公开(公告)号：US11948710B2

公开(公告)日：2024-04-02

申请号：US18271622

申请日：2022-03-30

申请人： NIPPON STEEL CORPORATION

发明人： Hiroyasu Fujii ,  Jun Maki ,  Kazutoshi Takeda ,  Akira Akagi ,  Yuya Fujii

IPC分类号： H01F1/147 ,  B32B15/04 ,  B32B15/18 ,  C23C22/03 ,  C23C22/82

CPC分类号： H01F1/147 ,  B32B15/043 ,  B32B15/18 ,  C23C22/03 ,  C23C22/82 ,  B32B2255/06 ,  B32B2255/26 ,  B32B2307/206 ,  B32B2307/704 ,  B32B2307/714 ,  B32B2307/748

摘要： A non-oriented electrical steel sheet according to an embodiment of the present invention is a non-oriented electrical steel sheet including a base metal steel sheet and a composite coating film that is formed on surfaces of the base metal steel sheet and includes Zn-containing phosphate and an organic resin, wherein the non-oriented electrical steel sheet contains crystalline aluminum phosphate showing diffraction lines belonging to ICDD No. 01-074-3256 when the composite coating film is measured by a wide-angle X-ray diffraction method.

公开(公告)号：US09435033B2

公开(公告)日：2016-09-06

申请号：US14044248

申请日：2013-10-02

申请人： UT-Battelle, LLC

发明人： Jun Qu ,  Huimin Luo

IPC分类号： C23C22/48 ,  C23C22/57 ,  C23C22/03 ,  C23C22/74 ,  C23C22/00

CPC分类号： C23C22/03 ,  C23C22/48 ,  C23C22/57 ,  C23C22/74

摘要： A method for conversion coating a magnesium-containing surface, the method comprising contacting the magnesium-containing surface with an ionic liquid compound under conditions that result in decomposition of the ionic liquid compound to produce a conversion coated magnesium-containing surface having a substantially improved corrosion resistance relative to the magnesium-containing surface before said conversion coating. Also described are the resulting conversion-coated magnesium-containing surface, as well as mechanical components and devices containing the conversion-coated magnesium-containing surface.

摘要翻译： 一种用于转化涂覆含镁表面的方法，所述方法包括在导致离子液体化合物分解以产生具有显着改善的腐蚀的转化涂覆的含镁表面的条件下使含镁表面与离子液体化合物接触 在所述转化涂层之前相对于含镁表面的电阻。 还描述了所得到的转化涂覆的含镁表面，以及包含转化涂覆的含镁表面的机械组件和装置。

公开(公告)号：US09255332B2

公开(公告)日：2016-02-09

申请号：US14018483

申请日：2013-09-05

申请人： PPG Industries Ohio, Inc.

发明人： Mark W. McMillen ,  Nathan J. Silvernail ,  Peter L. Votruba-Drzal

IPC分类号： C23C22/78 ,  C23C22/03

CPC分类号： C23C22/78 ,  C23C22/03 ,  Y10T428/256

摘要： An activating rinse for treating a substrate is disclosed. The activating rinse comprises a first component comprising a dispersion of divalent or trivalent metal phosphate particles having an average particle size that is not greater than 10 μm, and a second component comprising first and second copolymers. The first copolymer is formed by the polymerization of ethylene oxide, propylene oxide, or combinations thereof, wherein one end of the first copolymer is terminated by an amine group, a hydroxyl group, or an alkyl group. The second copolymer is formed by the polymerization of styrene and a second monomer containing at least one carboxylate group, anhydride group, or combinations thereof. The second monomer is present in an amount of less than 50 percent by weight of the total weight of the second component. Also disclosed are methods for treating a substrate with the activating rinse and substrates treated with the activating rinse.

摘要翻译： 公开了一种用于处理基材的活化冲洗液。 活化漂洗液包括含有平均粒度不大于10μm的二价或三价金属磷酸盐颗粒的分散体的第一组分和包含第一和第二共聚物的第二组分。 第一共聚物通过环氧乙烷，环氧丙烷或其组合的聚合形成，其中第一共聚物的一端用胺基，羟基或烷基封端。 第二共聚物通过苯乙烯和含有至少一个羧酸酯基团，酸酐基团或其组合的第二单体的聚合而形成。 第二单体的存在量小于第二组分总重量的50重量％。 还公开了用活化冲洗剂处理底物的方法和用活化冲洗剂处理的底物。

公开(公告)号：US20150090369A1

公开(公告)日：2015-04-02

申请号：US14044248

申请日：2013-10-02

申请人： UT-Battelle, LLC

发明人： Jun Qu ,  Huimin Luo

IPC分类号： C23C22/03 ,  C23C22/73 ,  C23C22/82

CPC分类号： C23C22/03 ,  C23C22/48 ,  C23C22/57 ,  C23C22/74

摘要： A method for conversion coating a magnesium-containing surface, the method comprising contacting the magnesium-containing surface with an ionic liquid compound under conditions that result in decomposition of the ionic liquid compound to produce a conversion coated magnesium-containing surface having a substantially improved corrosion resistance relative to the magnesium-containing surface before said conversion coating. Also described are the resulting conversion-coated magnesium-containing surface, as well as mechanical components and devices containing the conversion-coated magnesium-containing surface.

