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    EXTREME SYNTHESIS OF CRYSTALLINE AEROGEL MATERIALS FROM AMORPHOUS AEROGEL PRECURSORS
    1.
    发明申请
    EXTREME SYNTHESIS OF CRYSTALLINE AEROGEL MATERIALS FROM AMORPHOUS AEROGEL PRECURSORS 审中-公开
    来自无机空气前驱体的结晶气体材料的极限合成

    公开(公告)号：US20110129614A1

    公开(公告)日：2011-06-02

    申请号：US12958224

    申请日：2010-12-01

    申请人： Peter J. Pauzauskie ,  Jonathan C. Crowhurst ,  Marcus A. Worsley ,  Joe H. Satcher, JR.

    发明人： Peter J. Pauzauskie ,  Jonathan C. Crowhurst ,  Marcus A. Worsley ,  Joe H. Satcher, JR.

    IPC分类号： B05D3/06 ,  H01B1/00 ,  C09K3/00

    CPC分类号： C09K11/65 ,  C01B13/322 ,  C01B33/1585 ,  C01P2002/02 ,  C01P2002/72 ,  C01P2002/84 ,  C01P2004/03 ,  C01P2004/04 ,  C01P2006/10 ,  C01P2006/12 ,  C09C1/44

    摘要： In one embodiment, a system includes a pressure cell adapted for enclosing a porous structure; an inert pressure medium within the pressure cell; and a heat source for heating the porous structure. In another embodiment, a composition of matter includes a crystalline porous structure having a density of about 30 to about 50 mg/cm3. A method according to one embodiment includes positioning an amorphous porous structure in a pressure cell; injecting an inert pressure medium within the pressure cell; and pressurizing the pressure cell to a pressure that thermodynamically favors a crystalline phase of the porous structure over an amorphous phase of the porous structure to transition the amorphous porous structure into a crystalline porous structure. Additional embodiments are also presented.

    摘要翻译： 在一个实施例中，系统包括适于封闭多孔结构的压力池; 压力池内的惰性压力介质; 以及用于加热多孔结构的热源。 在另一个实施方案中，物质组合物包括密度为约30至约50mg / cm 3的结晶多孔结构。 根据一个实施方案的方法包括将无定形多孔结构定位在压力池中; 在压力池内注入惰性压力介质; 并且将所述压力室加压至在所述多孔结构的非晶相上热力学有利于所述多孔结构的结晶相的压力，以使所述无定形多孔结构转变为结晶多孔结构。 还提供了另外的实施例。

    METHODS FOR CONTROLLING PORE MORPHOLOGY IN AEROGELS USING ELECTRIC FIELDS AND PRODUCTS THEREOF
    4.
    发明申请
    METHODS FOR CONTROLLING PORE MORPHOLOGY IN AEROGELS USING ELECTRIC FIELDS AND PRODUCTS THEREOF 有权
    使用电场及其产品控制空间形态的方法

    公开(公告)号：US20120052511A1

    公开(公告)日：2012-03-01

    申请号：US13180440

    申请日：2011-07-11

    申请人： Marcus A. Worsley ,  Theodore F. Baumann ,  Joe H. Satcher, JR. ,  Tammy Y. Olson ,  Joshua D. Kuntz ,  Klint A. Rose

    发明人： Marcus A. Worsley ,  Theodore F. Baumann ,  Joe H. Satcher, JR. ,  Tammy Y. Olson ,  Joshua D. Kuntz ,  Klint A. Rose

    IPC分类号： B32B3/26 ,  C12N5/00 ,  B32B5/22 ,  H01B1/08 ,  H01B1/04 ,  G01N33/53 ,  H01B1/00

    CPC分类号： H01B1/08 ,  B01J13/0091 ,  Y10T428/249953 ,  Y10T428/249986

    摘要： In one embodiment, an aerogel or xerogel includes column structures of a material having minor pores therein and major pores devoid of the material positioned between the column structures, where longitudinal axes of the major pores are substantially parallel to one another. In another embodiment, a method includes heating a sol including aerogel or xerogel precursor materials to cause gelation thereof to form an aerogel or xerogel and exposing the heated sol to an electric field, wherein the electric field causes orientation of a microstructure of the sol during gelation, which is retained by the aerogel or xerogel. In one approach, an aerogel has elongated pores extending between a material arranged in column structures having structural characteristics of being formed from a sol exposed to an electric field that causes orientation of a microstructure of the sol during gelation which is retained by the elongated pores of the aerogel.

