公开(公告)号：US20140170055A1

公开(公告)日：2014-06-19

申请号：US14235758

申请日：2012-07-26

Applicant: Kazuhiro Ikeda ,  Keiko Arimoto ,  Katsuko Yamamoto ,  Hitoshi Sumiya

Inventor： Kazuhiro Ikeda ,  Keiko Arimoto ,  Katsuko Yamamoto ,  Hitoshi Sumiya

IPC: C01B31/06

CPC classification number: C01B32/25 ,  B01J3/062 ,  B01J2203/061 ,  B01J2203/0655

Abstract: Nano polycrystalline diamond is composed of carbon and a plurality of impurities other than carbon. A concentration of each of the plurality of impurities is not higher than 0.01 mass %, and the nano polycrystalline diamond has a crystal grain size (a maximum length) not greater than 500 nm. The nano polycrystalline diamond can be fabricated by preparing graphite in which a concentration of an impurity is not higher than 0.01 mass % and converting graphite to diamond by applying an ultra-high pressure and a high temperature to graphite.

Abstract translation: 纳米多晶金刚石由碳和除碳以外的多种杂质组成。 多个杂质的浓度不高于0.01质量％，纳米多晶金刚石的结晶粒径（最大长度）不大于500nm。 可以通过制备其中杂质浓度不高于0.01质量％的石墨并通过对石墨施加超高压和高温将石墨转化为金刚石来制造纳米多晶金刚石。

公开(公告)号：US20130199107A1

公开(公告)日：2013-08-08

申请号：US13641390

申请日：2011-04-20

Applicant: Robert Fries

Inventor： Robert Fries

IPC: B24D3/34

CPC classification number: B24D3/348 ,  B01J3/062 ,  B01J2203/061 ,  B01J2203/062 ,  B01J2203/0645 ,  B01J2203/0655 ,  B01J2203/066 ,  B01J2203/0685 ,  B22F2998/10 ,  C22C1/051 ,  C22C26/00 ,  E21B10/567 ,  C22C1/05 ,  C25D15/00 ,  B22F3/14

Abstract: A polycrystalline superhard material comprises a sintered mass of superhard grains having a mean superhard grain contiguity of at least 62 percent and at most 92 percent. There is also disclosed a method of making such a polycrystalline superhard material. The method comprises providing a precursor body comprising superhard grains and interstices between the superhard grains, and introducing additive particles into the interstices to form a pre-sinter body. The pre-sinter body is submitted to a temperature and pressure at which superhard material is thermodynamically stable, sintering it and forming polycrystalline superhard material.

Abstract translation: 多晶超硬材料包括具有至少62％且至多92％的平均超硬颗粒接近度的超硬颗粒的烧结块。 还公开了制造这种多晶超硬材料的方法。 该方法包括提供包含超硬颗粒和超硬颗粒之间的间隙的前体体，并将添加剂颗粒引入到间隙中以形成预烧结体。 预烧结体承受超硬材料在热力学上稳定的温度和压力，烧结并形成多晶超硬材料。

公开(公告)号：US20120260582A1

公开(公告)日：2012-10-18

申请号：US13416201

申请日：2012-03-09

Applicant: Chien-Min Sung

Inventor： Chien-Min Sung

IPC: B24D3/06

CPC classification number: B24D18/0009 ,  B01J3/062 ,  B01J2203/061 ,  B01J2203/062 ,  B01J2203/0645 ,  B01J2203/0655 ,  B01J2203/066 ,  B01J2203/068 ,  B24D3/06 ,  B24D18/0027 ,  B28D1/121 ,  B28D1/127

Abstract: Superabrasive tools and methods for the making thereof are disclosed and described. In one aspect, superabrasive particles are chemically bonded to a matrix support material according to a predetermined pattern by a braze alloy. The brazing alloy may be provided as a powder, thin sheet, or sheet of amorphous alloy. A template having a plurality of apertures arranged in a predetermined pattern may be used to place the superabrasive particles on a given substrate or matrix support material.

