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    Rigid polyurethane foam
    2.
    发明授权
    Rigid polyurethane foam 有权

    公开(公告)号：US09683071B2

    公开(公告)日：2017-06-20

    申请号：US14136278

    申请日：2013-12-20

    申请人： BASF SE

    发明人： Michael L. Jackson

    IPC分类号： C08G18/66 ,  C08J9/14 ,  C08G18/42 ,  C08G101/00

    CPC分类号： C08G18/6637 ,  C08G18/4236 ,  C08G18/6622 ,  C08G2101/0025 ,  C08J9/141 ,  C08J2203/14 ,  C08J2205/10 ,  C08J2375/04

    摘要： A rigid polyurethane foam includes the reaction product of an isocyanate and an isocyanate reactive component in the presence of a blowing agent. The isocyanate reactive component includes an aromatic polyester polyol, a rigid polyol, and an aliphatic polyester polyol. The rigid polyurethane foam has a tensile adhesion of greater than 35 kPa (5 psi) when disposed on a metal substrate or a polyester, polyurethane, or epoxy coated metal substrate, each having a substrate temperature of greater than 41° C. (105° F.), and tested in accordance with ASTM D1623-09. A method of forming a composite article comprising a substrate and the rigid polyurethane foam includes the steps of combining the isocyanate reactive component and the isocyanate in the presence of the blowing agent to form a reaction mixture and applying the reaction mixture to the substrate having a substrate temperature of greater than 41° C. (105° F.) to form the composite article.

    Microcellular polyurethane elastomer and manufacturing method of the same
    3.
    发明授权
    Microcellular polyurethane elastomer and manufacturing method of the same 失效
    微孔聚氨酯弹性体及其制造方法相同

    公开(公告)号：US4647596A

    公开(公告)日：1987-03-03

    申请号：US856217

    申请日：1986-04-28

    申请人： Seiji Ishii ,  Masanori Miyoshi ,  Takumi Ishiwaka ,  Osamu Kondo

    发明人： Seiji Ishii ,  Masanori Miyoshi ,  Takumi Ishiwaka ,  Osamu Kondo

    IPC分类号： C08G18/00 ,  C08G18/40 ,  C08G18/42 ,  C08G18/66 ,  C08G18/14

    CPC分类号： C08G18/4277 ,  C08G18/4202 ,  C08G18/6637 ,  C08G2101/0066 ,  C08G2350/00 ,  Y10S521/904

    摘要： Polyol component essentially consists of polyesterpolyetherpolyol containing polyesterpolyol by the weight ratio of 100:0 to 20:80, in which the polyesterpolyetherpolyol is a copolymer of polytetramethyleneglycol (PTMG) and .epsilon.-caprolactone by the weight ratio of 20:80 to 80:20 with an average molecular weight of 1000 to 3000 and the polyesterpolyol is a condensate of adipic acid as a main acid component with an average molecular weight of 1000 to 3000, is reacted with isocyanate component essentially consists of 4,4'-diphenylmethanediisocyanate (MDI) to make a prepolymer with terminal radical of NCO.Microcellular polyurethane produced from the prepolymer by foaming and polymerization reaction has the durability for vibration-proof material of car use, combining the advantage of PTMG such as high initial modulus at elongation, low heat built up, low-temperature property and hydrolysis-durability under high humid and hot conditions, with the advantage of polycaprolactone such as good molding property and anti-bending-fatigue property, as well as making up for the disadvantage of both polyols each other. Thus improving the problems of microcellular polyurethane using MDI such as low initial modulus at elongation and high heat built up.

    摘要翻译： 多元醇组分主要由聚酯多元醇多元醇组成，重量比为100:0至20:80，其中聚酯多元醇是聚四亚甲基二醇（PTMG）与ε-己内酯的共聚物，重量比为20:80至80:20， 平均分子量为1000〜3000，聚酯多元醇是己二酸作为主要酸成分的平均分子量为1000〜3000的缩合物，与异氰酸酯成分基本上由4,4'-二苯基甲烷二异氰酸酯（MDI）组成， 制备具有NCO末端基团的预聚物。 通过发泡和聚合反应由预聚物生产的微孔聚氨酯具有耐汽车使用的防振材料的耐久性，结合PTMG的优点，如伸长时的高初始模量，低热累积，低温性能和水解耐久性 高湿热条件下，具有良好的成型性和抗弯曲疲劳性等聚己内酯的优点，并且弥补了这两种多元醇的缺点。 从而改善了使用MDI的微孔聚氨酯的问题，如伸长时的低初始模量和高热积聚。

