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    Crude oil desalting method
    2.
    发明授权
    Crude oil desalting method 失效
    原油脱盐方法

    公开(公告)号：US06228239B1

    公开(公告)日：2001-05-08

    申请号：US09258620

    申请日：1999-02-26

    申请人： Pacifico V. Manalastas ,  Ramesh Varadaraj ,  David W. Savage ,  Guido Sartori ,  Ramesh R. Hemrajani ,  Cornelius Hendrick Brons

    发明人： Pacifico V. Manalastas ,  Ramesh Varadaraj ,  David W. Savage ,  Guido Sartori ,  Ramesh R. Hemrajani ,  Cornelius Hendrick Brons

    IPC分类号： B01D1706

    CPC分类号： C10G33/00 ,  C10G31/08 ,  C10G33/02 ,  C10G33/04

    摘要： In one embodiment, the invention is related to a process for desalting crude oil that requires less wash water than conventional desalting methods. In the preferred embodiment of the invention, a chemical demulsifier formulation comprising an emulsion-breaking chemical and a solvent carrier is added to the crude oil. Wash water is then added to the crude oil until the volume of water in the oil ranges from about 0.1 to about 3 vol. %. Subsequently, the mixture of crude oil, wash water, and chemical demulsifier formulation is subjected to opposed-flow mixing. Chemical emulsion-breakers useful in the invention have a hydrophobic tail group and a hydrophilic head group. Preferably, the emulsion breaker has the formula: x ranges from 1 to 5, y ranges from 0 to 2, and R is an alkyl group having 4-9 carbon atoms, and n ranges from 3 to 9.

    摘要翻译： 在一个实施方案中，本发明涉及与常规脱盐方法相比需要较少洗涤水的原油脱盐方法。 在本发明的优选实施方案中，将包含破乳化学品和溶剂载体的化学破乳剂制剂加入到原油中。 然后将洗涤水加入到原油中，直到油中的水的体积为约0.1至约3体积％。 ％。 随后，将原油，洗涤水和化学破乳剂制剂的混合物进行相反流混合。 可用于本发明的化学乳液破乳剂具有疏水性尾基和亲水性头基。 优选地，破乳剂具有下式：x为1至5，y为0至2，R为具有4-9个碳原子的烷基，n为3至9。

    Chemical demulsifier for desalting heavy crude
    3.
    发明授权
    Chemical demulsifier for desalting heavy crude 失效
    化学破乳剂用于脱盐重质原油

    公开(公告)号：US06168702A

    公开(公告)日：2001-01-02

    申请号：US09258618

    申请日：1999-02-26

    申请人： Ramesh Varadaraj ,  David W. Savage ,  Cornelius H. Brons

    发明人： Ramesh Varadaraj ,  David W. Savage ,  Cornelius H. Brons

    IPC分类号： B01D1706

    CPC分类号： C10G33/04

    摘要： The chemical demulsifier formulation has the formula: wherein R1 is H or an alkoxide of from 5 to about 20 carbon atoms; x is an integer of from about 8 to about 22 when R1 is hydrogen and from about 2 to about 5 when R1 is alkoxide; R2 is independently selected from H, (CH2CH2O)mH; R3 is independently selected from H, (CH2CH2O)nH, and (CH2CH(CH3)O)nH; m and n are integers from 1 to 50; and y and z are integers ranging from 2 to 10.

    摘要翻译： 化学破乳剂制剂具有下式：其中R1是H或5至约20个碳原子的醇盐; 当R 1为氢时，x为约8至约22的整数，当R 1为醇盐时，x为约2至约5; R2独立地选自H，（CH 2 CH 2 O）m H; R 3独立地选自H，（CH 2 CH 2 O）n H和（CH 2 CH（CH 3）O）n H; m和n是1至50的整数; y和z为2〜10的整数。

    Removal of naphthenic acids in crude oils and distillates
    4.
    发明授权
    Removal of naphthenic acids in crude oils and distillates 失效
    去除原油和馏出物中的环烷酸

