摘要:
A graphite electrode includes a pole having a socket in an internal screw shape at an end portion, and a nipple in an external screw shape that can be fastened to the socket, wherein a value obtained by subtracting an effective diameter on a small diameter end side of the nipple from an effective diameter on a small diameter end side of the socket is 0.05 to 0.7 mm, and a value obtained by subtracting a taper angle of the socket from a taper angle of the nipple is −2 minutes to −3 minutes 30 seconds.
摘要:
A method for the production of polygranular graphite bodies including the step of provisioning a mixture including a high-temperature treated anthracite having a high vitrinite content and a petroleum-based needle coke and/or a pitch-based needle coke, and provisioning at least one binder coke precursor. The method also includes the steps of forming a green body from the mixture from the provisioning step, and carbonizing and graphitizing the green body.
摘要:
Method of manufacturing a fused silica crucible, including manufacturing a plurality of carbon electrodes for melting a vitreous silica object to be melted by arc discharge by rubbing the surface of a carbon electrode of the electrodes with a vitreous silica of the same type as the vitreous silica object to be melted, by at least one of: inserting a front end of the carbon electrode into a storage tank storing powdered vitreous silica, by at least one of rotating and reciprocating in an axial direction the storage tank and the carbon electrode relative to each other; rubbing the surface of the carbon electrode by ejecting powdered vitreous silica from a nozzle onto the surface of the electrode; rubbing the surface of the electrode with a vitreous silica grinder; and rubbing the surface of the electrode against a rotating surface of a portion of a fused vitreous silica crucible.
摘要:
A sputtering target for producing a metallic glass membrane characterized in comprising a structure obtained by sintering atomized powder having a composition of a ternary compound system or greater with at least one or more metal elements selected from Pd, Zr, Fe, Co, Cu and Ni as its main component (component of greatest atomic %), and being an average grain size of 50 μm or less. The prepared metallic glass membrane can be used as a substitute for conventional high-cost bulk metallic glass obtained by quenching of molten metal. This sputtering target for producing the metallic glass membrane is also free from problems such as defects in the metallic glass membrane and unevenness of composition, has a uniform structure, can be produced efficiently and at low cost, and does not generate many nodules or particles. Further provided is a method for manufacturing such a sputtering target for forming the metallic glass membrane.
摘要:
The present invention relates to a process for the preparation of compounds of general formula (I) Lia-bM1bV2-cM2c(PO4)x (I) with M1: Na, K, Rb and/or Cs, M2: Ti, Zr, Nb, Cr, Mn, Fe, Co, Ni, Al, Mg and/or Sc, a: 1.5-4.5, b: 0-0.6, c: 0-1.98 and x: number to equalize the charge of Li and V and M1 and/or M2, if present, wherein a−b is >0, by providing an essentially aqueous mixture comprising at least one lithium-comprising compound, at least one vanadium-comprising compound in which vanadium has the oxidation state +5 and/or +4, and at least one M1-comprising compound, if present, and/or at least one M2-comprising compound, if present, and at least one reducing agent which is oxidized to at least one compound comprising at least one phosphorous atom in oxidation state +5, drying and calcining.
摘要:
A graphite electrode for an electrothermic reduction furnace is formed from anode grade coke and graphitized at a graphitization temperature below 2700° C. The resulting electrode is particularly suited for carbothermal reduction of alumina. It has an iron content of about 0.05% by weight, a specific electrical resistivity of above 5 μOhm·m, and a thermal conductivity of less than 150 W/m·K. The graphite electrode is manufactured by first mixing calcined anode coke with a coal-tar pitch binder, and a green electrode is formed from the mixture at a temperature close to the softening point of the pitch binder. The green electrode is then baked to carbonize the pitch binder to solid coke. The resultant carbonized electrode, after further optional processing is then graphitized at a temperature below 2700° C. for a time sufficient to cause the carbon atoms in the carbonized electrode to organize into the crystalline structure of graphite.
摘要:
A threaded connection is secured against loosening/unscrewing for columns of carbon and/or graphite electrodes. The electrodes are connected in columns with threaded connection elements, i.e., carbon connecting pins. At least one part has a wedge ramp on the root of the thread winding. When the components of the threaded connection are screwed together, the crests of the thread windings of one part abut with the wedge ramps of the other threaded connection component. A contact line is created, possibly multiple sections of a contact line. When the parts are screwed together, all forces are transferred from one part to the other only via the contact line. In a special case, the contour of the thread winding along whose root the wedge ramp is running is reduced e.g. to a connecting line between two wedge ramps located one above the other in the cross-section.
摘要:
A carbon material is formed by heat-treating a carbonaceous material in a reaction mix of oxides of boron and boron nitride in a nitrogen atmosphere to temperatures of 1600 to 2000° C. The surface of the carbonaceous material is transformed into a carbon material that is resistant to oxidation to temperatures of 900° C., enabling machined components to be utilized for weeks at that temperature. The carbon material is also stable in inert or vacuum environments to temperatures in the range of 1500 to 2000° C., enabling its use as aluminum evaporative boats and the like.
摘要:
A cylindrical graphite electrode with a consumable end includes one or more slots comprising a discontinuous portion of the carbon which extend along the length of the carbon body through at least a portion of the cross-section substantially to the consumable end. The slot may extend from the surface into the body or the slot may extend within the body below the surface. The slot may be filled with a carbonaceous material different from the carbon of the body. The slot may extend helically along the length and around a portion of the periphery of the body. The slots may be formed prior to or after heat treating of the electrode. As the electrode is exposed to a thermal shock, a crack is initiated in and propagates along the electrode and intersects with the slot, wherein substantial further growth of the crack is arrested at the slot.
摘要:
The subject invention is a plug for sealing recesses in anode blocks designed to hold anode rods, wherein the anode blocks are intended for the electrolytic extraction of base metals during their calcination treatment. The proposed plug is characterized by the fact that it is die-formed and composed of a material containing cellulose. This provides a very close seal in the anode recess, such that coke granules, which are inserted as fill material to displace oxygen in gaps between several anode blocks within a calcining furnace, cannot enter the anode recesses. Undesirable conglutination inside the anode recesses and burning of the material defining the anode recesses, caused by the unavoidable presence of some oxygen residue during the calcination process, can no longer occur. Because of the great solidity of the plug, deformations of the recesses in the lower rows of anode blocks in the calcining furnace are prevented. At the conclusion of the calcination process, after the anode recesses are precipitation-hardened, the cellulose containing plugs are carbonized, whereby the coal or ashes remaining in the recesses can be removed by vacuuming, without any difficulty in a subsquent operation.