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    Fluid hydrocracking catalyst precursor and method
    1.
    发明授权
    Fluid hydrocracking catalyst precursor and method 失效
    流体加氢裂化催化剂前体及方法

    公开(公告)号：US5954945A

    公开(公告)日：1999-09-21

    申请号：US827191

    申请日：1997-03-27

    申请人： Roger H. Cayton ,  Ronald B. Fisher ,  Jeffrey T. Miller ,  John A. Waynick

    发明人： Roger H. Cayton ,  Ronald B. Fisher ,  Jeffrey T. Miller ,  John A. Waynick

    IPC分类号： C10G47/26 ,  C10G47/02

    CPC分类号： C10G47/26

    摘要： A method for converting a hydrocarbonaceous feedstock to a lower boiling temperature product is described which comprises suspending metal sulfide particles and oxide particles in a reaction zone including hydrogen and the hydrocarbonaceous feedstock at hydrocracking conditions. The metal sulfide particles and the oxide particles are introduced into the reaction zone through particle precursor fluids which precipitate upon heating to form the particles. The metal sulfide particles contain sulfidable transition metals. The oxide particles contain oxidisable elements such as magnesium, aluminum, silicon, phosphorous, calcium, scandium, titanium, gallium, germanium, zirconium, cerium, and mixtures thereof and are not hydrogenation catalysts under the reactor conditions. The oxide particles resist being chemically reduced by reducing agents in the reaction zone. Surprisingly, the presence of the oxide particles is associated with a significant reduction of coke production in the reaction zone. A hydrogenation catalyst precursor comprising a hydrocarbonaceous feedstock, a sulfide particle precursor fluid, and an oxide particle precursor fluid is also described.

    摘要翻译： 描述了将烃原料转化为低沸点产物的方法，其包括在加氢裂化条件下将包含氢和烃原料的金属硫化物颗粒和氧化物颗粒悬浮在反应区中。 金属硫化物颗粒和氧化物颗粒通过在加热时沉淀形成颗粒的颗粒前体流体引入反应区。 金属硫化物颗粒含有可硫化的过渡金属。 氧化物颗粒含有可氧化元素如镁，铝，硅，磷，钙，钪，钛，镓，锗，锆，铈及其混合物，并且在反应器条件下不是氢化催化剂。 氧化物颗粒抵抗由反应区中的还原剂化学还原。 令人惊奇的是，氧化物颗粒的存在与反应区中焦炭产生的显着降低有关。 还描述了包含烃原料，硫化物颗粒前体流体和氧化物颗粒前体流体的氢化催化剂前体。

    Fluid hydrocracking catalyst precursor and method
    2.
    发明授权
    Fluid hydrocracking catalyst precursor and method 有权
    流体加氢裂化催化剂前体及方法

    公开(公告)号：US06274530B1

    公开(公告)日：2001-08-14

    申请号：US09338331

    申请日：1999-06-22

    申请人： Roger H. Cayton ,  Ronald B. Fisher ,  Jeffrey T. Miller ,  John A. Waynick

    发明人： Roger H. Cayton ,  Ronald B. Fisher ,  Jeffrey T. Miller ,  John A. Waynick

    IPC分类号： B01J2702

    CPC分类号： C10G47/26

    摘要： A method for converting a hydrocarbonaceous feedstock to a lower boiling temperature product is described which comprises suspending metal sulfide particles and oxide particles in a reaction zone including hydrogen and the hydrocarbonaceous feedstock at hydrocracking conditions. The metal sulfide particles and the oxide particles are introduced into the reaction zone through particle precursor fluids which precipitate upon heating to form the particles. The metal sulfide particles contain sulfidable transition metals. The oxide particles contain oxidizable elements such as magnesium, aluminum, silicon, phosphorous, calcium, scandium, titanium, gallium, germanium, zirconium, cerium, and mixtures thereof and are not hydrogenation catalysts under the reactor conditions. The oxide particles resist being chemically reduced by reducing agents in the reaction zone. Surprisingly, the presence of the oxide particles is associated with a significant reduction of coke production in the reaction zone. A hydrogenation catalyst precursor comprising a hydrocarbonaceous feedstock, a sulfide particle precursor fluid, and an oxide particle precursor fluid is also described.

