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    Process for the continuous preparation of 3-halopropylorganosilanes
    1.
    发明授权
    Process for the continuous preparation of 3-halopropylorganosilanes 失效
    连续制备3-卤代丙基有机硅烷的方法

    公开(公告)号：US06242630B1

    公开(公告)日：2001-06-05

    申请号：US08908095

    申请日：1997-08-11

    申请人： Stefan Bade ,  Uwe Schoen ,  John Burkhard ,  Franz-Michael Bollenrath ,  Norbert Hofmann ,  Hermann-Josef Korte ,  Hartwig Rauleder ,  Uwe Tanger

    发明人： Stefan Bade ,  Uwe Schoen ,  John Burkhard ,  Franz-Michael Bollenrath ,  Norbert Hofmann ,  Hermann-Josef Korte ,  Hartwig Rauleder ,  Uwe Tanger

    IPC分类号： C07F708

    CPC分类号： C07F7/14 ,  C07F7/0829 ,  C07F7/1876

    摘要： A process for the continuous preparation of 3-halopropylorganosilanes of the general structure RbH3-a-bXaSiCH2CH2CH2Y  (III), where: R is CH3, C2H5, C3H7, OCH3, OC2H5 or OC3H7, X is F, Cl, Br or I, Y is F, Cl, Br or I, and a and b are each one of the numbers 0, 1, 2 or 3 and the sum a+b is 1, 2 or 3, comprising reacting, as starting materials, an allyl halide with a silane carrying at least one H atom, wherein the starting materials are present in stoichiometric amounts or one of the starting materials is present in substoichiometric amounts, wherein the reaction carried out is a partial reaction of from 10% to 80%, on a molar basis, of the starting materials, based on either material, when both are present in stoichiometric amounts, or based on the substoichiometric material.

    摘要翻译： 连续制备通常结构的3-卤代丙基有机硅烷的方法，其中R为CH 3，C 2 H 5，C 3 H 7，OCH 3，OC 2 H 5或OC 3 H 7，X为F，Cl，Br或I，Y为F，Cl，Br或I， 和b分别为数字0,1,2或3中的一个，并且和a + b为1,2或3，包括使烯丙基卤化物与携带至少一个H原子的硅烷作为原料，其中， 原料以化学计量的量存在，或者一种起始原料以亚化学计量的量存在，其中进行的反应是基于摩尔的10％至80％的起始原料的部分反应，基于任一材料 ，当两者都以化学计量的量存在时，或基于亚化学计量的材料。

    Process for preparing vinylchlorosilanes
    2.
    发明授权
    Process for preparing vinylchlorosilanes 有权
    制备乙烯基氯硅烷的方法

    公开(公告)号：US06222056B1

    公开(公告)日：2001-04-24

    申请号：US09556404

    申请日：2000-04-24

    申请人： Stefan Bade ,  Hartwig Rauleder ,  Uwe Schoen ,  Franz-Michael Bollenrath

    发明人： Stefan Bade ,  Hartwig Rauleder ,  Uwe Schoen ,  Franz-Michael Bollenrath

    IPC分类号： C07F714

    CPC分类号： C07F7/122

    摘要： The invention relates to a process for preparing vinylchlorosilanes by thermal non-catalyzed reaction of chlorosilanes with vinyl chloride at from 550 to 700° C., using a ring-gap reactor which includes rapidly cooling the hot reaction gases after they have flowed through the ring-gap space, by quenching them with a liquid.

    摘要翻译： 本发明涉及一种通过氯代硅烷与氯乙烯在550-700℃下的热非催化反应制备乙烯基氯硅烷的方法，该方法包括一个环流反应器，该反应器包括在热反应气体流过环后快速冷却 间隙，用液体淬火。

    Process for preparing vinyl chlorosilanes
    3.
    发明授权
    Process for preparing vinyl chlorosilanes 有权
    制备乙烯基氯硅烷的方法

    公开(公告)号：US06291698B1

    公开(公告)日：2001-09-18

    申请号：US09556403

    申请日：2000-04-24

    申请人： Stefan Bade ,  Bernt Kesper ,  Robert Koell ,  Hartwig Rauleder ,  Uwe Schoen

    发明人： Stefan Bade ,  Bernt Kesper ,  Robert Koell ,  Hartwig Rauleder ,  Uwe Schoen

    IPC分类号： C07F708

    CPC分类号： C07F7/122

    摘要： The invention relates to a process for preparing vinyl chlorosilanes, that includes thermally and non-catalytically reacting chlorosilane with vinyl chloride at a temperature of 550 to 700° C. by flowing the chlorosilane and vinyl chloride through a ring-gap space in a ring-gap reactor to produce a reaction gas; the ring-gap space having a cross-sectional area and a volume; and, after the flowing, further reacting, adiabatically, the reaction gas in a second zone to produce a hot reaction gas that contains vinylchiorosilane; wherein the second zone has a cross-sectional area that is greater than the cross-sectional area of the ring-gap space; and wherein the second zone has a volume that is in a ratio to the volume of the ring-gap space of 0.15:1 to 1.5:1. The invention also provides an apparatus for carrying out the above process.

