SURFACE-MODIFIED NANODIAMONDS AND METHOD FOR PRODUCING SURFACE-MODIFIED NANO CARBON PARTICLES

    公开(公告)号:US20240116762A1

    公开(公告)日:2024-04-11

    申请号:US18503620

    申请日:2023-11-07

    IPC分类号: C01B32/28 C09C1/44 C09C3/08

    摘要: Provided is a surface-modified nanodiamond having excellent dispersibility in an organic solvent, and a method capable of introducing various surface-modifying groups and easily producing surface-modified nanocarbon particles with little zirconia contamination. The surface-modified nanodiamond includes nanodiamond particles and a group that surface-modifies the nanodiamond particles and is represented by Formula (1): —X—R1 (1) [where X represents —NH—, —O—, —O—C(═O)—, —C(═O)—O—, —NH—C(═O)—, —C(═O)—NH—, or —S—; the bond extending left from X is bonded to a nanodiamond particle; R1 represents a monovalent organic group that does not have a hydroxy group, carboxy group, amino group, mono-substituted amino group, terminal alkenyl group, and terminal epoxy group; an atom bound to X is a carbon atom; and a molar ratio of carbon atoms to the total amount of heteroatoms selected from the group consisting of nitrogen atoms, oxygen atoms, sulfur atoms, and silicon atoms is 4.5 or greater.

    NANO-REINFORCEMENT FILLER MATERIAL FOR EPOXY RESIN SYSTEMS AND METHODS OF MAKING THE SAME

    公开(公告)号:US20180312647A1

    公开(公告)日:2018-11-01

    申请号:US15582475

    申请日:2017-04-28

    IPC分类号: C08J5/00 C09C1/44 C09C3/10

    摘要: A method of making a nano-reinforcement filler material for an epoxy resin system for a composite structure is provided. The method includes forming a polymer suspension of polymer nanoparticles suspended in deionized (DI) water, and sonicating the polymer suspension. The method includes forming a graphene oxide (GO) suspension of GO sheets suspended in DI water, and sonicating the GO suspension. The method includes mixing the sonicated polymer suspension and the sonicated GO suspension to obtain a sonicated mixture. The method includes heating the sonicated mixture in an inert atmosphere at an effective temperature, and using an electrostatic process to uniformly wrap individual polymer nanoparticles with individual GO sheets, via an electrostatic interaction reaction, to obtain the nano-reinforcement filler material comprising polymer-GO core-shell nanoparticles. The method includes washing and drying the nano-reinforcement filler material, and using it in the epoxy resin system for the composite structure.