    摘要翻译： 描述了将烃原料转化为低沸点产物的方法，其包括在加氢裂化条件下将包含氢和烃原料的金属硫化物颗粒和氧化物颗粒悬浮在反应区中。 金属硫化物颗粒和氧化物颗粒通过在加热时沉淀形成颗粒的颗粒前体流体引入反应区。 金属硫化物颗粒含有可硫化的过渡金属。 氧化物颗粒含有可氧化元素如镁，铝，硅，磷，钙，钪，钛，镓，锗，锆，铈及其混合物，并且在反应器条件下不是氢化催化剂。 氧化物颗粒抵抗由反应区中的还原剂化学还原。 令人惊奇的是，氧化物颗粒的存在与反应区中焦炭产生的显着降低有关。 还描述了包含烃原料，硫化物颗粒前体流体和氧化物颗粒前体流体的氢化催化剂前体。

    Resid hydroprocessing method utilizing a metal-impregnated, carbonaceous particle catalyst
    3.
    发明授权
    Resid hydroprocessing method utilizing a metal-impregnated, carbonaceous particle catalyst 失效
    使用金属浸渍的碳质颗粒催化剂的残留加氢处理方法

    公开(公告)号：US5951849A

    公开(公告)日：1999-09-14

    申请号：US761746

    申请日：1996-12-05

    申请人： Jeffrey T. Miller ,  Ronald B. Fisher ,  Tracy L. Marshbanks

    发明人： Jeffrey T. Miller ,  Ronald B. Fisher ,  Tracy L. Marshbanks

    IPC分类号： B01J27/04 ,  C10G47/06 ,  C10G47/26

    CPC分类号： C10G47/26 ,  Y10S977/775

    摘要： A method for converting a hydrocarbonaceous feedstock to a lower boiling product is described which comprises suspending metal-impregnated carbonaceous particles in a reaction zone including hydrogen and the hydrocarbonaceous feedstock at hydrocracking conditions. The metal impregnated on the particles may be sulfided in the reaction zone. The impregnated particles are shown to be surprisingly selective catalysts, and anomalous ranges of particle size and concentration are identified. Methods for preparing the particles are additionally presented.

    摘要翻译： 描述了一种将含烃原料转化为低沸点产物的方法，其包括在加氢裂化条件下将金属浸渍的碳质颗粒悬浮在包含氢和烃原料的反应区中。 浸渍在颗粒上的金属可能在反应区中被硫化。 浸渍的颗粒被证明是令人惊讶的选择性催化剂，并且确定了颗粒尺寸和浓度的异常范围。 另外提供了制备颗粒的方法。

    Para-Xylene Selective Adsorbent Compositions and Methods
    5.
    发明申请
    Para-Xylene Selective Adsorbent Compositions and Methods 审中-公开
    对二甲苯选择性吸附剂组合物和方法

    公开(公告)号：US20080200742A1

    公开(公告)日：2008-08-21

    申请号：US11470346

    申请日：2006-09-06

    申请人： Ruth Ann Doyle ,  Bryce A. Williams ,  Jeffrey T. Miller

    发明人： Ruth Ann Doyle ,  Bryce A. Williams ,  Jeffrey T. Miller

    IPC分类号： C07C5/22 ,  B01D59/26

    CPC分类号： B01J20/183 ,  B01J20/0292 ,  B01J20/2803 ,  B01J20/28069 ,  B01J20/28083 ,  B01J20/28085 ,  B01J20/28092 ,  C07C7/13 ,  C07C15/067

    摘要： Adsorbent compositions for vapor-phase adsorption processes, which are selective for para-xylene. Such compositions can be used in gas-phase adsorption processes for the separation of para-xylene or the separation of para-xylene and ethylbenzene from mixed xylenes or a C8 aromatic mixture, respectively. The adsorbent compositions generally comprise materials of a molecular sieve material and a binder, wherein the adsorbent composition has a macropore volume of at least about 0.02 cc/g and a mesopore volume of less than about 0.20 cc/g.

    摘要翻译： 用于气相吸附方法的吸附剂组合物，其对对二甲苯是选择性的。 这种组合物可以用于分离对二甲苯的气相吸附方法或分别从混合二甲苯或C 8 C 8芳族混合物中分离对二甲苯和乙苯。 吸附剂组合物通常包括分子筛材料和粘合剂的材料，其中吸附剂组合物具有至少约0.02cc / g的大孔体积和小于约0.20cc / g的中孔体积。

    Catalyst and process for high selectivity reforming with Pt/Re on Ba-K-L zeolite
    6.
    发明授权
    Catalyst and process for high selectivity reforming with Pt/Re on Ba-K-L zeolite 失效
    Pt / Re对Ba-K-L沸石进行高选择性重整的催化剂和方法

    公开(公告)号：US4954245A

    公开(公告)日：1990-09-04

    申请号：US287397

    申请日：1988-12-20

    申请人： Jeffrey T. Miller ,  Victor K. Shum

    发明人： Jeffrey T. Miller ,  Victor K. Shum

    IPC分类号： B01J29/60 ,  C10G35/095

    CPC分类号： B01J29/60 ,  C10G35/095 ,  B01J2229/26 ,  B01J2229/42

    摘要： This invention comprises a reforming catalyst and process with an unsulfided catalyst comprising Zeolite L, in which the cationic sites have been exchanged to contain potassium or barium or both; a Group VIII noble metal and rhenium, where the ratio of noble metal to rhenium is from about 0.1:1 to about 10:0. This catalyst gives improved selectivity toward aromatics formation and has improved sulfur tolerance compared to other L zeolite reforming catalysts.