    摘要翻译： 本发明涉及一种制备乙烯基氯硅烷的方法，其包括在550-700℃的温度下使氯代硅烷与氯乙烯进行热和非催化反应，通过使氯代硅烷和氯乙烯通过环 - 间隙反应器产生反应气体; 所述环间隙具有横截面积和体积; 并且在流动之后，绝热地将第二区中的反应气体进行反应，以产生含有乙烯基氯硅烷的热反应气体; 其中所述第二区域具有大于所述环形间隙的横截面面积的横截面面积; 并且其中所述第二区域具有与所述环隙空间的体积的比率为0.15:1至1.5:1的体积。 本发明还提供一种用于执行上述过程的装置。

    Process for preparing epoxysilanes
    4.
    发明授权
    Process for preparing epoxysilanes 有权
    制备环氧硅烷的方法

    公开(公告)号：US06402961B1

    公开(公告)日：2002-06-11

    申请号：US09621076

    申请日：2000-07-21

    申请人： Stefan Bade ,  Uwe Schoen ,  Hartwig Rauleder

    发明人： Stefan Bade ,  Uwe Schoen ,  Hartwig Rauleder

    IPC分类号： B01D1508

    CPC分类号： C07F7/1892

    摘要： A process for preparing epoxysilanes by reacting a hydrogensilane with an allyl glycidyl ether in the presence of a catalyst and working up the crude product obtained, where the catalyst is removed from the crude product and the crude product is subsequently distilled.

    摘要翻译： 一种通过在催化剂存在下使氢硅烷与烯丙基缩水甘油醚反应来制备环氧硅烷的方法，并处理所得到的粗产物，其中从粗产物中除去催化剂和粗产物。

    Process for preparing 3-glycidyloxypropyltrialkoxysilanes
    5.
    发明授权
    Process for preparing 3-glycidyloxypropyltrialkoxysilanes 有权
    制备3-缩水甘油氧基丙基三烷氧基硅烷的方法

    公开(公告)号：US6100408A

    公开(公告)日：2000-08-08

    申请号：US246953

    申请日：1999-02-09

    申请人： Jaroslaw Monkiewicz ,  Stefan Bade ,  Uwe Schoen

    发明人： Jaroslaw Monkiewicz ,  Stefan Bade ,  Uwe Schoen

    IPC分类号： B01J23/42 ,  B01J35/10 ,  C07B61/00 ,  C07F7/18 ,  C07F7/08 ,  C07D303/02

    CPC分类号： C07F7/1876

    摘要： The invention relates to a process for preparing 3-glycidyloxypropyltrialkoxysilanes of the general formulaCH.sub.2 (O)CHCH.sub.2 --O--(CH.sub.2).sub.3 Si(OR).sub.3 (I),in which R is an alkyl radical, by reacting allyl glycidyl etherCH.sub.2 (O)CHCH.sub.2 --O--CH.sub.2 CH.dbd.CH.sub.2 (II),with a trialkoxysilane of the general formulaHSi(OR).sub.3 (III),in which R is again an alkyl radical, in a heterogeneous, platinum-catalyzed hydrosilylation reaction, where the catalyst employed is a platinum(0) catalyst on a nonmetallic support.

    摘要翻译： 本发明涉及一种制备通式CH 2（O）CHCH 2 -O-（CH 2）3 Si（OR）3（I）的3-缩水甘油氧基丙基三烷氧基硅烷的方法，其中R是烷基，烯丙基缩水甘油醚CH2（ O）CHCH 2 -O-CH 2 CH = CH 2（II）与通式为HSi（OR）3（III）的三烷氧基硅烷，其中R再次为烷基，在异质铂催化的氢化硅烷化反应中，其中 所使用的催化剂是在非金属载体上的铂（0）催化剂。

    CRYOGENIC STORAGE DEVICE
    6.
    发明申请
    CRYOGENIC STORAGE DEVICE 有权
    低温储存装置

    公开(公告)号：US20110219788A1

    公开(公告)日：2011-09-15

    申请号：US13129870

    申请日：2009-11-09

    申请人： Heiko Zimmermann ,  Uwe Schoen ,  Guenter R. Fuhr ,  Dirk Leuthold ,  Marianne Belke

    发明人： Heiko Zimmermann ,  Uwe Schoen ,  Guenter R. Fuhr ,  Dirk Leuthold ,  Marianne Belke

