷基，芳烷基或芳基; 其中R1和R2或R5和R6可以连接形成环; 并且其中当R 1和R 2或R 5和R 6均为H时，所述化合物为游离碱形式或盐形式。

    Process for preparation of iodopropargyl carbamates
    10.
    发明授权
    Process for preparation of iodopropargyl carbamates 失效
    碘代炔丙基氨基甲酸酯的制备方法

    公开(公告)号：US5326899A

    公开(公告)日：1994-07-05

    申请号：US76561

    申请日：1993-06-14

    申请人： Barry C. Lange

    发明人： Barry C. Lange

    IPC分类号： B01J21/04 ,  B01J27/08 ,  B01J27/26 ,  B01J31/02 ,  B01J31/04 ,  B01J31/12 ,  C07B61/00 ,  C07C269/04 ,  C07C271/12 ,  C07C261/00

    CPC分类号： C07C269/04 ,  C07C271/12

    摘要： A Process for producing N-alkyl iodopropargyl carbamate comprising:A. reacting a dialkyl(C.sub.1 -C.sub.3) carbonate with propargyl alcohol in the presence of a first catalyst under conditions to produce dipropargyl carbonate;B. reacting said dipropargyl carbonate with an alkyl(C.sub.1 -C.sub.6)amine, optionally in the presence of a second catalyst, to produce N-alkyl(C.sub.1 -C.sub.6) propargyl carbamate;C. reacting said N-alkyl(C.sub.1 -C.sub.6) propargyl carbamate with an iodinating agent to produce N-alkyl(C.sub.1 -C.sub.6) iodopropargyl carbamate is disclosed.

    摘要翻译： 一种N-烷基碘炔丙基氨基甲酸酯的制备方法，其包括：A.在第一催化剂存在下，在产生碳酸二丙酯的条件下，使碳酸二烷基酯（C 1 -C 3）与炔丙醇反应; B.任选在第二催化剂存在下，使所述碳酸二丙酯与烷基（C 1 -C 6）反应，生成N-烷基（C 1 -C 6）炔丙基氨基甲酸酯; C.公开了使所述N-烷基（C 1 -C 6）炔丙基氨基甲酸酯与碘化剂反应以制备N-烷基（C1-C6）碘炔丙基氨基甲酸酯。