    摘要翻译： 本发明包括重整催化剂和具有包含沸石L的未硫化催化剂的方法，其中阳离子位点已经被交换以含有钾或钡或两者; 第VIII族贵金属和铼，其中贵金属与铼的比例为约0.1:1至约10:0。 该催化剂提高了芳烃形成的选择性，并且与其它L沸石重整催化剂相比具有改善的耐硫化性。

    Methods of Making Xylene Isomers
    8.
    发明申请
    Methods of Making Xylene Isomers 审中-公开
    制备二甲苯异构体的方法

    公开(公告)号：US20130184509A1

    公开(公告)日：2013-07-18

    申请号：US13783654

    申请日：2013-03-04

    申请人： Hilary E. Schwartz ,  Jeffrey T. Miller ,  Brian J. Henley ,  George A. Huff

    发明人： Hilary E. Schwartz ,  Jeffrey T. Miller ,  Brian J. Henley ,  George A. Huff

    IPC分类号： C07C6/00 ,  C07C5/27

    CPC分类号： C07C6/00 ,  C07C5/2708 ,  C07C6/126 ,  C07C2529/26 ,  Y02P20/52 ,  C07C15/08

    摘要： Disclosed herein are methods of making xylene isomers. The methods generally include contacting an aromatics-comprising feed with a non-sulfided catalyst under conditions suitable for converting the feed to a product comprising xylene isomers. The catalyst includes a support impregnated with a hydrogenation component. The support includes a macroporous binder and a sieve selected from the group consisting of a medium pore sieve, a large pore sieve, and mixtures thereof. The selection of the sieve will depend upon the size of the molecules in the feed, intermediate, and product that can be expected from the catalytic reactions. When the molecules are expected to be large, a large pore sieve should be used. In contrast, when the molecules are expected to be smaller, either a large pore sieve, a medium pore sieve, or a mixture thereof may be used. The macropores within the support have been found to be especially beneficial because they help to overcome diffusional limitations observed when utilizing highly-active catalysts lacking such macropores.

    摘要翻译： 本文公开了制备二甲苯异构体的方法。 所述方法通常包括在适于将进料转化为包含二甲苯异构体的产物的条件下使包含芳烃的进料与非硫化催化剂接触。 催化剂包括浸渍有氢化组分的载体。 载体包括大孔粘合剂和选自中孔筛，大孔筛及其混合物的筛子。 筛子的选择将取决于催化反应可以预期的进料，中间体和产物中分子的大小。 当分子预期较大时，应使用大孔隙筛。 相反，当分子预期更小时，可以使用大孔隙筛孔，中孔筛或其混合物。 发现载体中的大孔是特别有益的，因为它们有助于克服当使用缺乏这种大孔的高活性催化剂时观察到的扩散限制。

    Para-xylene selective adsorbent compositions and methods
    9.
    发明授权
    Para-xylene selective adsorbent compositions and methods 有权
    对二甲苯选择性吸附剂组合物和方法

    公开(公告)号：US07122496B2

    公开(公告)日：2006-10-17

    申请号：US10427879

    申请日：2003-05-01

    申请人： Ruth Ann Doyle ,  Bryce A. Williams ,  Jeffrey T. Miller

    发明人： Ruth Ann Doyle ,  Bryce A. Williams ,  Jeffrey T. Miller

    IPC分类号： B01J29/06 ,  B01J21/00

    CPC分类号： B01J20/183 ,  B01J20/0292 ,  B01J20/2803 ,  B01J20/28069 ,  B01J20/28083 ,  B01J20/28085 ,  B01J20/28092 ,  C07C7/13 ,  C07C15/067

    摘要： Adsorbent compositions for vapor-phase adsorption processes, which are selective for para-xylene. Such compositions can be used in gas-phase adsorption processes for the separation of para-xylene or the separation of para-xylene and ethylbenzene from mixed xylenes or a C8 aromatic mixture, respectively. The adsorbent compositions generally comprise materials of a molecular sieve material and a binder, wherein the adsorbent composition has a macropore volume of at least about 0.20 cc/g and a mesopore volume of less than about 0.20 cc/g.

    摘要翻译： 用于气相吸附方法的吸附剂组合物，其对对二甲苯是选择性的。 这种组合物可以用于分离对二甲苯的气相吸附方法或分别从混合二甲苯或C 8 C 8芳族混合物中分离对二甲苯和乙苯。 吸附剂组合物通常包括分子筛材料和粘合剂的材料，其中吸附剂组合物具有至少约0.20cc / g的大孔体积和小于约0.20cc / g的中孔体积。