Abstract translation: 公开和描述了超研磨工具及其制造方法。 在一个方面，超磨料颗粒通过钎焊合金根据预定图案化学键合到基质载体材料上。 钎焊合金可以提供为粉末，薄片或非晶合金片。 可以使用具有以预定图案布置的多个孔的模板来将超研磨颗粒放置在给定的基底或基质支撑材料上。

公开(公告)号：US20110293905A1

公开(公告)日：2011-12-01

申请号：US13113779

申请日：2011-05-23

Applicant: Chien-Min Sung

Inventor： Chien-Min Sung

IPC: B24D3/06 ,  B32B5/16 ,  C09K3/14

CPC classification number: B24B53/017 ,  B01J3/062 ,  B01J2203/061 ,  B01J2203/062 ,  B01J2203/0645 ,  B01J2203/0655 ,  B01J2203/066 ,  B01J2203/068 ,  B24B53/02 ,  B24D3/06 ,  B24D11/005 ,  Y10T428/24893

Abstract: A superabrasive tools having uniformly leveled superabrasive particles and associated methods are provided. In one aspect, for example, a superabrasive can include a metal matrix configured for bonding superabrasive particles and a plurality superabrasive particles held in the metal matrix at specific positions according to a predetermined pattern, wherein tips of each of the plurality of the superabrasive particles protrude from the metal matrix to a uniform height.

Abstract translation: 提供了具有均匀平整的超研磨颗粒和相关方法的超级磨料工具。 一方面，例如，超级磨料可以包括金属基体，其被配置为根据预定图案将超研磨颗粒和保持在金属基体中的多个超研磨颗粒结合到特定位置，其中多个超级磨料颗粒中的每一个的尖端突出 从金属基体到均匀的高度。

公开(公告)号：US20110271900A1

公开(公告)日：2011-11-10

申请号：US13144512

申请日：2010-01-15

Applicant: Raymond Anthony Spits ,  Carlton Nigel Dodge

Inventor： Raymond Anthony Spits ,  Carlton Nigel Dodge

IPC: C30B9/10 ,  C30B29/04

CPC classification number: C30B29/04 ,  B01J3/062 ,  B01J23/745 ,  B01J23/75 ,  B01J23/755 ,  B01J2203/061 ,  B01J2203/062 ,  B01J2203/0655 ,  B01J2203/068

Abstract: A high pressure high temperature (HPHT) method for synthesizing single crystal diamond, wherein a single crystal diamond seed having an aspect ratio of at least (1) and a growth surface substantially parallel to a {110} crystallographic plane is utilised is described. The growth is effected at a temperature in the range from 1280° C. to 1390° C.

Abstract translation: 描述了用于合成单晶金刚石的高压高温（HPHT）方法，其中使用具有至少（1）的纵横比和基本上平行于{110}晶面的生长表面的单晶金刚石晶种。 生长在1280℃至1390℃的温度下进行。

公开(公告)号：US20100028246A1

公开(公告)日：2010-02-04

申请号：US11721394

申请日：2004-12-09

Applicant: Corina Vera Helga Stromann ,  Francis Tshisikhawe ,  John Olaf Hansen ,  Robert Charles Burns

Inventor： Corina Vera Helga Stromann ,  Francis Tshisikhawe ,  John Olaf Hansen ,  Robert Charles Burns

IPC: C01B31/06

CPC classification number: B01J3/062 ,  B01J2203/061 ,  B01J2203/062 ,  B01J2203/0655 ,  B01J2203/068 ,  C01B32/25

Abstract: In a method of synthesising diamond, a reaction mixture of a carbon source and a solvent/catalyst is pretreated at a high temperature and a high vacuum to remove substantially all of the atmospheric gases and other light volatile atoms. Then, at a reduced temperature, the removed gas is replaced with a desirable process gas. The pre-treated reaction mixture is then subjected to elevated temperature and pressure conditions in the diamond stable region of the carbon phase diagram in the presence of the process gas to produce the diamond. The process gas is selected to enhance the diamond growth rate, reduce solvent/catalyst inclusions, shift the morphology of the synthesised diamond (grown crystals) towards major crystal faces and blocker shape, reduce cracking and strain in the grown crystals, preferably at a desirably high growth rate, and permit the controlled and uniform doping of the diamond crystal with a hetero-atom such as P (phosphorus) or S (sulphur).

