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公开(公告)号：US11767225B2
公开(公告)日：2023-09-26
申请号：US16324296
申请日：2017-08-10
Applicant: Research Triangle Institute
Inventor： Ignacio Luz Minguez , Mustapha Soukri , Marty Lail
CPC classification number: C01B39/026 , B01J20/103 , B01J20/226 , B01J20/3236 , B01J20/3265 , B01J29/06 , B01J31/1691 , C01B39/00 , C01B39/02 , C01B39/48 , B01D2253/108 , B01D2253/204 , B01D2259/4583
Abstract: A method, comprising i) contacting an aqueous solution of an organic ligand salt of the formula AX(L−X) with a mesoporous material (MPM) to form an impregnated mesoporous salt material of the formula AX(L−X)/MPM, ii) treating the impregnated mesoporous salt material with an aqueous acidic solution to form an impregnated mesoporous acid material of the formula HX(L−X)/MPM, iii) contacting an aqueous solution of a metal precursor of the formula M+y(B)y with the impregnated mesoporous acid material to form an impregnated mesoporous metal organic framework precursor of the formula [M+y(B)y][Hx(L−x)]/MPM, and iv) at least one of 1) heating the impregnated mesoporous metal organic framework precursor in the absence of a solvent or 2) exposing the impregnated mesoporous metal organic framework precursor to a volatile vapor in the absence of a solvent such that the heating or the exposing forms a hybrid material of the formula (M+yL−x)/MPM, wherein the hybrid material comprises a nano-crystalline metal organic framework (MOF) embedded within the mesoporous material.
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2.发明公开公开(公告)号：US20240327229A1
公开(公告)日：2024-10-03
申请号：US18732873
申请日：2024-06-04
Applicant: Research Triangle Institute
Inventor： Ignacio Luz Minguez , Mustapha Soukri , David Dausch
IPC: C01B33/025 , B82Y30/00 , B82Y40/00 , C07F3/02 , H01M4/36 , H01M4/38 , H01M10/0525
CPC classification number: C01B33/025 , C07F3/02 , H01M4/362 , H01M4/386 , H01M10/0525 , B82Y30/00 , B82Y40/00 , C01P2002/01 , C01P2002/82 , C01P2004/64 , C01P2004/80 , C01P2006/14 , C01P2006/40
Abstract: An anode material for a lithium ion battery comprises a carbonaceous silicon composite material. The composite material comprises Si nanoparticles, and nanostructured and microporous graphitic carbon and/or silicon carbide, wherein the graphitic carbon and/or silicon carbide are derived at least in part from carbonized metal organic framework.
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公开(公告)号：US20210309588A1
公开(公告)日：2021-10-07
申请号：US17262490
申请日：2019-07-17
Inventor： Iker Aguirrezabal , Ignacio Luz Minguez , Mustapha Soukri , Marty Lail , Pedro Luis Arias
Abstract: Described herein is a catalytic reaction process including introducing one or more gas-phase reactants into a reactor comprising a microporous catalyst having a pore size less than or equal to 2 nm and adjusting the temperature and/or the pressure of the reactor such that one or more of the gas-phase reactants condense within the micropores of the catalyst thereby causing the catalytic reaction to take place in a liquid phase. Additionally, a process for engineering defects on a carboxylate-based metal organic framework (MOF) catalyst is described. The process includes providing a carboxylate-based MOF catalyst; and heating the carboxylate-based MOF catalyst in an inert gas atmosphere at temperatures between about 150° C. and about 900° C.
