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公开(公告)号：US20070282135A1
公开(公告)日：2007-12-06
申请号：US11447020
申请日：2006-06-06
申请人： Steffen Maas , Thorsten Johann , Michael Koch , Tilman Sirch , Stephan Schlitter , Stefan Rittinger , Michael Steiniger , Todd C. Spengeman
发明人： Steffen Maas , Thorsten Johann , Michael Koch , Tilman Sirch , Stephan Schlitter , Stefan Rittinger , Michael Steiniger , Todd C. Spengeman
IPC分类号： C07C45/62
CPC分类号： C07C29/141 , C07C31/20
摘要： Process for the catalytic hydrogenation of methylolalkanals of the general formula where R1 and R2 are each, independently of one another, a further methylol group or an alkyl group having from 1 to 22 carbon atoms or an aryl or aralkyl group having from 6 to 33 carbon atoms, in the liquid phase by means of hydrogen over a hydrogenation catalyst, wherein hydrogen is used in a molar ratio to methylolalkanal of greater than 1.
摘要翻译： 用于通式的羟甲基烷烃的催化氢化方法其中R 1和R 2各自彼此独立地是另外的羟甲基或具有1个 至22个碳原子或具有6至33个碳原子的芳基或芳烷基，在液相中通过氢气在氢化催化剂上氢化，其中氢以与羟甲基烷醛的摩尔比大于1。
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公开(公告)号：US07388116B2
公开(公告)日：2008-06-17
申请号：US11447020
申请日：2006-06-06
申请人： Steffen Maas , Thorsten Johann , Michael Koch , Tilman Sirch , Stephan Schlitter , Stefan Rittinger , Michael Steiniger , Todd C Spengeman
发明人： Steffen Maas , Thorsten Johann , Michael Koch , Tilman Sirch , Stephan Schlitter , Stefan Rittinger , Michael Steiniger , Todd C Spengeman
IPC分类号： C07C27/04
CPC分类号： C07C29/141 , C07C31/20
摘要： Process for the catalytic hydrogenation of methylolalkanals of the general formula where R1 and R2 are each, independently of one another, a further methylol group or an alkyl group having from 1 to 22 carbon atoms or an aryl or aralkyl group having from 6 to 33 carbon atoms, in the liquid phase by means of hydrogen over a hydrogenation catalyst, wherein hydrogen is used in a molar ratio to methylolalkanal of greater than 1.
摘要翻译： 用于通式的羟甲基烷烃的催化氢化方法其中R 1和R 2各自彼此独立地是另外的羟甲基或具有1个 至22个碳原子或具有6至33个碳原子的芳基或芳烷基，在液相中通过氢气在氢化催化剂上氢化，其中氢以与羟甲基烷醛的摩尔比大于1。
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公开(公告)号：US20090069604A1
公开(公告)日：2009-03-12
申请号：US12279792
申请日：2007-02-23
申请人： Steffen Maas , Thorsten Johann , Michael Koch , Tilman Sirch , Stephan Schlitter , Stefan Rittinger , Michael Steiniger
发明人： Steffen Maas , Thorsten Johann , Michael Koch , Tilman Sirch , Stephan Schlitter , Stefan Rittinger , Michael Steiniger
IPC分类号： C07C45/62
CPC分类号： C07C29/141 , C07C31/20 , C07C31/22 , C07C31/245
摘要： A process for catalytically hydrogenating methylolalkanals of the general formula in which R1 and R2 are each independently a further methylol group or an alkyl group having from 1 to 22 carbon atoms or an aryl or aralkyl group having from 6 to 33 carbon atoms, in the liquid phase over a hydrogenation catalyst, which comprises setting a pH of from 7.0 to 9.0 in the hydrogenation effluent by adding at least one tertiary amine, an inorganic base or an inorganic or organic acid to the hydrogenation feed.