Abstract translation: 在合成金刚石的方法中，碳源和溶剂/催化剂的反应混合物在高温和高真空下预处理以除去基本上所有的大气气体和其它轻挥发性原子。 然后，在降低的温度下，用所需的处理气体代替去除的气体。 然后将预处理的反应混合物在工艺气体存在下在碳相图的金刚石稳定区域中进行升高的温度和压力条件以制备金刚石。 选择工艺气体以增加金刚石生长速率，减少溶剂/催化剂夹杂物，将合成的金刚石（生长晶体）的形态转移到主晶面和阻挡体形状，减少生长晶体中的开裂和应变，优选理想的 并且允许用诸如P（磷）或S（硫）的杂原子控制和均匀掺杂金刚石晶体。

公开(公告)号：US20080219914A1

公开(公告)日：2008-09-11

申请号：US11916148

申请日：2006-05-26

Applicant: Clint Guy Smallman ,  Geoffrey John Davies ,  Johannes Lodewikus Myburgh

Inventor： Clint Guy Smallman ,  Geoffrey John Davies ,  Johannes Lodewikus Myburgh

IPC: C01B31/06 ,  B01J3/06

CPC classification number: B01J3/062 ,  B01J2203/061 ,  B01J2203/062 ,  B01J2203/0655 ,  B01J2203/068

Abstract: The invention relates to a method for manufacture of diamond, the method including the steps of providing a first coating of solvent metal or solvent metal alloy on a diamond seed to create a coated diamond seed, situating the coated diamond seed adjacent a catalyst system comprising a solvent metal and/or a source of carbon, and subjecting the coated diamond seed and catalyst system to increased temperature wherein the melting point of the first coating is at least 20 deg C. below that of the catalyst system. The invention further relates to a compact comprising a plurality of diamond seeds wherein at least one seed includes a first coating comprising a solvent metal and/or solvent metal based alloy, the compact further comprising a catalyst system comprising a solvent metal and/or a source of carbon wherein the melting point of the first coating is at least 20 deg C. below that of the catalyst system.

Abstract translation: 本发明涉及一种用于制造金刚石的方法，该方法包括以下步骤：在金刚石种子上提供溶剂金属或溶剂金属合金的第一涂层以产生涂覆的金刚石晶种，将涂覆的金刚石晶粒定位在催化剂体系附近，该催化剂体系包含 溶剂金属和/或碳源，并且使经涂覆的金刚石晶种和催化剂体系升温，其中第一涂层的熔点低于催化剂体系的熔点至少20℃。 本发明还涉及包含多个金刚石种子的压块，其中至少一种种子包括包含溶剂金属和/或溶剂金属基合金的第一涂层，该压块还包括包含溶剂金属和/或源的催化剂体系 的碳，其中第一涂层的熔点低于催化剂体系的熔点至少20℃。

公开(公告)号：US20060016127A1

公开(公告)日：2006-01-26

申请号：US11175017

申请日：2005-07-05

Applicant: Chien-Min Sung

Inventor： Chien-Min Sung

IPC: B24D18/00

CPC classification number: B01J3/062 ,  B01J2203/061 ,  B01J2203/062 ,  B01J2203/0625 ,  B01J2203/0645 ,  B01J2203/0655 ,  B01J2203/066 ,  B01J2203/068 ,  B01J2203/0685 ,  B22F2005/001 ,  B22F2999/00 ,  B23D61/18 ,  B23D65/00 ,  B23P15/28 ,  B24D3/08 ,  B24D7/066 ,  B24D18/00 ,  B24D99/005 ,  B24D2203/00 ,  C04B35/52 ,  C09K3/1409 ,  C09K3/1445 ,  C22C1/051 ,  C22C26/00 ,  C22C2204/00 ,  E21B10/5676 ,  Y10T428/2991 ,  B22F2207/03 ,  B22F1/0011 ,  B22F3/004 ,  B22F2003/1046

Abstract: An improved method for synthesizing superabrasive particles provides high quality industrial superabrasive particles with high yield and a narrow size distribution. The synthesis method can include forming a growth precursor of a substantially homogeneous mixture of raw material and catalyst material or layers of raw material and metal catalyst. The growth precursor can have a layer of adhesive over at least a portion thereof. A plurality of crystalline seeds can be placed in a predetermined pattern on the layer of adhesive. The growth precursor can be maintained at a temperature and pressure at which the superabrasive crystal is thermodynamically stable for a time sufficient for a desired degree of growth. Advantageously, the patterned placement of crystalline seeds and disclosed processes allow for production of various morphologies of synthetic diamonds, including octahedral and cubic diamonds, and improved growth conditions generally. As a result, the grown superabrasive particles typically have a high yield of high quality particles and a narrow distribution of particle sizes.

