公开(公告)号：US20240351958A1

公开(公告)日：2024-10-24

申请号：US18302653

申请日：2023-04-18

Applicant: Honeywell International Inc.

Inventor： Mehrad Mehr ,  Bahram Jadidian

IPC: C04B41/45 ,  C04B35/83 ,  C04B38/00 ,  C04B41/50 ,  C04B41/87

CPC classification number: C04B41/4556 ,  C04B35/83 ,  C04B38/0058 ,  C04B38/0067 ,  C04B41/5059 ,  C04B41/5061 ,  C04B41/87 ,  C04B2235/422 ,  C04B2235/5248

Abstract: An article includes a substrate. The substrate includes at least two phases. The first phase includes a carbon-carbon (C/C) composite. The second phase includes a metal carbide. The second phase is disposed within a plurality of interconnected pores of the first phase, wherein the second phase extends from a surface of the substrate to a depth of at least 300 micrometers below the surface of the substrate.

公开(公告)号：US12024476B2

公开(公告)日：2024-07-02

申请号：US16797610

申请日：2020-02-21

Applicant: Honeywell International Inc.

Inventor： Bahram Jadidian ,  Richard George Rateick, Jr. ,  Mehrad Mehr ,  Donald Olson

IPC: B32B9/00 ,  C04B35/83 ,  C04B41/00 ,  C04B41/45 ,  C04B41/50 ,  C04B41/52 ,  C04B41/89 ,  F16D65/12 ,  F16D69/02 ,  B82Y30/00

CPC classification number: C04B41/5024 ,  C04B35/83 ,  C04B41/009 ,  C04B41/4515 ,  C04B41/4539 ,  C04B41/5059 ,  C04B41/5061 ,  C04B41/52 ,  C04B41/89 ,  F16D65/125 ,  F16D69/023 ,  B82Y30/00 ,  C04B2235/66 ,  C04B2235/9607 ,  C04B2235/9684 ,  Y10T428/30

Abstract: An article including carbon-carbon composite substrate may be treated with an antioxidant coating prior to use in an oxidizing environment. The antioxidant coating may be configured to reduce oxidation at an external surface of the C—C composition and reduce ingress of oxidants into pores or other open passages defined by the C—C composite substrate to avoid internal oxidation. An example article includes a C—C composite substrate, a bond coat, and an antioxidant coating. The C—C composite substrate defines a friction surface and a non-friction surface. The bond coat is disposed on the non-friction surface. The antioxidant coating may be disposed on at least a portion of the bond coat. The antioxidant coating may include ytterbium disilicate and a sintering aid.

公开(公告)号：US20170362130A1

公开(公告)日：2017-12-21

申请号：US15538604

申请日：2015-12-24

Applicant: TUNGALOY CORPORATION

Inventor： Yusuke HIRANO ,  Kentaro SHIRO

IPC: C04B35/5831 ,  C04B41/87 ,  B23B27/18 ,  C04B41/89 ,  C04B35/63 ,  C23C14/18

CPC classification number: C04B35/5831 ,  B23B27/14 ,  B23B27/18 ,  B23B27/20 ,  C04B35/119 ,  C04B35/6262 ,  C04B35/62685 ,  C04B35/6303 ,  C04B35/645 ,  C04B41/009 ,  C04B41/5063 ,  C04B41/5068 ,  C04B41/87 ,  C04B41/89 ,  C04B2235/3217 ,  C04B2235/3225 ,  C04B2235/3244 ,  C04B2235/3246 ,  C04B2235/3813 ,  C04B2235/3826 ,  C04B2235/3839 ,  C04B2235/386 ,  C04B2235/3865 ,  C04B2235/3886 ,  C04B2235/402 ,  C04B2235/5436 ,  C04B2235/6581 ,  C04B2235/785 ,  C04B2235/786 ,  C04B2235/80 ,  C23C14/18 ,  C04B41/4529 ,  C04B41/5061 ,  C04B41/5066 ,  C04B41/5062

Abstract: A cBN sintered body has 40%-85% cBN by volume and 15% to 60% binder phase by volume. and inevitable impurities. The binder phase has an Al compound including Al and at least one element selected from N, O and B, and a Zr compound including Zr and at least one element selected from C, N, O and B. The Zr compound includes ZrO, or ZrO and ZrO2. In an X-ray diffraction, where a peak intensity of a (111) plane of the ZrO is I1, a peak intensity of a (101) plane of tetragonal ZrO2 is I2t and a peak intensity of a (111) plane of cubic ZrO2 is I2c, a ratio of the intensity of I1 to total intensities of I1, I2t and I2c is 0.6-1.0, and an average grain size of the Al compound is 80 nm-300 nm.