摘要翻译： 一种用于转化涂覆含镁表面的方法，所述方法包括在导致离子液体化合物分解以产生具有显着改善的腐蚀的转化涂覆的含镁表面的条件下使含镁表面与离子液体化合物接触 在所述转化涂层之前相对于含镁表面的电阻。 还描述了所得到的转化涂覆的含镁表面，以及包含转化涂覆的含镁表面的机械组件和装置。

公开(公告)号：US20090050143A1

公开(公告)日：2009-02-26

申请号：US12293216

申请日：2007-03-23

申请人： Larry D. Boardman ,  Peter R. Johnson ,  Gary A. Korba ,  Mark E. Mueller ,  Mark J. Pellerite ,  Ravi Ravichandran

发明人： Larry D. Boardman ,  Peter R. Johnson ,  Gary A. Korba ,  Mark E. Mueller ,  Mark J. Pellerite ,  Ravi Ravichandran

IPC分类号： A61M15/00 ,  C23C22/05

CPC分类号： A61M15/009 ,  A61M2205/0222 ,  B65D83/54 ,  B82Y30/00 ,  C23C22/03 ,  C23C30/00

摘要： A container, such as a metered dose inhaler, suitable for use with a propellant-based medicinal formulation, the container comprising one or more treated metal surfaces that come into contact with the medicinal formulation, wherein the one or more treated metal surfaces are characterized by an organic surface treatment compound covalently bonded to the metal surface through a reactive head group selected from either phosphonic acid or carboxylic acid and wherein the organic surface treatment compound is further characterized by an exposed, substantially non-reactive tail group disposed away from the metal surface. Also, metered dose inhaler canisters and valves with treated surfaces.

摘要翻译： 一种容器，例如计量吸入器，适用于基于推进剂的药物制剂，所述容器包括与药物制剂接触的一种或多种经处理的金属表面，其中所述一种或多种经处理的金属表面的特征在于 通过选自膦酸或羧酸的反应性头基团共价结合到金属表面的有机表面处理化合物，其中有机表面处理化合物的进一步特征在于远离金属表面放置的暴露的，基本上不反应的尾基 。 此外，计量吸入器罐和具有处理表面的阀。

公开(公告)号：US20070023115A1

公开(公告)日：2007-02-01

申请号：US11472201

申请日：2006-06-20

申请人： Adriano Ferreira ,  Thomas Davisson ,  Sadashiv Nadkarni

发明人： Adriano Ferreira ,  Thomas Davisson ,  Sadashiv Nadkarni

IPC分类号： C22F1/04

CPC分类号： C23C22/03 ,  C23C22/82

摘要： A method of treating a surface of a metal foil or sheet to make the surface wettable. The method comprises obtaining a metal foil or sheet having an oil-coated surface to be treated, applying a solution of phosphoric acid in a polar, non-aqueous, water-free solvent evenly to the surface at a rate of application in a range of at least 10 mg/ft2, the phosphoric acid being contained in the solution at a concentration such that the phosphoric acid contacts the surface in an amount of 0.5 to 2.0 mg/ft2; and removing the solvent by either drying the surface or heating the foil or sheet at an elevated temperature above ambient to evaporate the oil from the surface to be treated with the proviso that the elevated temperature does not fall in the range between 130 to 240° C. The resulting foil has a wettable surface and can be used, for example, for coating with a layer of another material (e.g. polymer or adhesive) and achieve high peel strength.

摘要翻译： 一种处理金属箔或片的表面以使表面可润湿的方法。 该方法包括获得具有待处理的油涂层表面的金属箔或片材，在极性，非水性，无水溶剂中将磷酸溶液以适用的速度均匀地施加到表面上， 至少10mg / ft 2，磷酸以浓度使得磷酸以0.5-2.0mg / ft 2的量与表面接触， SUP>; 并且通过干燥表面或者在高于环境温度的高温下加热箔或片来除去溶剂，以便从被处理表面蒸发油，条件是升高的温度不在130-240℃的范围内 所得到的箔具有可润湿表面，并且可以用于例如用另一种材料（例如聚合物或粘合剂）层涂覆并实现高剥离强度。

