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    Flavoring with norbornanol derivatives
    3.
    发明授权
    Flavoring with norbornanol derivatives 失效
    用降冰片烷醇衍生物调味

    公开(公告)号：US4089986A

    公开(公告)日：1978-05-16

    申请号：US834399

    申请日：1977-09-19

    申请人： Kenneth K. Light ,  Manfred Hugo Vock ,  Edward J. Shuster ,  Frederick Louis Schmitt

    发明人： Kenneth K. Light ,  Manfred Hugo Vock ,  Edward J. Shuster ,  Frederick Louis Schmitt

    IPC分类号： C07C69/02 ,  A23G4/00 ,  A23G4/06 ,  A23L27/20 ,  A61K8/33 ,  A61K8/34 ,  A61K8/35 ,  A61K8/37 ,  A61Q13/00 ,  C07C27/00 ,  C07C31/137 ,  C07C33/05 ,  C07C35/29 ,  C07C41/00 ,  C07C43/115 ,  C07C43/162 ,  C07C43/305 ,  C07C45/00 ,  C07C49/317 ,  C07C49/527 ,  C07C67/00 ,  C07C239/00 ,  C07C251/44 ,  C07D303/04 ,  C11B9/00 ,  A23L1/226

    CPC分类号： A23G4/06 ,  C07C35/29 ,  C11B9/0046 ,  C11D3/0084

    摘要： Processes and compositions are described for the use in foodstuff, chewing gum, toothpaste and medicinal product flavor and aroma and perfume aroma augmenting, enhancing, modifying and imparting compositions and as foodstuff, chewing gum, toothpaste, medicinal product, perfume and perfumed article aroma imparting materials of 3,3-dimethyl-2(3-butenyl) norbornanol-2 (hereinafter referred to as the "norbornanol derivative" having the structure: ##STR1## (which structure is intended to cover both the "endo" and the "exo" isomers thereof) produced by a process which comprises reacting an allylic Grignard reagent having the structure: wherein X is chloro, bromo or iodo with camphene oxide having the structure: ##STR2## by either "exo" camphene oxide or "endo" camphene oxide or a mixture of "exo" and "endo" camphene oxide. Addition of the said norbornanol derivative to consumable materials is indicated to produce:(a) In foodstuffs, foodstuff flavorings, chewing gums, toothpastes and medicinal products, sweet, fruity, berry-like aromas with woody, incense-like, cedarwood-like, tea-like and floral nuances and incense-like and cedarwood-like flavors with rosey, berry and tea-like nuances; and(b) In perfumes, colognes and perfumed articles, sweet, woody, thujone-like aromas with strong fir-balsam, armoise, cedarleaf, piney, earthy and camphoraceous nuances.

    摘要翻译： 描述了用于食品，口香糖，牙膏和药用产品风味和芳香和香料香气的方法和组合物，其增强，增强，改性和赋予组合物以及作为食品，口香糖，牙膏，药用产品，香料和香料制品香气赋予 3,3-二甲基-2（3-丁烯基）降冰片烷醇-2的材料（以下称为“降冰片醇衍生物”，具有以下结构：（该结构旨在涵盖“endo”和“exo 通过包括使具有以下结构的烯丙基格利雅试剂（其中X为氯，溴或碘）与具有以下结构的camp氧化物反应的方法制得的：其异构体：通过“外部”camp oxide或“内 氧化camp oxide oxide or：camp camp camp camp camp camp camp camp camp camp camp camp：：：：：：：：：：：：：：：：：

    Bicyclo{8 2.2.1{9 {0 Hept-5(6)-yl compounds
    7.
    发明授权
    Bicyclo{8 2.2.1{9 {0 Hept-5(6)-yl compounds 失效
    双环{8 2.2.1 {9 {0 Hept-5（6） - 基化合物