公开(公告)号：US20160281240A1

公开(公告)日：2016-09-29

申请号：US15076593

申请日：2016-03-21

Applicant: KING FAHD UNIVERSITY OF PETROLEUM AND MINERALS

Inventor： BEKIR SAMI YILBAS ,  HAIDER ALI

IPC: C23C30/00

CPC classification number: C23C30/00 ,  B01J19/121 ,  B23K26/352 ,  C04B41/009 ,  C04B41/5001 ,  C04B41/5062 ,  C04B41/85 ,  C04B41/87 ,  C04B35/48 ,  C04B41/4535 ,  C04B41/4554 ,  C04B41/5058 ,  C04B41/5061 ,  C04B41/0036 ,  C04B41/4519 ,  C04B41/4558

Abstract: The method of laser treating an alumina surface includes applying a coating of a phenolic resin including particles of titanium carbide (TiC) and boron carbide (B4C) to an alumina (Al2O3) surface to form a resin-coated alumina surface, heating the resin-coated alumina surface to form a carbon-coated alumina surface, and scanning the carbon-coated alumina surface a nitrogen gas-assisted CO2 laser beam to form a laser-treated surface. The particles of titanium carbide (TiC) and boron carbide (B4C) each have a diameter of about 350 nm.

Abstract translation: 激光处理氧化铝表面的方法包括将包括碳化钛（TiC）和碳化硼（B4C）的颗粒的酚醛树脂的涂层施加到氧化铝（Al 2 O 3）表面上以形成树脂涂覆的氧化铝表面， 涂覆氧化铝表面以形成碳涂覆的氧化铝表面，并且将碳涂覆的氧化铝表面扫描氮气辅助CO 2激光束以形成经激光处理的表面。 碳化钛（TiC）和碳化硼（B4C）的颗粒各自具有约350nm的直径。

公开(公告)号：US20160068449A1

公开(公告)日：2016-03-10

申请号：US14784104

申请日：2014-11-25

Applicant: SUMITOMO ELECTRIC HARDMETAL CORP.

Inventor： Nozomi TSUKIHARA ,  Makoto SETOYAMA ,  Katsumi OKAMURA

IPC: C04B41/87 ,  C04B41/00 ,  C04B41/50

CPC classification number: C04B41/87 ,  C01B21/0648 ,  C01P2004/61 ,  C04B35/58014 ,  C04B35/581 ,  C04B35/5831 ,  C04B35/645 ,  C04B41/009 ,  C04B41/5062 ,  C04B41/5068 ,  C04B41/52 ,  C04B41/89 ,  C04B2235/3856 ,  C04B2235/386 ,  C04B2235/3865 ,  C04B2235/3886 ,  C04B2235/5436 ,  C04B2235/5445 ,  C23C30/005 ,  C04B41/4529 ,  C04B41/455 ,  C04B41/5063 ,  C04B41/5066 ,  C04B41/5061

Abstract: A cutting tool includes a base material and a coating formed on the base material. The base material is a sintered body containing 30 to 80% by volume of cubic boron nitride, and a binder. The surface in contact with the coating, of the base material, has a plurality of convex portions made of the cubic boron nitride and a plurality of concave portions made of the binder. A surface roughness Rsub of the surface in contact with the base material, is 0.1 to 0.4 μm. A surface roughness Rsurf of an outermost surface of the coating is 0 to 0.15 μm. A surface roughness Rasurf of the outermost surface of the coating is 0 to 0.1 μm. The surface roughness Rsub of the surface in contact with the coating, of the base material, is greater than the surface roughness Rsurf of the outermost surface of the coating.

