公开(公告)号：US10711174B2

公开(公告)日：2020-07-14

申请号：US15825480

申请日：2017-11-29

申请人： Prahlad Yadav ,  Mohammed Al-Rabah ,  Gaurav Agrawal

发明人： Prahlad Yadav ,  Mohammed Al-Rabah ,  Gaurav Agrawal

IPC分类号： C09K8/035 ,  C09K8/06 ,  C09K8/86 ,  E21B43/16 ,  C09K8/04 ,  C01F11/34 ,  C01G9/04 ,  C01F11/24 ,  C09K8/58

摘要： A method of improving rheological properties of a divalent brine based downhole treatment fluid at an elevated temperature comprises adding to the divalent brine based downhole treatment fluid a rheological modifier, which comprises a carboxylic acid ester, or a phosphate ester blended with an ethoxylated glycol, or a combination comprising at least one of the foregoing in an amount effective to improve the rheological properties of the divalent brine based downhole treatment fluid at a temperature of greater than about 200° F. The divalent brine based downhole treatment fluid comprises calcium bromide, calcium chloride, zinc bromide, zinc chloride, or a combination comprising at least one of the foregoing.

公开(公告)号：US10099986B2

公开(公告)日：2018-10-16

申请号：US15547425

申请日：2016-01-29

申请人： CENTRE NATIONAL DE LA RECHERCHE SCIENTIFIQUE ,  UNIVERSITE DE MONTPELLIER

发明人： Claude Grison ,  Vincent Escande

IPC分类号： C07C45/65 ,  C01F7/00 ,  C01G9/00 ,  C01G49/10 ,  C07C45/62 ,  C07C29/17 ,  C07C29/143 ,  C01F7/56 ,  C01G9/04 ,  C07F7/08

摘要： Disclosed is an adduct between a Lewis acid, preferably aluminum trichloride, iron trichloride, or zinc dichloride, and a hydrosilane;—a method for preparing same; and a method for for reducing, particularly, an aldehyde, a ketone, an α,β-unsaturated ketone, an imine, or an α,β-unsaturated imine.

公开(公告)号：US20180055779A1

公开(公告)日：2018-03-01

申请号：US15684134

申请日：2017-08-23

申请人： Akina, Inc.

发明人： Kinam Park ,  Yeonhee Yun ,  Sarah Michelle Skidmore ,  Byung Kook Lee ,  John Solomon Garner

IPC分类号： A61K9/50 ,  A61K9/51 ,  C01G9/04 ,  C08G63/08

CPC分类号： A61K9/5031 ,  A61K9/0019 ,  A61K9/0024 ,  A61K9/113 ,  A61K9/143 ,  A61K9/146 ,  A61K9/1647 ,  A61K9/5153 ,  A61K38/4893 ,  A61K47/34 ,  A61K47/36 ,  C01G9/04 ,  C08G63/08

摘要： Methods for the formulation of biodegradable microparticles for delivery of protein drugs, such as botulinum toxin, have been developed. The methods include the steps of precipitating and washing proteins with organic solvent to remove water prior to dispersing in polymer-dissolved organic solvent to prevent exposure to water/solvent interfaces and maintain bioactivity of the protein drugs and fabrication of microparticles by either template or emulsion method. Biodegradable microparticles, formed of one or more biodegradable polymers having entrapped in the polymer one or more protein agents, such as botulinum toxin, are also provided. Precipitated botulinum toxin and botulinum toxin-loaded microparticles can also be formulated into thermogels or crosslinked hydrogels. The stability of the protein within these microparticles, as well as the controlled release of the entrapped agents, provides for sustained efficacy of the agents.

公开(公告)号：US20150329458A1

公开(公告)日：2015-11-19

申请号：US14424760

申请日：2013-08-27

申请人： MICROVAST POWER SYSTEMS CO., LTD.