摘要翻译： 一种催化氢化通式的羟甲基烷烃的方法，其中R 1和R 2各自独立地为在另外的羟甲基或具有1至22个碳原子的烷基或具有6至33个碳原子的芳基或芳烷基，在液体 其包括通过向氢化进料中加入至少一种叔胺，无机碱或无机或有机酸将氢化流出物中的pH设定为7.0至9.0来进行。
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4.发明授权Method for the continuous production of an amine using an aluminum—copper catalyst 有权使用铝 - 铜催化剂连续生产胺的方法公开(公告)号：US09174201B2
公开(公告)日：2015-11-03
申请号：US13119948
申请日：2009-09-09
申请人： Martin Ernst , Bernd Stein , Steffen Maas , Jörg Pastre , Thorsten Johann , Johann-Peter Melder
发明人： Martin Ernst , Bernd Stein , Steffen Maas , Jörg Pastre , Thorsten Johann , Johann-Peter Melder
IPC分类号： C07C211/14 , C07C211/35 , C07C209/26 , B01J23/72 , B01J35/02 , B01J37/00 , C07C209/16 , B01J21/04 , B01J37/02 , B01J37/18
CPC分类号： B01J23/72 , B01J21/04 , B01J35/023 , B01J37/0009 , B01J37/0201 , B01J37/18 , C07C209/16 , C07C209/26 , C07C2601/14 , Y02P20/582 , C07C211/08 , C07C211/10 , C07C211/12 , C07C211/14 , C07C211/35
摘要： Process for the continuous preparation of an amine by reaction of a primary or secondary alcohol, aldehyde and/or ketone with hydrogen and a nitrogen compound selected from the group consisting of ammonia, primary and secondary amines at a temperature in the range from 60 to 300° C. in the presence of a catalyst comprising copper oxide and aluminum oxide, wherein the reaction takes place in the gas phase and the catalytically active composition of the catalyst before reduction with hydrogen comprisesfrom 20 to 75% by weight of aluminum oxide (Al2O3),from 20 to 75% by weight of oxygen-comprising compounds of copper, calculated as CuO,from 0 to 2% by weight of oxygen-comprising compounds of sodium, calculated as Na2O, andless than 5% by weight of oxygen-comprising compounds of nickel, calculated as NiO, and the shaped catalyst body has a pellet shape having a diameter in the range from 1 to 4 mm and a height in the range from 1 to 4 mm.
摘要翻译： 通过伯醇或仲醇，醛和/或酮与氢和选自氨，伯胺和仲胺的氮化合物在60至300℃的温度下反应连续制备胺的方法 在包含氧化铜和氧化铝的催化剂存在下，其中反应在气相中进行，催化剂在用氢还原前的催化活性组合物包含20至75重量％的氧化铝（Al 2 O 3 ），20至75重量％的以氧化铜计的含氧化合物的铜（以CuO计）为0至2重量％的含氧化合物的钠（以Na 2 O计）和小于5重量％ 包括以NiO计算的镍化合物，并且成型催化剂体具有直径在1至4mm范围内且高度在1至4mm范围内的颗粒形状。
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5.发明申请METHOD FOR THE CONTINUOUS PRODUCTION OF AN AMINE USING AN ALUMINUM-COPPER CATALYST 有权使用铝 - 铜催化剂连续生产胺的方法公开(公告)号：US20110172430A1
公开(公告)日：2011-07-14
申请号：US13119948
申请日：2009-09-09
申请人： Martin Ernst , Bernd Stein , Steffen Maas , Jörg Pastre , Thorsten Johann , Johann-Peter Melder
发明人： Martin Ernst , Bernd Stein , Steffen Maas , Jörg Pastre , Thorsten Johann , Johann-Peter Melder
IPC分类号： C07D211/00 , C07C209/00 , C07D207/06
CPC分类号： B01J23/72 , B01J21/04 , B01J35/023 , B01J37/0009 , B01J37/0201 , B01J37/18 , C07C209/16 , C07C209/26 , C07C2601/14 , Y02P20/582 , C07C211/08 , C07C211/10 , C07C211/12 , C07C211/14 , C07C211/35
摘要： Process for the continuous preparation of an amine by reaction of a primary or secondary alcohol, aldehyde and/or ketone with hydrogen and a nitrogen compound selected from the group consisting of ammonia, primary and secondary amines at a temperature in the range from 60 to 300° C. in the presence of a catalyst comprising copper oxide and aluminum oxide, wherein the reaction takes place in the gas phase and the catalytically active composition of the catalyst before reduction with hydrogen comprises PS from 20 to 75% by weight of aluminum oxide (Al2O3),from 20 to 75% by weight of oxygen-comprising compounds of copper, calculated as CuO, from 0 to 2% by weight of oxygen-comprising compounds of sodium, calculated as Na2O, and less than 5% by weight of oxygen-comprising compounds of nickel, calculated as NiO, and the shaped catalyst body has a pellet shape having a diameter in the range from 1 to 4 mm and a height in the range from 1 to 4 mm.
摘要翻译： 通过伯醇或仲醇，醛和/或酮与氢和选自氨，伯胺和仲胺的氮化合物在60至300℃的温度下反应来连续制备胺的方法 在包含氧化铜和氧化铝的催化剂存在下，其中反应在气相中进行，并且在用氢还原之前催化活性组合物包含20至75重量％的氧化铝（PS） Al 2 O 3），20至75重量％的含氧化合物的铜（以CuO计），0至2重量％的含氧化合物的钠（以Na 2 O计）和小于5重量％的氧 令人惊奇的以NiO计算的镍化合物，成型的催化剂体具有直径在1至4mm范围内且高度在1至4mm范围内的颗粒形状。
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6.发明授权Use of a supported catalyst containing precious metal for oxidative dehydrogenation 有权使用含贵金属的载体催化剂进行氧化脱氢公开(公告)号：US08779212B2
公开(公告)日：2014-07-15
申请号：US12933441
申请日：2009-03-16
CPC分类号： B01J31/1616 , B01J21/16 , B01J23/007 , B01J23/38 , B01J23/50 , B01J23/72 , B01J23/8926 , B01J37/0219 , B01J37/086 , B01J2231/763 , B01J2531/17 , C07C45/38 , C07C47/21
摘要： The use of a supported noble metal catalyst obtainable by applying a sparingly soluble noble metal compound to a support from solution or suspension, and subsequently treating thermally, for preparing olefinically unsaturated carbonyl compounds.