    IPC分类号： F25D13/06 ,  F25B49/00

    CPC分类号： A01N1/0252 ,  F25B2700/04 ,  F25D3/102 ,  F25D3/11 ,  F25D29/001 ,  F25D2600/02 ,  F25D2700/12 ,  F25D2700/16 ,  G01N1/42 ,  G01N2035/00435

    摘要： The invention relates to a cryogenic storage device and to a method for operating a cryogenic storage device, particularly for cryogenic storage of biological samples, comprising a sample carrying device that is set up to accommodate samples, a cryogenic container that is set up to accommodate the sample carrying device, a container cooling device with which the cryogenic container can be cooled, an intermediate storage container that is set up for intermediate storage of the sample carrying device, a transport device with which the sample carrying device can be moved between the cryogenic container and the intermediate storage container and a sensor device with which at least one operating parameter of the cryogenic storage device can be registered. The transport device is set up to be activated in dependence on an output signal from the sensor device upon registering a predetermined operating condition of the cryogenic storage device, so that the sample carrying device is moved from the cryogenic container to the intermediate storage container. Additionally or alternatively, an intermediate storage cooling device that is set up for cooling the intermediate storage container can be activated in dependence on an output signal of the sensor device.

    摘要翻译： 本发明涉及一种低温存储装置和一种用于操作低温存储装置的方法，特别是用于生物样品的低温储存的方法，包括设置用于容纳样品的样品携带装置，设置为容纳 样品运送装置，用于冷冻低温容器的容器冷却装置，设置用于样品运送装置的中间储存的中间储存容器，运送装置，使样品运送装置能够在低温容器 以及可以登记低温储存装置的至少一个操作参数的中间储存容器和传感器装置。 传送装置被设置为在登记低温存储装置的预定操作条件时依赖于来自传感器装置的输出信号被激活，使得样品携带装置从低温容器移动到中间储存容器。 另外或替代地，可以根据传感器装置的输出信号激活设置用于冷却中间存储容器的中间存储冷却装置。

    Cryogenic storage device
    9.
    发明授权
    Cryogenic storage device 有权
    低温储存装置

    公开(公告)号：US08925334B2

    公开(公告)日：2015-01-06

    申请号：US13129870

    申请日：2009-11-09

    申请人： Heiko Zimmermann ,  Uwe Schoen ,  Guenter R. Fuhr ,  Dirk Leuthold ,  Marianne Belke

    发明人： Heiko Zimmermann ,  Uwe Schoen ,  Guenter R. Fuhr ,  Dirk Leuthold ,  Marianne Belke

    IPC分类号： F25D13/06 ,  F17C3/10 ,  F25D25/00 ,  F25D11/00 ,  A01N1/02 ,  G01N1/42 ,  G01N35/00

    CPC分类号： A01N1/0252 ,  F25B2700/04 ,  F25D3/102 ,  F25D3/11 ,  F25D29/001 ,  F25D2600/02 ,  F25D2700/12 ,  F25D2700/16 ,  G01N1/42 ,  G01N2035/00435

    摘要： The invention relates to a cryogenic storage device and to a method for operating a cryogenic storage device, particularly for cryogenic storage of biological samples, comprising a sample carrying device that is set up to accommodate samples, a cryogenic container that is set up to accommodate the sample carrying device, a container cooling device with which the cryogenic container can be cooled, an intermediate storage container that is set up for intermediate storage of the sample carrying device, a transport device with which the sample carrying device can be moved between the cryogenic container and the intermediate storage container and a sensor device with which at least one operating parameter of the cryogenic storage device can be registered. The transport device is set up to be activated in dependence on an output signal from the sensor device upon registering a predetermined operating condition of the cryogenic storage device, so that the sample carrying device is moved from the cryogenic container to the intermediate storage container. Additionally or alternatively, an intermediate storage cooling device that is set up for cooling the intermediate storage container can be activated in dependence on an output signal of the sensor device.

    摘要翻译： 本发明涉及一种低温存储装置和一种用于操作低温存储装置的方法，特别是用于生物样品的低温储存的方法，包括设置用于容纳样品的样品携带装置，设置为容纳 样品运送装置，用于冷冻低温容器的容器冷却装置，设置用于样品运送装置的中间储存的中间储存容器，运送装置，使样品运送装置能够在低温容器 以及可以登记低温储存装置的至少一个操作参数的中间储存容器和传感器装置。 传送装置被设置为在登记低温存储装置的预定操作条件时依赖于来自传感器装置的输出信号被激活，使得样品携带装置从低温容器移动到中间储存容器。 另外或替代地，可以根据传感器装置的输出信号激活设置用于冷却中间存储容器的中间存储冷却装置。