发明人： Xiaoping ZHOU

IPC分类号： C07C51/00 ,  B01J27/135 ,  B01J27/125 ,  B01J27/132 ,  B01J27/08 ,  C01G30/00 ,  C01G19/06 ,  C01G9/04 ,  C01G37/04 ,  C01F7/56 ,  C01G3/05 ,  C01G19/08 ,  C01G19/00 ,  C01G51/08 ,  B01J27/138

CPC分类号： C07C51/00 ,  B01J27/08 ,  B01J27/125 ,  B01J27/132 ,  B01J27/135 ,  B01J27/138 ,  C01F7/56 ,  C01G3/05 ,  C01G9/04 ,  C01G19/00 ,  C01G19/06 ,  C01G19/08 ,  C01G30/007 ,  C01G37/04 ,  C01G51/085 ,  C07C67/00 ,  C07C59/08 ,  C07C69/68

摘要： The present disclosure provides a catalyst for preparing lactic acid and derivatives thereof, comprising at least one of metallic compounds MXn, wherein M is selected from Na, K, Mg, Ca, Sr, Ba, Al, Ga, In, Sn, Sb, Bi, Cr, Mn, Fe, Co, Ni and Zn, and n is an integer of 1 to 6. The present disclosure further provides a method for synthesis of lactic acid and derivatives thereof, wherein at least one raw material including carbohydrates, at least one alcohol, at least one of the aforesaid catalysts and at least one solvent are heated to react to prepare lactic acid and derivatives thereof.

摘要翻译： 本发明提供了一种制备乳酸及其衍生物的催化剂，其包含至少一种金属化合物MXn，其中M选自Na，K，Mg，Ca，Sr，Ba，Al，Ga，In，Sn，Sb， Bi，Cr，Mn，Fe，Co，Ni和Zn，n为1〜6的整数。本发明还提供了一种乳酸及其衍生物的合成方法，其中，至少含有碳水化合物的原料， 至少一种醇，至少一种上述催化剂和至少一种溶剂被加热反应以制备乳酸及其衍生物。

公开(公告)号：US08992882B2

公开(公告)日：2015-03-31

申请号：US12528738

申请日：2008-02-13

申请人： Joe D. Sauer ,  George W. Cook, Jr.

发明人： Joe D. Sauer ,  George W. Cook, Jr.

IPC分类号： C01B9/00 ,  H01M6/04 ,  C01G9/04 ,  C07C209/12 ,  H01M12/08

CPC分类号： C01G9/04 ,  C01P2006/40 ,  C01P2006/80 ,  C07C209/12 ,  H01M12/085 ,  Y02E60/128 ,  C07C211/63

摘要： Ultra-high purity zinc bromide and quaternary ammonium bromides suitable for use in zinc-bromine batteries, and methods for making same, are provided.

摘要翻译： 提供了适用于锌 - 溴电池的超高纯度溴化锌和溴化季铵及其制备方法。

公开(公告)号：US20110097161A1

公开(公告)日：2011-04-28

申请号：US12999297

申请日：2009-06-18

申请人： Andreas Becker ,  Placido Garcia-Juan

发明人： Andreas Becker ,  Placido Garcia-Juan

IPC分类号： B65G51/00 ,  C01G9/04 ,  B32B5/16 ,  B23K35/34 ,  B65G35/00

CPC分类号： B23K35/3601 ,  B23K35/3605 ,  C01G9/006 ,  C01P2004/51 ,  C01P2004/61 ,  C01P2006/20 ,  Y10T428/2982

摘要： Fluidizable potassium fluorozincate which is very suitable for dry fluxing applications can be prepared from a diluted potassium base selected from the group consisting of KOH, KHCO3 and K2CO3, ZnO and HF. The cumulative volume of the particles has an X10 value of equal to or greater than 1.5 microns, preferably, equal to or greater than 2 microns. It is very suitable for pneumatic transport for aluminum brazing.