摘要翻译： 使用负载的贵金属催化剂，其通过将溶于或悬浮液的微溶贵金属化合物施加到载体上，随后热处理，制备烯属不饱和羰基化合物。
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公开(公告)号：US08563785B2
公开(公告)日：2013-10-22
申请号：US13608577
申请日：2012-09-10
申请人： Michael Limbach , Joaquim Henrique Teles , Radwan Abdallah , Torsten Mäurer , Thorsten Johann , Manuel Danz
发明人： Michael Limbach , Joaquim Henrique Teles , Radwan Abdallah , Torsten Mäurer , Thorsten Johann , Manuel Danz
IPC分类号： C07C29/56
摘要： A process for isomerizing olefinically unsaturated alcohols over supported noble metal catalysts with a support based on carbon in an oxygenous atmosphere.
摘要翻译： 在含氧气氛中具有基于碳的载体的负载型贵金属催化剂上异构化烯属不饱和醇的方法。
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公开(公告)号：US20130006021A1
公开(公告)日：2013-01-03
申请号：US13608577
申请日：2012-09-10
申请人： Michael Limbach , Joaquim Henrique Teles , Radwan Abdallah , Torsten Mäurer , Thorsten Johann , Manuel Danz
发明人： Michael Limbach , Joaquim Henrique Teles , Radwan Abdallah , Torsten Mäurer , Thorsten Johann , Manuel Danz
IPC分类号： C07C29/56
摘要： A process for isomerizing olefinically unsaturated alcohols over supported noble metal catalysts with a support based on carbon in an oxygenous atmosphere.
摘要翻译： 在含氧气氛中具有基于碳的载体的负载型贵金属催化剂上异构化烯属不饱和醇的方法。
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公开(公告)号：US08263813B2
公开(公告)日：2012-09-11
申请号：US12920150
申请日：2009-02-27
申请人： Michael Limbach , Joaquim Henrique Teles , Radwan Abdallah , Torsten Mäurer , Thorsten Johann , Manuel Danz
发明人： Michael Limbach , Joaquim Henrique Teles , Radwan Abdallah , Torsten Mäurer , Thorsten Johann , Manuel Danz
摘要： A process for isomerizing olefinically unsaturated alcohols over supported noble metal catalysts with a support based on carbon in an oxygenous atmosphere.
摘要翻译： 在含氧气氛中具有基于碳的载体的负载型贵金属催化剂上异构化烯属不饱和醇的方法。
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10.发明授权公开(公告)号：US07495132B2
公开(公告)日：2009-02-24
申请号：US10587191
申请日：2005-01-28
申请人： Christian Walsdorff , Thorsten Johann , Beatrice Roessler , Hartmut Hibst , Joaquim Henrique Teles , Sebastian Storck , Jens Klein
发明人： Christian Walsdorff , Thorsten Johann , Beatrice Roessler , Hartmut Hibst , Joaquim Henrique Teles , Sebastian Storck , Jens Klein
CPC分类号： C07C45/65 , B01J23/6445 , B01J23/6447 , B01J23/6522 , B01J23/681 , B01J23/8973 , B01J35/008 , B01J37/0201 , B01J37/0221 , B01J37/03 , C07C47/21 , C07C49/603
摘要： The present invention relates to a catalytically active composition comprising as active component Pd and Bi and at least one element selected from the group (a) consisting of Rh, Au, Sb, V, Cr, W, Mn, Fe, Co, Ni, Na, Cs and Ba, or Pd, Rh and Bi and optionally an element selected from the group (a′) consisting of Au, Sb, V, Cr, W, Mn, Fe, Co, Ni, Pt, Cu, Ag, Na, Cs, Mg, Ca and Ba. The present invention further provides a process for dehydrogenating hydrocarbons, preferably oxo-functionalized hydrocarbons such as cyclopentanone, cyclohexanone and isovaleraldehyde, using the catalytically active composition.
摘要翻译： 本发明涉及包含作为活性成分Pd和Bi的至少一种元素的催化活性组合物和选自由Rh，Au，Sb，V，Cr，W，Mn，Fe，Co，Ni组成的组（a）中的至少一种元素， Na，Cs和Ba或Pd，Rh和Bi以及任选的选自Au，Sb，V，Cr，W，Mn，Fe，Co，Ni，Pt，Cu，Ag， Na，Cs，Mg，Ca和Ba。 本发明还提供了一种使用催化活性组合物使烃优选氧化官能化烃如环戊酮，环己酮和异戊醛脱氢的方法。
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