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公开(公告)号：US12109549B2
公开(公告)日：2024-10-08
申请号：US17054590
申请日：2019-05-17
Applicant: Research Triangle Institute
Inventor： Ignacio Luz Minguez , Mustapha Soukri , Marty Lail , Lora Goon Toy
CPC classification number: B01J20/226 , B01D53/02 , B01D53/228 , B01J20/28026 , B01J20/28033 , B01J20/28059 , B01J20/28061 , B01J20/28064 , B01J20/28066 , B01J20/28083 , B01D2253/204
Abstract: A method for making a metal organic framework suspension is described herein. The method includes providing a hybrid material comprising a nano-crystalline metal organic framework comprising micropores and a mesoporous polymeric material comprising mesopores, wherein the nano-crystalline metal organic framework is homogeneously dispersed and substantially present only within the mesopores or void spaces of the mesoporous polymeric material; and wherein the hybrid material has a weight percentage of the metal organic framework in the range of 5-50% relative to the total weight of the hybrid material. The method includes contacting the hybrid material with a solvent in which the mesoporous polymeric material is soluble, thereby forming a polymeric solution in which the nano-crystalline metal organic framework is substantially homogeneously dispersed and suspended.
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公开(公告)号：US11795554B2
公开(公告)日：2023-10-24
申请号：US16786150
申请日：2020-02-10
Applicant: Research Triangle Institute
Inventor： Aravind Villava Rayer Rabindran , Elliot Reid , Ignacio Luz Minguez , Mustapha Soukri , Marty Lail , Shaojun James Zhou
IPC: C25B3/07 , C25B3/26 , C25B3/25 , B01J31/16 , B01J37/08 , C09D11/52 , C25B11/043 , C07C31/10 , C25B15/08
CPC classification number: C25B3/25 , B01J31/1616 , B01J37/08 , C09D11/52 , C25B11/043 , B01J2531/16 , C07C31/10 , C25B15/08
Abstract: A carbon dioxide reduction reaction electrocatalyst comprises a pyrolyzed copper-based metal-organic framework (MOF) that produces isopropanol from electrochemical reduction of carbon dioxide. A process for producing isopropanol from electrochemical reduction of carbon dioxide comprises applying a potential in an electrochemical cell in the range of about −2V to about −3V versus a silver chloride electrode.
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Patent Agency Ranking
公开(公告)号：US12116286B2
公开(公告)日：2024-10-15
申请号：US17962217
申请日：2022-10-07
Applicant: Research Triangle Institute
Inventor： Ignacio Luz Minguez , Mustapha Soukri , Marty Lail
CPC classification number: C01B39/026 , B01J20/103 , B01J20/226 , B01J20/3236 , B01J20/3265 , B01J29/06 , B01J31/1691 , C01B39/00 , C01B39/02 , C01B39/48 , B01D2253/108 , B01D2253/204 , B01D2259/4583
Abstract: A method, comprising i) contacting an aqueous solution of an organic ligand salt of the formula Ax(L−x) with a mesoporous material (MPM) to form an impregnated mesoporous salt material of the formula Ax(L−x)/MPM, ii) treating the impregnated mesoporous salt material with an aqueous acidic solution to form an impregnated mesoporous acid material of the formula Hx(L−x)/MPM, iii) contacting an aqueous solution of a metal precursor of the formula M+y(B)y with the impregnated mesoporous acid material to form an impregnated mesoporous metal organic framework precursor of the formula [M+y(B)y][Hx(L−x)]/MPM, and iv) at least one of 1) heating the impregnated mesoporous metal organic framework precursor in the absence of a solvent or 2) exposing the impregnated mesoporous metal organic framework precursor to a volatile vapor in the absence of a solvent such that the heating or the exposing forms a hybrid material of the formula (M+yL−x)/MPM, wherein the hybrid material comprises a nano-crystalline metal organic framework (MOF) embedded within the mesoporous material.
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7.发明公开公开(公告)号：US20230398112A1
公开(公告)日：2023-12-14
申请号：US18020687
申请日：2021-07-30
Applicant: Research Triangle Institute
Inventor： Ian Edward Stewart , Ignacio Luz Minguez , Anthony James Hickey
IPC: A61K31/4965 , A61K9/16 , A61K9/00 , A61K49/18 , A61K49/04
CPC classification number: A61K31/4965 , A61K9/1611 , A61K9/0073 , A61K49/1887 , A61K49/0419
Abstract: Spray-dried metal-organic frameworks (MOFs) comprising therapeutic and/or diagnostic metal ions and therapeutic and/or diagnostic organic ligands are described. Both the metal ion and organic ligand can have activity related to the treatment and/or diagnosis of a pulmonary disease or disorder, such as tuberculosis, or another disease related to a pulmonary infection. The MOFs can be adminstered to subjects via inhalation (e.g., as aerosols). Methods of treating and diagnosing pulmonary diseases or disorders are also described.