Abstract translation: 切割工具包括基材和形成在基材上的涂层。 基材是含有30〜80体积％立方氮化硼的烧结体和粘合剂。 与基材的涂层接触的表面具有由立方氮化硼制成的多个凸部和由粘合剂制成的多个凹部。 与基材接触的表面的表面粗糙度Rsub为0.1〜0.4μm。 涂层的最外表面的表面粗糙度Rsurf为0〜0.15μm。 涂层最表面的表面粗糙度Rasurf为0〜0.1μm。 与基材的涂层接触的表面的表面粗糙度Rsub大于涂层的最外表面的表面粗糙度Rsurf。

公开(公告)号：US20160040279A1

公开(公告)日：2016-02-11

申请号：US14780169

申请日：2014-02-26

Applicant: SUMITOMO ELECTRIC HARDMETAL CORP.

Inventor： Makoto SETOYAMA ,  Katsumi OKAMURA ,  Nozomi TSUKIHARA

IPC: C23C14/06 ,  C23C28/04 ,  C23C28/00

CPC classification number: C23C14/0641 ,  B23C2226/12 ,  B23C2228/10 ,  C04B41/009 ,  C04B41/52 ,  C04B41/89 ,  C23C14/0664 ,  C23C28/042 ,  C23C28/044 ,  C23C28/42 ,  C04B35/5831 ,  C04B41/4529 ,  C04B41/5063 ,  C04B41/5068 ,  C04B41/5062 ,  C04B41/522 ,  C04B41/5066 ,  C04B41/5133 ,  C04B41/5061

Abstract: In a surface-coated boron nitride sintered body tool, at least a cutting edge portion contains a cubic boron nitride sintered body and a coating layer formed on a surface of the cubic boron nitride sintered body. A layer B of the coating layer is formed by alternately laminating one or more layers of each of two or more thin-film layers having different compositions. A B1 thin-film layer as one of the thin-film layers is formed by alternately laminating one or more layers of each of two or more compound layers having different compositions. Each of the compound layers has a thickness not less than 0.5 nm and less than 30 nm. A B2 thin-film layer as one of the thin-film layers different from the B1 thin-film layer has a thickness more than 30 nm and less than 200 nm.

Abstract translation: 在表面涂覆的氮化硼烧结体工具中，至少切削刃部包含立方氮化硼烧结体和在立方氮化硼烧结体的表面上形成的涂层。 通过交替层叠具有不同组成的两层或更多层薄膜层中的一层或多层来形成涂层B。 作为薄膜层之一的B1薄膜层通过交替层叠具有不同组成的两个或更多个化合物层中的每一个的一层或多层而形成。 每个化合物层的厚度不小于0.5nm且小于30nm。 作为与B1薄膜层不同的薄膜层之一的B2薄膜层的厚度大于30nm且小于200nm。

公开(公告)号：US20150321966A1

公开(公告)日：2015-11-12

申请号：US14652210

申请日：2014-01-28

Applicant: TOYO TANSO CO., LTD.

Inventor： Masato Shinohara

IPC: C04B41/89 ,  C04B35/52 ,  C04B41/50

CPC classification number: C04B41/89 ,  C04B35/522 ,  C04B41/00 ,  C04B41/009 ,  C04B41/4529 ,  C04B41/5059 ,  C04B41/5061 ,  C04B41/52 ,  C04B41/53 ,  C23C16/4581 ,  C30B29/36 ,  C30B35/00 ,  H01L21/683 ,  H01L21/68757 ,  Y10T428/24612 ,  Y10T428/265 ,  Y10T428/30 ,  C04B41/4531 ,  C04B41/4519 ,  C04B41/5001 ,  C04B41/5346 ,  C04B41/455 ,  C04B41/5057

Abstract: Provided is a silicon carbide-tantalum carbide composite having excellent durability. A silicon carbide-tantalum carbide composite (1) includes: a body (10) whose surface layer is at least partly formed of a first silicon carbide layer (12); a tantalum carbide layer (20); and a second silicon carbide layer (13). The tantalum carbide layer (20) is disposed over the first silicon carbide layer (12). The second silicon carbide layer (13) is interposed between the tantalum carbide layer (20) and the first silicon carbide layer (12). The second silicon carbide layer (13) has a C/Si composition ratio of not less than 1.2 as measured by X-ray photoelectron spectroscopy. The second silicon carbide layer (13) has a peak intensity ratio G/D of not less than 1.0 between the G-band and D-band of carbon as measured by Raman spectroscopy.

