摘要:
In order to control the position of a specimen on a specimen holder with high accuracy, a specimen cartridge (1) is made of a good thermal conductor, an outer frame (5) is made of heat insulating material and a connecting rod is made of a poor thermal conductor. The temperature distribution of the specimen (2) becomes uniform and the temperature drift is reduced. Further, thermal expansion of a specimen cartridge tilting rod (3) does not affect the tilting angle. These features make it possible to perform various highly accurate observations and measurements with an electron microscope.
摘要:
An anti-reflection film (2) is produced on the panel surface of a cathode-ray tube (1) by:
(A) preparing a solution (8) for forming an anti-reflection film (2), which contains water and an alkoxide having the formula,
M(OR) n
wherein M is Si or a metal selected from the group consisting of Ti, Al, Zr, Sn, In, Sb and Zn; R is an alkyl group having 1-10 carbon atoms; n is an integer of from 1 to 8; and when n is not 1, the alkyl groups represented by R may be the same or different, (B) coating the solution (8) for forming an anti-reflection film (2) on the outermost surface of the panel of a cathode-ray tube (1), and (C) applying an ultraviolet light (7) to the solution (8) for forming an anti-reflection film (2) coated on said surface to cure the solution to form a transparent film with fine roughness.
This production method is carried out using an apparatus having:
(a) a coating means (3) for coating the above solution (8) for forming an anti-reflection film (2) on the outermost surface of the panel of a cathode-ray tube (1), (b) a transferring means (4) for transferring the solution-coated cathode-ray tube (1), and (c) an ultraviolet light-applying means (7) for photocuring the solution (8) coated on the cathode-ray tube (1) during the transfer of the solution-coated cathode-ray tube.
In the above method, when a silicon alkoxide is used as the metal alkoxide, there can be obtained a cathode-ray tube having an anti-reflection film made of alkali-free silica on the outermost surface of the panel, said anti-reflection film giving a ratio of Si-O-Si peak intensity to Si-OH peak intensity of 4 or more when measured for infrared spectrum. Further embodiments include an antistatic layer and the inclusion of an organic dye into the anti-reflection film.
摘要:
The invention relates to resin-molded axial lead-type semiconductor devices comprising a sub-assembly consisting of a semiconductor pellet (1) brazed between a pair of axial leads (5). The sub-assembly is sealed in an epoxy resin, which is formed by applying an epoxy resin, preferably a one-can-epoxy resin, onto the sub-assembly followed by curing the epoxy resin. Preferably, an epoxy resin having a thixotropic index of 1.0 to 2.5 and a gelation time 0.8 to 3 minutes is used. The invention further relates to a process for manufacturing these semiconductor devices which is characterised by:
(A) horizontally holding the sub-assembly and dropping a predetermined amount of an epoxy resin onto the semiconductor pellet while turning the sub-assembly with the axial leads as rotation axis, (B) curing the epoxy resin, preferably by heating at 160° to 180°C for a period of 2 to 10 min, while turning the sub-assembly, so that the surface portions of the epoxy resin are cured, and (C) curing the epoxy resin, preferably by heating at 160° to 200°C for a period of 3 to 24 h while maintaining the sub-assembly stationary without turning it, so that the epoxy resin is completely hardened.
摘要:
An analytical electron microscope automatically identifies objects in a sample (31) on the basis of shape of the object, change of thickness of the object and/or change of element (such as change of element type or concentration). Therefore, the operator of the analytical electron microscope can specify a desired object, and an example or examples of that object in a sample can be identified automatically. The characteristics need to identify the object are determined by detecting the effect of the sample on the electron beam (32) of the analytical electron microscope, using, for example, an energy dispersive type X-ray analyzer (75) and an electron energy loss spectrometer (74). Once an example of the object has been identified, it may be analyzed further. The analytical electron microscope may also analyze a sample (31) to identify and classify the objects present.