摘要翻译： 非常适用于干燥助熔应用的可流化的氟锌酸钾可以从选自KOH，KHCO 3和K 2 CO 3，ZnO和HF的稀释的钾碱制备。 颗粒的累积体积具有等于或大于1.5微米，优选等于或大于2微米的X 10值。 非常适合用于铝钎焊的气动输送。

公开(公告)号：US20050211631A1

公开(公告)日：2005-09-29

申请号：US10502497

申请日：2003-01-22

申请人： Pascal Muller ,  Athmane Benchara ,  Eric Meux ,  Pierre Devigili

发明人： Pascal Muller ,  Athmane Benchara ,  Eric Meux ,  Pierre Devigili

IPC分类号： C22B19/00 ,  B01D11/02 ,  B01J41/04 ,  B01J49/00 ,  C01G9/00 ,  C01G9/04 ,  C01G53/00 ,  C01G53/08 ,  C02F1/26 ,  C02F1/42 ,  C22B3/42 ,  C22B3/44 ,  C22B19/20 ,  C22B23/00

CPC分类号： C22B23/0453 ,  B01J41/04 ,  B01J49/57 ,  C01G9/006 ,  C01G53/006 ,  C01P2006/80 ,  C22B3/42 ,  C22B19/26 ,  Y02P10/234

摘要： A method for the separation of zinc and a second metal which does not form an anionic complex in the presence of chloride ions, zinc and the second metal being present in an effluent in the form of ZnCl2 and a second metal chloride. The formation of the anionic complex is obtained by bringing the effluent into contact with the resin saturated with chloride ions. The second metal chloride is extracted by means of a first eluent, followed by extraction of zinc with a degree of oxidation of +II. Generally, the second metal is a transition metal such as Cr, Cu, Ni, Fe and, more specifically, nickel.

摘要翻译： 锌和第二金属的分离方法，其在氯离子存在下不形成阴离子络合物，锌和第二金属存在于ZnCl 2和第二金属氯化物形式的流出物中。 通过使流出物与氯离子饱和的树脂接触来获得阴离子络合物的形成。 通过第一洗脱液萃取第二种金属氯化物，然后以+ II的氧化程度提取锌。 通常，第二金属是过渡金属如Cr，Cu，Ni，Fe，更具体地说是镍。

公开(公告)号：US6030433A

公开(公告)日：2000-02-29

申请号：US750342

申请日：1997-02-05

申请人： Hendrik Jan Luggenhorst ,  Edgar Manfred Lawrence Peek

发明人： Hendrik Jan Luggenhorst ,  Edgar Manfred Lawrence Peek

IPC分类号： B09B3/00 ,  C01B9/02 ,  C01G1/06 ,  C01G9/04 ,  C01G21/16 ,  C22B7/00

CPC分类号： C01B9/02 ,  C01G1/06 ,  C22B7/001 ,  C22B7/006 ,  Y02P10/214 ,  Y02P10/234 ,  Y10S75/961

摘要： A method for extracting metals from metal-containing materials, especially waste, by pyrohydrolysis. The metal-containing materials which contain at least one or more of the metals from the group consisting of Zn, Cd, Pb, Hg, Cu, Sn (as Sn(0) and Sn(II)), As, Sb, Au, Ag and Bi, are made to react at 700-1100.degree. C., advantageously 800-900.degree. C., with a gas composition which at least comprises 25-45% by volume of water vapor, 0-12% by volume of carbon dioxide, 2-20% by volume of hydrogen chloride, 0-15% by volume of carbon monoxide, the remainder being nitrogen and possibly oxygen. The metals from the above-mentioned group are extracted in the form of volatile metal chlorides. More particularly, metal-containing materials are used which also contain one or more metals from the group consisting of Fe, Cr, Mn, Ni, Mg, Ca, Al, Si, Ti, Co and Zr, this last group of materials being hydrolysed, under the reaction conditions, to give non-volatile metal oxides, or remain, in the oxidic form, or form (2) a non-volatile metal chloride and therefore remain behind in the starting material.

