Method for preparing analytical standard, and analytical standard prepared by the same
    10.
    发明申请
    Method for preparing analytical standard, and analytical standard prepared by the same 失效
    制备分析标准的方法及其制备的分析标准

    公开(公告)号:US20090001323A1

    公开(公告)日:2009-01-01

    申请号:US11905605

    申请日:2007-10-02

    IPC分类号: G01N37/00

    摘要: There is provided a method for preparing an analytical standard used for microbeam X-ray fluorescence analysis which includes: a mixing step A in which an element is added to a base material, and the base material and the element are mixed by stirring to obtain a mixed solution; a deaeration step B in which the mixed solution is deaerated; a freeze step D in which the mixed solution is slowly frozen; and a cutting step F in which a thin section is cut out from the frozen mixed solution. In order to surely remove bubbles from the mixed solution, the deaeration step B may contain a stationary step in which the mixed solution is allowed to stand still at room temperature; or the stationary step includes a removal step in which gas contained in the mixed solution which is allowed to stand still is removed with a suction apparatus.

    摘要翻译: 提供了一种制备用于微束X射线荧光分析的分析标准的方法,其包括:混合步骤A,其中将元素添加到基材中,并且通过搅拌将基材和元素混合以获得 混合溶液; 脱气工序B,其中混合溶液脱气; 冷冻步骤D,其中混合溶液缓慢冷冻; 以及切割步骤F,其中从冷冻混合溶液中切出薄片。 为了从混合溶液中确定地除去气泡,脱气工序B可以含有使混合溶液在室温下静置的固定步骤; 或者固定步骤包括除去步骤,其中使用抽吸装置除去容纳在静止的混合溶液中的气体。