    公开(公告)号：US6096196A

    公开(公告)日：2000-08-01

    申请号：US49465

    申请日：1998-03-27

    申请人： Ramesh Varadaraj ,  Thomas M. Pugel ,  David W. Savage

    发明人： Ramesh Varadaraj ,  Thomas M. Pugel ,  David W. Savage

    IPC分类号： C10G19/02 ,  C10G21/20 ,  C10G29/00 ,  C10G29/20 ,  C10G19/00

    CPC分类号： C10G21/20 ,  C10G19/02 ,  C10G29/20 ,  C10G2300/203

    摘要： The instant invention is directed a process for extracting organic acids from a starting crude oil comprising the steps of: (a) treating the starting crude oil containing naphthenic acids with an amount of an alkoxylated amine and water under conditions and for a time and at a temperature sufficient to form a water-in-oil emulsion of amine salt wherein said alkoxylated amine is selected from the group consisting of alkoxylated amines having the following formulae (A) and (B): ##STR1## where m+n=5 to 50 and R=linear or branched alkyl group of C.sub.8 to C.sub.20.(B) H-(OCH.sub.2 CH.sub.2).sub.y -(CH.sub.2 CHCH.sub.3 O).sub.p -{NHCH.sub.2 CH.sub.2 NH}.sub.x -(CH.sub.2 CH.sub.2 O).sub.z -(CH.sub.2 CHCH.sub.3 O).sub.q -Hwhere x=1 to 3 and y+z=2 to 6, and wherein p+q=0 to 15, mixtures of formula (A) and mixtures of formula (B); wherein said starting crude oil is selected from the group consisting of crude oils, crude oil blends, and crude oil distillates; and (b) separating said emulsion of step (a) into a plurality of layers, wherein one of such layers contains a treated crude oil having decreased amounts of organic acids; (c) recovering said layer of step (b) containing said treated crude oil having a decreased amount of organic acid and layers containing water and alkoxylated amine salt.

    摘要翻译： 本发明涉及一种从起始原油中提取有机酸的方法，包括以下步骤：（a）在条件和时间和时间内用一定量的烷氧基化胺和水处理含有环烷酸的起始原油 温度足以形成胺盐的油包水乳液，其中所述烷氧基化胺选自具有下式（A）和（B）的烷氧基​​化胺：其中m + n = 5-50且R = （B）H-（OCH 2 CH 2）y - （CH 2 CHCH 3 O）对{（NHCH 2 CH 2 NH）x - （CH 2 CH 2 O）z - （CH 2 CH 3 O）q-H，其中x = 1至3，y + z = 2至6，并且其中p + q = 0至15，式（A）和式（B）的混合物的混合物; 其中所述起始原油选自原油，原油混合物和原油馏出物; 和（b）将步骤（a）的所述乳液分离成多个层，其中这些层之一含有具有降低量的有机酸的经处理的原油; （c）回收所述含有所述经处理的原油的步骤（b）的层具有减少量的有机酸和含有水和烷氧基化胺盐的层。

    Process for the desulfurization of heavy oils and bitumens
    5.
    发明申请
    Process for the desulfurization of heavy oils and bitumens 有权
    重油和沥青脱硫工艺

    公开(公告)号：US20090152168A1

    公开(公告)日：2009-06-18

    申请号：US12287744

    申请日：2008-10-14

    申请人： Michael Siskin ,  Rustom M. Billimoria ,  David W. Savage ,  Roby Bearden, JR.

    发明人： Michael Siskin ,  Rustom M. Billimoria ,  David W. Savage ,  Roby Bearden, JR.

    IPC分类号： C10G19/00

    CPC分类号： C10G45/02 ,  C10G19/02

    摘要： The present invention relates to a process for desulfurizing bitumen and other heavy oils such as low API gravity, high viscosity crudes, tar sands bitumen, or shale oils with alkali metal compounds under conditions to promote in-situ regeneration of the alkali metal compounds. The present invention employs the use of superheated water and hydrogen under conditions to improve the desulfurization and alkali metal hydroxide regeneration kinetics at sub-critical temperatures.

    摘要翻译： 本发明涉及一种在碱性金属化合物的原位再生条件下使沥青和其它重油如API重力低，高粘度原油，焦油砂沥青或页岩油脱硫的方法。 本发明使用过热水和氢气条件来改善亚临界温度下的脱硫和碱金属氢氧化物再生动力学。

    Zeolite composition for use in olefinic separations
    6.
    发明授权
    Zeolite composition for use in olefinic separations 失效
    用于烯烃分离的沸石组合物

    公开(公告)号：US5292990A

    公开(公告)日：1994-03-08

    申请号：US625337

    申请日：1990-12-10

    申请人： Edward Kantner ,  David W. Savage ,  Richard J. Bellows

    发明人： Edward Kantner ,  David W. Savage ,  Richard J. Bellows

    IPC分类号： B01J29/40 ,  C10G25/03 ,  C07C7/12

    CPC分类号： B01J29/40 ,  C10G25/03 ,  B01J2229/26 ,  B01J2229/42

    摘要： Basically, the present invention is predicated on the discovery that zeolites that have a high silica to alumina ratio, e.g., a ratio of 20 and above, pore diameters of greater than about 5.0.ANG., and which have substantially no active acid sites, i.e., zeolites which are non-reactive toward olefin isomerization and oligomerization, are especially useful in substantially separating linear olefins and paraffins from hydrocarbon mixtures containing at least linear and branched aliphatic hydrocarbons and optionally containing aromatic and other hydrocarbons.

    摘要翻译： 基本上，本发明基于以下发现：发现具有高二氧化硅与氧化铝比例的比例，例如20以上的孔径大于约5.0（Aangstroem），并且基本上没有活性酸性位点， 即对烯烃异构化和低聚不具有反应性的沸石特别可用于从至少含有直链和支链脂族烃并任选含有芳烃和其它烃的烃混合物中基本分离直链烯烃和链烷烃。