公开(公告)号：US06762123B2

公开(公告)日：2004-07-13

申请号：US10345706

申请日：2003-01-16

申请人： Giuseppe Curro ,  Antonio Scandurra

发明人： Giuseppe Curro ,  Antonio Scandurra

IPC分类号： H01L2144

CPC分类号： H01L21/321 ,  C23C22/03 ,  C23C22/08 ,  C23C22/10 ,  H01L21/02071 ,  H01L2924/0002 ,  H01L2924/00

摘要： A method of producing a protective inhibitor layer of moisture-generated corrosion for aluminum (Al) alloy metallization layers, particularly in semiconductor electronic devices, includes chemically treating the metallization layer in at least two steps using a mixture of concentrated nitric acid and trace phosphoric acid to produce a thin protective phosphate layer. Alternatively, the method may include dipping the electronic device at least once in a mixture of a polar organic solvent and phosphoric acid (H3PO4) or phosphate derivatives thereof in a low percentage amount (e.g., with a phosphate reactant such as orthophosphoric acid or even R—HxPOy, where R is an alkaline type of ion group or an alkyl radical). The thin film may be formed on top of a thin layer of native aluminum oxide hydrate Al2O3.xH2O.

摘要翻译： 特别是在半导体电子器件中制备用于铝（Al）合金金属化层的湿气生成腐蚀保护抑制层的方法包括使用浓硝酸和痕量磷酸的混合物至少两步来对金属化层进行化学处理 以产生薄的保护性磷酸盐层。 或者，该方法可以包括以低百分比将电子设备浸入至极性有机溶剂和磷酸（H 3 PO 4）或其磷酸盐衍生物的混合物中一次（例如，使用磷酸盐反应物如正磷酸或甚至R -HxPOy，其中R是碱性离子基团或烷基基团）。 该薄膜可以形成在天然氧化铝水合物Al 2 O 3·xH 2 O薄层的顶部上。

公开(公告)号：US6036762A

公开(公告)日：2000-03-14

申请号：US225630

申请日：1999-01-05

申请人： Sankar Sambasivan

发明人： Sankar Sambasivan

IPC分类号： C23C22/03 ,  C23F11/04 ,  C09D5/08 ,  C09K15/02

CPC分类号： C23C22/03

摘要： A precursor solution for the preparation of metal phosphates is provided. Two components are prepared in which the first is a metal salt dissolved in alcohol, and the second component is phosphorous pentoxide dissolved in alcohol. The two components are mixed and may be applied as a liquid coating to a variety of substrates. The coated substrate is then heated, causing removal of all other components and leaving a layer of pure metal phosphate.

摘要翻译： 提供了用于制备金属磷酸盐的前体溶液。 制备两种成分，其中第一种是溶解在醇中的金属盐，第二种成分是溶解在醇中的五氧化二磷。 这两种组分是混合的并且可以作为液体涂料施加到各种基材上。 然后将涂覆的基材加热，除去所有其它组分并留下一层纯金属磷酸盐。

公开(公告)号：US4451301A

公开(公告)日：1984-05-29

申请号：US475799

申请日：1983-03-16

申请人： Dieter J. Mueller

发明人： Dieter J. Mueller

IPC分类号： C23C22/03 ,  C23F7/10

CPC分类号： C23C22/03

摘要： Homogeneous phosphating solutions comprise low-boiling halogenated hydrocarbons, aqueous phosphoric acid, methanol or an alcohol mixture consisting predominantly of methanol, nitroaromatics, ureas, optional conventional stabilizers, inhibitors, or accelerators, and, additionally, 0.01-2.0% by weight of formic acid esters as activating crystal nucleators.

摘要翻译： 均相磷酸盐溶液包括低沸点卤代烃，磷酸水溶液，甲醇或主要由甲醇，硝基芳族化合物，脲，任选的常规稳定剂，抑制剂或促进剂组成的醇混合物，另外还含有0.01-2.0重量％的甲酸 酯作为活化晶体成核剂。

公开(公告)号：US4182639A

公开(公告)日：1980-01-08

申请号：US958457

申请日：1978-11-06

申请人： Arthur J. Pignocco ,  Michael E. Waitlevertch

发明人： Arthur J. Pignocco ,  Michael E. Waitlevertch

IPC分类号： B32B25/08 ,  B29B15/00 ,  B29C55/00 ,  B29C65/70 ,  C08J5/04 ,  C08J5/06 ,  C23C22/03 ,  C23F7/12 ,  B60C9/16

CPC分类号： C08J5/06 ,  C23C22/03 ,  D07B1/0666 ,  C08J2321/00 ,  D07B2201/2011 ,  D07B2201/2013 ,  D07B2205/3089 ,  Y10S156/91 ,  Y10T428/12535 ,  Y10T428/12562 ,  Y10T428/12924 ,  Y10T428/24 ,  Y10T428/2944 ,  Y10T428/2945

摘要： Brass-coated steel cord is provided with improved adhesive characteristics for use in tire making, by coating it with certain combinations of sulfur-containing accelerators and phosphate corrosion inhibitors.

摘要翻译： 黄铜涂层钢丝帘线通过用含硫促进剂和磷酸盐腐蚀抑制剂的某些组合进行涂布而提供改进的用于轮胎制造的粘合特性。