    公开(公告)号：US3927116A

    公开(公告)日：1975-12-16

    申请号：US14765071

    申请日：1971-05-27

    申请人： UNION CARBIDE CORP

    发明人： RICK EDWARD A ,  TINSLEY SAMUEL W

    IPC分类号： C07C35/29 ,  C08G59/24 ,  C08K5/06 ,  C07C35/28 ,  C07C43/18

    CPC分类号： C08G59/24 ,  C07C35/29 ,  C08K5/06

    摘要： 2-Vinylbicyclo(2.2.1)hept-5(6)-yl and 2epoxyethylbicyclo(2.2.1)hept-5(6)-yl compounds, wherein the vinyl compounds are prepared by the addition of the active hydrogencontaining compounds to the strained-ring double bond of the bicyclo-heptene ring in 2-vinylbicyclo(2.2.1)hept-5-ene and the epoxy compounds are prepared by the epoxidation of the vinyl compounds. The compounds find utility as solvents for resins and oils, monomers for preparing synthetic waxes and resins, chemical intermediates for pharmaceuticals, wetting agents, insecticides, emulsifying agents, detergents, bactericides and fungicides.

    摘要翻译： 2-乙烯基双环[2.2.1]庚-5（6） - 基和2-环氧乙基双环[2.2.1]庚-5（6） - 基化合物，其中乙烯基化合物是通过加入含活性氢的 通过环氧化乙烯基化合物制备2-乙烯基双环[2.2.1]庚-5-烯中双环庚烯环的应变环双键的化合物和环氧化合物。 该化合物可用作树脂和油的溶剂，用于制备合成蜡和树脂的单体，药物的化学中间体，润湿剂，杀虫剂，乳化剂，洗涤剂，杀菌剂和杀真菌剂。

    Process for preparing beta-santalol from 3-methylnorcamphor
    8.
    发明授权
    Process for preparing beta-santalol from 3-methylnorcamphor 失效
    从3-甲基喹啉制备苯三酚的方法

    公开(公告)号：US3662008A

    公开(公告)日：1972-05-09

    申请号：US3662008D

    申请日：1969-05-21

    申请人： PROCTER & GAMBLE

    发明人： KRETSCHMAR HERBERT C ,  ERMAN WILLIAM F

    IPC分类号： C07C35/29 ,  C07C45/28 ,  C07C45/59 ,  C07C45/68 ,  C07C47/225 ,  C07C49/433 ,  C07C49/653 ,  C11B9/00 ,  C07C35/02

    CPC分类号： C11B9/0046 ,  C07C35/29 ,  C07C45/28 ,  C07C45/59 ,  C07C45/68 ,  C07C47/225 ,  C07C49/433 ,  C07C49/653

    摘要： A PROCESS FOR PREPARING B-SANTALOL, USEFUL IN PERFUME COMPOSITIONS, FROM 3-METHYLNORCAMPHOR COMPRISING THE STEPS OF (1) ALKYLATING 3-METHYLNORCAMPHOR IN STRONG BASE WITH AN ALLYL HALIDE; (2) REACTING THE REACTION PRODUCT OF STEP (1) WITH A METHYLMETALLIC COMPOUND, SUCH AS METHYLITHIUM, FOLLOWED BY HYDROLYSIS; (3) BROMINATING THE REACTION PRODUCT OF STEP (2); (4) DEHYDROBROMINATING THE REACTION PRODUCT OF STEP (3) WITH A BASE, SUCH AS SODIUM AMIDE; (5) DEHYDRATING THE REACTION PRODUCT OF STEP (4) WITH A DEHYDRATING AGENT, SUCH AS THIONYL CHLORIDE; (6) REACTING THE REACTION PRODUCT OF STEP (5) WITH A COMPOUND, SUCH AS DI(SEC.-ISO-AMYL) BORANE FOLLOWED BY AN OXIDATION; (7) REACTING THE REACTION PRODUCT OF STEP (6) WITH (CARBETHOXYETHYLIDENE)TRIPHENYLPHOSPHORANE; AND (8) REDUCING THE REACTION PRODUCT OF STEP (7) WITH A REDUCING AGENT, SUCH AS LITHIUM ALUMINUM HYDRIDE, TO OBTAIN B-SANTALOL, AND NOVEL COMPOUNDS PRODUCED THEREIN ARE DISCLOSED.