摘要翻译： PCT No.PCT / NL95 / 00185 Sec。 371日期1997年2月5日 102（e）日期1997年2月5日PCT Filed Jun。1，1995 PCT Pub。 WO95 / 33686 PCT公开号 日期1995年12月14日一种通过热解解从含金属材料，特别是废物中提取金属的方法。 含有Zn，Cd，Pb，Hg，Cu，Sn（Sn（0）和Sn（II））中的至少一种或多种金属的含金属材料，As，Sb，Au， Ag和Bi在700-1100℃（有利地800-900℃）下与气体组合物反应，该组合物至少包含25-45体积％的水蒸汽，0-12体积％的碳 二氧化碳，2-20体积％的氯化氢，0-15体积％的一氧化碳，其余的是氮气和可能的氧气。 来自上述组的金属以挥发性金属氯化物的形式提取。 更具体地，使用含有Fe，Cr，Mn，Ni，Mg，Ca，Al，Si，Ti，Co和Zr的一种或多种金属的含金属材料，最后一组被水解的材料 在反应条件下，得到非挥发性金属氧化物，或保留为氧化形式，或形成（2）非挥发性金属氯化物，因此留在起始原料中。

公开(公告)号：US5856597A

公开(公告)日：1999-01-05

申请号：US846095

申请日：1997-04-25

申请人： K. Pushpananda A. Senaratne ,  Felix M. Orihuela ,  Arcelio J. Malcolm

发明人： K. Pushpananda A. Senaratne ,  Felix M. Orihuela ,  Arcelio J. Malcolm

IPC分类号： C01G9/04 ,  C07C17/16

CPC分类号： C07C17/16 ,  C01G9/04 ,  Y02P20/582

摘要： Gaseous anhydrous hydrogen chloride is introduced into an aqueous solution of zinc chloride under conditions effective to produce a more efficient Lucas reagent than a Lucas reagent made by mixing solid, anhydrous zinc chloride with 38% hydrochloric acid. For example, the reaction rate of such Lucas reagent with levo-menthol is much faster and requires a much shorter reaction period than Lucas reagent formed in the conventional manner from anhydrous, solid zinc chloride and concentrated (38%) hydrochloric acid. Also, the conversion to levo-menthyl chloride was higher when using Lucas reagent formed using gaseous anhydrous hydrogen chloride and aqueous zinc chloride solution. Also, Lucas reagent made in this manner is highly amenable to recycling, and requires only addition thereto of hydrogen chloride to replenish the catalyst for an ensuing run.

摘要翻译： 将气态无水氯化氢引入到氯化锌水溶液中，该条件有效地产生比通过将固体无水氯化锌与38％盐酸混合的Lucas试剂更有效的Lucas试剂。 例如，这种Lucas试剂与左旋薄荷醇的反应速度要快得多，并且比用无水固体氯化锌和浓缩（38％）盐酸以常规方式形成的Lucas试剂要短得多的反应时间。 此外，当使用使用气态无水氯化氢和氯化锌水溶液形成的Lucas试剂时，转化为氯化叶绿素较高。 此外，以这种方式制备的Lucas试剂高度易于再循环，并且仅需要加入氯化氢来补充催化剂用于随后的运行。

公开(公告)号：US5550100A

公开(公告)日：1996-08-27

申请号：US467379

申请日：1995-06-06

申请人： Yili Guo

发明人： Yili Guo

IPC分类号： A23C9/152 ,  A01N25/14 ,  A01N25/30 ,  B01F17/00 ,  B01J20/02 ,  C01G9/04 ,  C11D7/10

CPC分类号： B01F17/0007

摘要： New and improved compositions comprising particulates and an effective amount of manganese chloride to reduce significantly the wetting time and/or the dispersion time of said particulates relative to said time(s) in the absence of said salt(s) have been discovered. Methods for reducing the wetting time of particulates in liquid have also been discovered.

摘要翻译： 已经发现了新的和改进的组合物，其包含颗粒和有效量的氯化锰以显着减少在不存在所述盐的情况下相对于所述时间的所述颗粒的润湿时间和/或分散时间。 还发现了减少液体中微粒的润湿时间的方法。