Abstract translation: 提供了具有优异的耐久性的碳化硅 - 碳化钽复合材料。 碳化硅 - 碳化钽复合材料（1）包括：其表面层至少部分地由第一碳化硅层（12）形成的主体（10）; 碳化钽层（20）; 和第二碳化硅层（13）。 碳化钽层（20）设置在第一碳化硅层（12）的上方。 第二碳化硅层（13）介于碳化钽层（20）和第一碳化硅层（12）之间。 通过X射线光电子能谱测定，第二碳化硅层（13）的C / Si组成比不小于1.2。 通过拉曼光谱测定，第二碳化硅层（13）的G带和D带之间的峰值强度比G / D不小于1.0。

公开(公告)号：US08999531B2

公开(公告)日：2015-04-07

申请号：US13639994

申请日：2011-04-15

Applicant: Takahide Kudoh ,  Naohiro Kagawa ,  Takashi Umemura

Inventor： Takahide Kudoh ,  Naohiro Kagawa ,  Takashi Umemura

IPC: C04B41/00 ,  C22C26/00 ,  C04B35/5831 ,  C04B35/63 ,  C04B41/45 ,  C04B41/81 ,  B22F7/02

CPC classification number: C22C26/00 ,  B22F7/02 ,  C04B35/5831 ,  C04B35/6261 ,  C04B35/62675 ,  C04B35/62685 ,  C04B35/6303 ,  C04B35/645 ,  C04B37/026 ,  C04B41/009 ,  C04B41/4529 ,  C04B41/81 ,  C04B2235/3217 ,  C04B2235/3804 ,  C04B2235/3813 ,  C04B2235/3843 ,  C04B2235/3847 ,  C04B2235/3852 ,  C04B2235/3856 ,  C04B2235/3865 ,  C04B2235/3886 ,  C04B2235/402 ,  C04B2235/5436 ,  C04B2235/5445 ,  C04B2235/5472 ,  C04B2235/72 ,  C04B2235/785 ,  C04B2235/786 ,  C04B2235/80 ,  C04B2235/85 ,  C04B2235/96 ,  C04B2235/9607 ,  C04B2237/361 ,  C04B2237/401 ,  C22C2026/003 ,  Y10T428/24975 ,  Y10T428/25 ,  Y10T428/265 ,  C04B41/5061 ,  C04B41/5068 ,  C04B41/5062 ,  C04B41/5063 ,  C04B41/5066

Abstract: A coated cBN sintered body has excellent wear resistance, fracture resistance, adhesiveness between a substrate and a coating, and a tool life of which is elongated as compared with conventional cBN sintered bodies. The coated cBN sintered body has a cBN sintered body substrate and a coating coated on the surface thereof. The cBN sintered body includes 76 to 90% by volume of cBN, and 10 to 24% by volume of a binder phase and inevitable impurities. An average grain size of cBN is 0.5 to 5.0 μm, an average value of the thickness of the binder phase is 0.05 to 0.8 μm, and the standard deviation of the thickness of the binder phase is 0.8 μm or less.

Abstract translation: 涂布的cBN烧结体与传统的cBN烧结体相比具有优异的耐磨性，耐断裂性，基材与涂层之间的粘合性，并且其寿命延长。 涂布的cBN烧结体具有cBN烧结体基材和涂布在其表面上的涂层。 cBN烧结体包含76〜90体积％的cBN，10〜24体积％的粘结相和不可避免的杂质。 cBN的平均粒径为0.5〜5.0μm，粘结相的厚度的平均值为0.05〜0.8μm，粘结相的厚度的标准偏差为0.8μm以下。

公开(公告)号：US20130260035A1

公开(公告)日：2013-10-03

申请号：US13908085

申请日：2013-06-03

Applicant: Kennametal Inc.