    Rigid urethane foams
    9.
    发明申请
    Rigid urethane foams 审中-公开
    刚性聚氨酯泡沫

    公开(公告)号：US20040157945A1

    公开(公告)日：2004-08-12

    申请号：US10741467

    申请日：2003-12-19

    发明人： Thomas Allan Barber

    IPC分类号： C08G018/00

    CPC分类号： C08G18/4208 ,  C08G18/3218 ,  C08G18/6484 ,  C08G18/6637 ,  C08G2101/0025 ,  C08G2101/005 ,  C08G2101/0083

    摘要： Rigid urethane foams made from polyester polyols and processes for producing them are provided. The foams are made by reacting a mixture that comprises an aromatic polyester polyol having an average functionality of about 3.0 or less, a hydroxyl number above 100 mg/KOH/g, and an average molecular weight less than 3000; from about 1 weight percent to about 30 weight percent of a saccharide; a blowing agent; and an isocyanate, and said foams having an isocyanate index from about 0.8 to about 3.0. The foams have a high closed cell content and a high free rise compressive strength and slightly lower thermal resistance than expected for their density.

    摘要翻译： 提供由聚酯多元醇制成的刚性聚氨酯泡沫及其制备方法。 泡沫体通过使包含平均官能度为约3.0或更低，羟基数高于100mg / KOH / g，平均分子量小于3000的芳族聚酯多元醇的混合物反应制备; 约1重量％至约30重量％的糖; 发泡剂; 和异氰酸酯，并且所述泡沫具有约0.8至约3.0的异氰酸酯指数。 泡沫具有高的闭孔含量和高的自由上升抗压强度，并且比其预期的密度略低的热阻。

    Materials suitable as crosslinkable binder components
    10.
    发明授权
    Materials suitable as crosslinkable binder components 失效
    适合作为可交联粘合剂组分的材料

    公开(公告)号：US5922469A

    公开(公告)日：1999-07-13

    申请号：US839703

    申请日：1997-04-15

    申请人： Thomas Wunsch ,  Gregor Brodt ,  Ria Kress ,  Norbert Schneider ,  Albert Kohl ,  August Lehner ,  Werner Balz

    发明人： Thomas Wunsch ,  Gregor Brodt ,  Ria Kress ,  Norbert Schneider ,  Albert Kohl ,  August Lehner ,  Werner Balz

    IPC分类号： C08G18/12 ,  C08G18/61 ,  C08G18/65 ,  C08G18/66 ,  C09D5/23 ,  C09D175/00 ,  C09D175/04 ,  G11B5/702 ,  B32B27/40

    CPC分类号： G11B5/7021 ,  C08G18/12 ,  C08G18/61 ,  C08G18/6517 ,  C08G18/6535 ,  C08G18/6637 ,  Y10S428/90 ,  Y10T428/31609

    摘要： Preparation of materials (I) having an average molecular weight from 4000 to 30,000, obtainable by reacting1) a polyurethane (II) comprisinga) 1 mol of a diol (III) having an average molecular weight of from 400 to 4000,b) from 0.3 to 9 mol of an aliphatic or cycloaliphatic diol (IV) of 2 to 18 carbon atoms,c) from 0.3 to 9 mol of an aromatic diol (V) of 8 to 30 carbon atoms,d) from 0.01 to 1 mol of a trihydric alcohol (VI) of 3 to 18 carbon atoms,e) from 0.001 to 1 mol of a polyhydric alcohol (VII) of 3 to 14 carbon atoms which contains a tertiary amino group andf) an amount of a diisocyanate (VIII) of 6 to 30 carbon atoms such that the molar ratio of the isocyanate groups to the total number of hydroxyl groups in (III) to (VII) is from 1.05:1 to 1.4:1with2) a compound (IX) which contains one or more hydroxyl groups and one or more amino groups reactive toward isocyanate groups, the amount of (IX) being such that the number of reactive amino groups corresponds to the number of isocyanate groups in the polyurethane (II).The materials may be used as crosslinkable binder components for pigment-containing coatings, in particular for the production of magnetic recording materials.

    摘要翻译： 制备平均分子量为4000〜30,000的材料（I），其可通过使1）包含a）1摩尔平均分子量为400至4000的二醇（III）的聚氨酯（II）得到，b） 2〜18个碳原子的脂肪族或脂环族二醇（Ⅳ）为0.3〜9摩尔，c）0.3〜9摩尔碳原子数为8〜30的芳香族二醇（Ⅴ），d）0.01〜1摩尔 3〜18个碳原子的三元醇（Ⅵ），e）0.001〜1摩尔含有叔氨基的3〜14个碳原子的多元醇（Ⅶ），f）二异氰酸酯（Ⅷ） （III）至（VII）中的异氰酸酯基团与羟基的总摩尔比为1.05:1至1.4:1，其中2）含有一个或多个的化合物（IX） 或更多的羟基和一个或多个对异氰酸酯基反应的氨基，（IX）的量使得反应性氨基的数量对应于数目o 聚氨酯（II）中的异氰酸酯基团。 这些材料可以用作含颜料的涂料的可交联粘合剂组分，特别是用于生产磁记录材料。