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公开(公告)号：US20230039640A1
公开(公告)日：2023-02-09
申请号：US17962217
申请日：2022-10-07
Applicant: Research Triangle Institute
Inventor： Ignacio Luz Minguez , Mustapha Soukri , Marty Lail
Abstract: A method, comprising i) contacting an aqueous solution of an organic ligand salt of the formula Ax(L-x) with a mesoporous material (MPM) to form an impregnated mesoporous salt material of the formula Ax(L-x)/MPM, ii) treating the impregnated mesoporous salt material with an aqueous acidic solution to form an impregnated mesoporous acid material of the formula Hx(L- x)/MPM, iii) contacting an aqueous solution of a metal precursor of the formula M+y(B)y with the impregnated mesoporous acid material to form an impregnated mesoporous metal organic framework precursor of the formula [M+y(B)y][Hx(L-x)]/MPM, and iv) at least one of 1) heating the impregnated mesoporous metal organic framework precursor in the absence of a solvent or 2) exposing the impregnated mesoporous metal organic framework precursor to a volatile vapor in the absence of a solvent such that the heating or the exposing forms a hybrid material of the formula (M+yL-x)/MPM, wherein the hybrid material comprises a nano-crystalline metal organic framework (MOF) embedded within the mesoporous material.
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9.发明申请公开(公告)号：US20190169036A1
公开(公告)日：2019-06-06
申请号：US16324296
申请日：2017-08-10
Applicant: Research Triangle Institute
Inventor： Ignacio Luz Minguez , Mustapha Soukri , Marty Lail
Abstract: A method, comprising i) contacting an aqueous solution of an organic ligand salt of the formula AX(L−X) with a mesoporous material (MPM) to form an impregnated mesoporous salt material of the formula AX(L−X)/MPM, ii) treating the impregnated mesoporous salt material with an aqueous acidic solution to form an impregnated mesoporous acid material of the formula HX(L−X)/MPM, iii) contacting an aqueous solution of a metal precursor of the formula M+y(B)y with the impregnated mesoporous acid material to form an impregnated mesoporous metal organic framework precursor of the formula [M+y(B)y][Hx(L−x)]/MPM, and iv) at least one of 1) heating the impregnated mesoporous metal organic framework precursor in the absence of a solvent or 2) exposing the impregnated mesoporous metal organic framework precursor to a volatile vapor in the absence of a solvent such that the heating or the exposing forms a hybrid material of the formula (M+yL−x)/MPM, wherein the hybrid material comprises a nano-crystalline metal organic framework (MOF) embedded within the mesoporous material.
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公开(公告)号：US11795122B2
公开(公告)日：2023-10-24
申请号：US17262490
申请日：2019-07-17
Inventor： Iker Aguirrezabal , Ignacio Luz Minguez , Mustapha Soukri , Marty Lail , Pedro Luis Arias
CPC classification number: C07C2/32 , B01J31/1691 , B01J35/1057 , B01J2231/12 , B01J2531/821 , C07C2523/46 , C07C2531/22
Abstract: Described herein is a catalytic reaction process including introducing one or more gas-phase reactants into a reactor comprising a microporous catalyst having a pore size less than or equal to 2 nm and adjusting the temperature and/or the pressure of the reactor such that one or more of the gas-phase reactants condense within the micropores of the catalyst thereby causing the catalytic reaction to take place in a liquid phase. Additionally, a process for engineering defects on a carboxylate-based metal organic framework (MOF) catalyst is described. The process includes providing a carboxylate-based MOF catalyst; and heating the carboxylate-based MOF catalyst in an inert gas atmosphere at temperatures between about 150° C. and about 900° C.
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