Inventor： Zhigang Ban ,  Alfred S. Gates, JR. ,  Yixiong Liu ,  Jie Wu

IPC: B23B27/14

CPC classification number: B23B27/148 ,  B23B27/141 ,  B23B2226/18 ,  B23B2228/10 ,  B23B2260/144 ,  C04B41/009 ,  C04B41/52 ,  C04B41/89 ,  C23C28/044 ,  C23C28/42 ,  C23C30/005 ,  Y10T407/27 ,  C04B35/584 ,  C04B35/597 ,  C04B41/4531 ,  C04B41/5031 ,  C04B41/459 ,  C04B41/5061 ,  C04B41/5068

Abstract: A coated ceramic cutting insert for removing material from a workpiece, as well as a method for making the same, that includes a ceramic substrate with a rake surface and at least one flank surface wherein a cutting edge is at the juncture therebetween. A wear-resistant coating scheme that includes an alumina-containing base coating layer region, which has at least one exposed alumina coating layer, deposited by chemical vapor deposition on the substantially all of the surfaces of the ceramic substrate that experience wear during removal of material from the workpiece. The exposed alumina coating layer exhibits a blasted stress condition ranging between about 50 MPa (tensile stress) and about −2 GPa (compressive) as measured by XRD using the Psi tilt method and the (024) reflection of alumina. The exposed alumina coating layer is the result of wet blasting a titanium-containing outer coating layer region from the surface of the alumina-containing base coating layer region.

Abstract translation: 一种用于从工件去除材料的涂覆陶瓷切削刀片及其制造方法，其包括具有前刀面和至少一个侧面的陶瓷基体，其中切削刃处于它们之间的接合处。 一种耐磨涂层方案，其包括含氧化铝的基底涂层区域，其具有至少一个暴露的氧化铝涂层，其通过化学气相沉积沉积在陶瓷基底的基本上所有的表面上，在去除材料期间经历磨损 从工件。 暴露的氧化铝涂层表现出通过使用Psi倾斜法和氧化铝的（024）反射通过XRD测量的约50MPa（拉伸应力）和约-2GPa（压缩）之间的喷砂应力条件。 暴露的氧化铝涂层是从含氧化铝的基底涂层区域的表面湿式喷射含钛外涂层区域的结果。

公开(公告)号：US08147992B2

公开(公告)日：2012-04-03

申请号：US12400007

申请日：2009-03-09

Applicant: X. Daniel Fang ,  David J. Wills ,  Gilles Festeau

Inventor： X. Daniel Fang ,  David J. Wills ,  Gilles Festeau

IPC: B32B9/00

CPC classification number: C04B41/009 ,  C04B41/52 ,  C04B41/89 ,  C23C8/02 ,  C23C10/02 ,  C23C12/02 ,  C23C30/005 ,  Y10T407/25 ,  Y10T407/27 ,  Y10T428/24975 ,  Y10T428/265 ,  C04B41/4531 ,  C04B41/5063 ,  C04B41/5068 ,  C04B41/5061 ,  C04B41/524 ,  C04B35/117 ,  C04B35/119

Abstract: The present invention relates to ceramic cutting tools, such as, an aluminum oxide with zirconium oxide ceramic cutting tool with diffusion bonding enhanced layer and CVD coatings, particularly useful for machining modern metal materials. The method comprises a chemical reaction with a mixture including nitrogen and aluminum chloride introduced to form a diffusion bonding enhanced layer between the ceramic substrate and the CVD coatings. Thus formed diffusion bonding enhanced layer is highly adherent to the aluminum oxide with zirconium oxide ceramic substrate and significantly enhances the CVD coating properties, thus improving the machining performance in terms of the tool life of zirconium-based aluminum oxide with zirconium oxide ceramic cutting tools.

Abstract translation: 本发明涉及陶瓷切割工具，例如具有扩散粘合增强层的氧化锆陶瓷切割工具和CVD涂层的特别适用于加工现代金属材料的氧化铝。 该方法包括与引入的氮和氯化铝的混合物的化学反应，以在陶瓷基板和CVD涂层之间形成扩散结合增强层。 由此形成的扩散接合增强层与氧化锆陶瓷基体对氧化铝具有高附着性，并显着提高了CVD涂层性能，从而提高了锆基氧化铝与氧化锆陶瓷切割工具的工具寿命方面的加工性能。