Abstract translation: 合成超级磨料颗粒的改进方法提供高产率和窄尺寸分布的高质量工业超研磨颗粒。 合成方法可以包括形成原料和催化剂材料或原料和金属催化剂层的基本上均匀的混合物的生长前体。 生长前体可在其至少一部分上具有一层粘合剂。 多个结晶种子可以以预定图案放置在粘合剂层上。 生长前体可以保持在超磨料晶体在热力学稳定的温度和压力下达足以达到所需生长程度的时间。 有利地，结晶晶种的图案化布置和所公开的方法允许生产合成金刚石的各种形态，包括八面体和立方晶体，以及通常改善的生长条件。 结果，生长的超级磨料颗粒通常具有高产率的高质量颗粒和窄的粒度分布。

公开(公告)号：US20040031434A1

公开(公告)日：2004-02-19

申请号：US10643330

申请日：2003-08-19

Inventor： Russell P. VandenBiesen ,  Gregory R. Herro ,  Dean T. VandenBiesen

IPC: C30B033/06

CPC classification number: B01J3/065 ,  B01J2203/061 ,  B01J2203/0655 ,  B01J2203/068 ,  C30B23/00 ,  C30B29/04

Abstract: This invention is a method of making a synthetic gem comprising elements recovered from remains of a species of the Kingdom Animalia, comprising the steps of collecting substantially pure carbon from the remains and creating gems from the carbon using crystal growth sublimation.

Abstract translation: 本发明是一种制备合成宝石的方法，其包括从动物界的种类的残余物回收的元素，其包括以下步骤：从残余物中收集基本上纯的碳，并使用晶体生长升华从碳中产生宝石。

公开(公告)号：US06616725B2

公开(公告)日：2003-09-09

申请号：US09934459

申请日：2001-08-21

Applicant: Hyun Sam Cho ,  John Chen ,  Kyung Yul Han

Inventor： Hyun Sam Cho ,  John Chen ,  Kyung Yul Han

IPC: B24D300

CPC classification number: B22F1/025 ,  B01J3/062 ,  B01J2203/061 ,  B01J2203/062 ,  B01J2203/063 ,  B01J2203/0635 ,  B01J2203/0645 ,  B01J2203/0655 ,  B01J2203/066 ,  B01J2203/068 ,  C04B35/52 ,  C04B35/5626 ,  C04B35/5831 ,  C04B35/6303 ,  C04B35/645 ,  C04B2235/386 ,  C04B2235/402 ,  C04B2235/404 ,  C04B2235/405 ,  C04B2235/427 ,  C04B2235/428 ,  C04B2235/5276 ,  C04B2235/528 ,  C04B2235/5436 ,  Y10T428/30

Abstract: A self-grown monopoly compact grit and high pressure, high temperature process for preparing the same. The high pressure, high temperature sintered/synthesized monopoly compact grit is used in various industrial tools such as saw blades, grinding wheels, cutting tools and drill bits. Further, the monopoly compact grit of the present invention is produced from a seed of a mono-crystal of diamond or cubic boron nitride surrounded by either a self-grown crystal layer or an integrally bonded poly-crystalline sintered compact layer. The self-grown crystal layer is a new grown crystal structure where the seed crystal grows into a new phase through a normal diamond or cubic boron nitride synthesis process in the presence of a catalyst metal solvent. The compact layer is composed of about 50 to about 90 volume percent of diamond or cubic boron nitride, a typical binder material, which is a catalyst for crystal-to-crystal bonding, and a cementing agent which is a binding agent capable of forming stable carbide and nitride bonds.

Abstract translation: 自生成垄断的紧凑砂砾和高压，高温工艺制备相同。 高压，高温烧结/合成的垄断压实砂砾用于各种工业工具，如锯片，砂轮，切削工具和钻头。 此外，本发明的垄断压块砂砾由金刚石或立方氮化硼的单晶种子生产，其由自生长晶体层或整体结合的多晶烧结致密层包围。 自生晶体层是新生长的晶体结构，其中晶种在催化剂金属溶剂存在下通过正常的金刚石或立方氮化硼合成工艺生长成新相。 致密层由约50至约90体积％的金刚石或立方氮化硼组成，典型的粘合剂材料是用于晶体 - 晶体结合的催化剂，和作为能够形成稳定的粘合剂的粘合剂 碳化物和氮化物键。