    摘要翻译： 在一个实施方案中，气凝胶或干凝胶包括其中具有小孔的材料的柱结构，以及没有位于柱结构之间的材料的主要孔，其中主孔的纵轴基本上彼此平行。 在另一个实施方案中，一种方法包括加热包括气凝胶或干凝胶前体材料的溶胶，使其凝胶形成气凝胶或干凝胶，并将加热的溶胶暴露于电场，其中电场引起凝胶化过程中溶胶微结构的取向 ，由气凝胶或干凝胶保留。 在一种方法中，气凝胶具有延伸的细孔，所述孔在布置在柱结构中的材料之间延伸，所述材料具有由暴露于电场的溶胶形成的结构特征，所述溶胶引起凝胶化期间溶胶的微结构的取向， 气凝胶

    PYROPHORIC METAL-CARBON FOAM COMPOSITES AND METHODS OF MAKING THE SAME
    5.
    发明申请
    PYROPHORIC METAL-CARBON FOAM COMPOSITES AND METHODS OF MAKING THE SAME 有权
    PORROPHORIC金属碳泡沫复合材料及其制备方法

    公开(公告)号：US20100139823A1

    公开(公告)日：2010-06-10

    申请号：US12329437

    申请日：2008-12-05

    申请人： Alexander E. Gash ,  Joe H. Satcher, JR. ,  Randall L. Simpson ,  Theodore F. Baumann ,  Marcus A. Worsley

    发明人： Alexander E. Gash ,  Joe H. Satcher, JR. ,  Randall L. Simpson ,  Theodore F. Baumann ,  Marcus A. Worsley

    IPC分类号： C06B45/04

    CPC分类号： C06C15/00 ,  C06B45/00

    摘要： A method for creating a pyrophoric material according to one embodiment includes thermally activating a carbon foam for creating micropores therein; contacting the activated carbon foam with a liquid solution comprising a metal salt for depositing metal ions in the carbon foam; and reducing the metal ions in the foam to metal particles. A pyrophoric material in yet another embodiment includes a pyrophoric metal-carbon foam composite comprising a carbon foam having micropores and mesopores and a surface area of greater than or equal to about 2000 m2/g, and metal particles in the pores of the carbon foam. Additional methods and materials are also disclosed.

    摘要翻译： 根据一个实施例的用于产生自燃材料的方法包括热活化碳泡沫以在其中产生微孔; 使活性炭泡沫与包含用于在碳泡沫中沉积金属离子的金属盐的液体溶液接触; 并将泡沫中的金属离子还原成金属颗粒。 在另一个实施方案中的自燃材料包括自发金属 - 碳泡沫复合材料，其包含具有微孔和介孔的碳泡沫，并且表面积大于或等于约2000m 2 / g，以及碳泡沫的孔中的金属颗粒。 还公开了附加的方法和材料。

    Porous substrates filled with nanomaterials
    6.
    发明授权
    Porous substrates filled with nanomaterials 有权
    填充纳米材料的多孔基材

    公开(公告)号：US08809230B2

    公开(公告)日：2014-08-19

    申请号：US13195752

    申请日：2011-08-01

    申请人： Marcus A. Worsley ,  Theodore F. Baumann ,  Joe H. Satcher, Jr. ,  Michael Stadermann

    发明人： Marcus A. Worsley ,  Theodore F. Baumann ,  Joe H. Satcher, Jr. ,  Michael Stadermann

    IPC分类号： H01B1/18

    CPC分类号： H01B1/04 ,  B01J21/18 ,  B01J21/185 ,  B01J23/755 ,  B01J35/1028 ,  B01J37/0201 ,  B82Y30/00 ,  B82Y40/00 ,  C01B32/00 ,  C01B32/05 ,  C01B32/162 ,  C01B33/02 ,  C01B33/027 ,  C01B2202/06

    摘要： A composition comprising: at least one porous carbon monolith, such as a carbon aerogel, comprising internal pores, and at least one nanomaterial, such as carbon nanotubes, disposed uniformly throughout the internal pores. The nanomaterial can be disposed in the middle of the monolith. In addition, a method for making a monolithic solid with both high surface area and good bulk electrical conductivity is provided. A porous substrate having a thickness of 100 microns or more and comprising macropores throughout its thickness is prepared. At least one catalyst is deposited inside the porous substrate. Subsequently, chemical vapor deposition is used to uniformly deposit a nanomaterial in the macropores throughout the thickness of the porous substrate. Applications include electrical energy storage, such as batteries and capacitors, and hydrogen storage.

    摘要翻译： 一种组合物，其包括：至少一种多孔碳整料，例如包含内部孔的碳气凝胶，以及均匀地排列在整个内部孔中的至少一种纳米材料，例如碳纳米管。 纳米材料可以设置在整料的中间。 此外，提供了制造具有高表面积和良好体积导电性的整体式固体的方法。 制备厚度为100微米或更大并且在整个厚度上包含大孔的多孔基材。 至少一种催化剂沉积在多孔基材的内部。 随后，化学气相沉积用于在多孔基底的整个厚度上均匀地沉积在大孔中的纳米材料。 应用包括电能储存，如电池和电容器，以及氢气储存。