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    Method of forming a multilayer coating on a substrate with an aqueous based coating composition having improved metallic pigment orientation
    21.
    发明授权
    Method of forming a multilayer coating on a substrate with an aqueous based coating composition having improved metallic pigment orientation 失效
    在具有改进的金属颜料取向的含水基涂料组合物的基材上形成多层涂层的方法

    公开(公告)号：US5510148A

    公开(公告)日：1996-04-23

    申请号：US236055

    申请日：1994-05-02

    申请人： Dennis Taljan ,  James E. Poole ,  Marvis E. Hartman

    发明人： Dennis Taljan ,  James E. Poole ,  Marvis E. Hartman

    IPC分类号： C08K5/101 ,  C08F283/00 ,  C08K5/10 ,  C09D5/00 ,  C09D5/02 ,  C09D5/38 ,  C09D201/00 ,  C09D201/06 ,  B05D7/14

    CPC分类号： C08F283/008 ,  C09D5/024 ,  C09D5/38

    摘要： A method of forming a multilayer coating on a substrate utilizes a pigmented aqueous based coating composition. The aqueous based coating composition contains a polymeric film-forming resin and as an additive from about 1 to about 40 percent by weight based on the resin solids of the composition of an oligomeric ester having an acid value of from about 100 to about 500 of the structure: ##STR1## where X is the residue of a polyol containing from 1 to 50 carbon atoms per hydroxyl group after reaction with an acid or an anhydride, R is an organic moiety from the acid or anhydride and A has an average value of about 2 or greater. The coating compositions are particularly advantageous as metallic pigmented coating compositions for automotive basecoat applications because they exhibit excellent resistance to mottling, have good flop and have reduced sensitivity to fluctuations in relative humidity.

    摘要翻译： 在基材上形成多层涂层的方法使用着色的水基涂料组合物。 水基涂料组合物含有聚合物成膜树脂和约1至约40重量％的添加剂，基于组合物的树脂固体的低聚酯，其酸值为约100至约500的酸值 结构：其中X是与酸或酸酐反应后，每个羟基含有1至50个碳原子的多元醇的残基，R是酸或酸酐的有机部分，A的平均值约为 2以上。 涂料组合物作为用于汽车底涂层应用的金属着色涂料组合物是特别有利的，因为它们表现出优异的斑驳性，具有良好的翻转性并且降低了对相对湿度波动的敏感性。

    Use of polymeric quaternary ammonium hydroxides in electrodeposition
    23.
    发明授权
    Use of polymeric quaternary ammonium hydroxides in electrodeposition 失效
    聚合季铵氢氧化物在电沉积中的应用

    公开(公告)号：US4081341A

    公开(公告)日：1978-03-28

    申请号：US744532

    申请日：1976-11-24

    申请人： Roger M. Christenson ,  Joseph F. Bosso ,  Marvis E. Hartman ,  Wen-Hsuan Chang

    发明人： Roger M. Christenson ,  Joseph F. Bosso ,  Marvis E. Hartman ,  Wen-Hsuan Chang

    IPC分类号： C08G59/00 ,  C08G59/14 ,  C09D5/44 ,  C09D163/00 ,  C09D175/00 ,  C25D13/22 ,  C25D13/10 ,  C25D13/24

    CPC分类号： C09D5/4473

    摘要： Quaternary ammonium hydroxide-containing polymers and their use in cationic electrodeposition are disclosed. The quaternary ammonium hydroxide-containing polymers are particularly useful as feed resins for controlling the pH of aqueous dispersions of acidified cationic resins used in electrodeposition. Upon electrodeposition, such resins generate acid which can build up to undesirable levels in the electrodeposition bath. The quaternary ammonium hydroxide-containing polymers are strong bases and when fed into the bath react with the acid to form the corresponding quaternary ammonium salt. This controls the pH of the bath at acceptable levels and provides additional cationic resin for electrodeposition. Utilizing the invention in this manner minimizes the need for controlling acid build-up in the electrodeposition bath by conventional techniques such as by treating the bath with ultrafiltration or electrodialysis.The quaternary ammonium hydroxide-containing polymers are also useful as electrodeposition resins themselves in that they electrodeposit without generating acid counter ion.

    摘要翻译： 公开了含季铵氢氧化物的聚合物及其在阳离子电沉积中的用途。 含季铵氢氧化物的聚合物特别可用作用于控制用于电沉积的酸化阳离子树脂的水性分散体的pH的进料树脂。 电沉积后，这种树脂产生的酸可以在电沉积浴中产生不希望的水平。 含氢氧化季铵的聚合物是强碱，当进入浴时与酸反应形成相应的季铵盐。 这将浴的pH控制在可接受的水平，并提供额外的阳离子树脂用于电沉积。 以这种方式利用本发明使通过常规技术例如通过用超滤或电渗析处理浴来控制电沉积浴中的酸积累的需要最小化。

    Ambient temperature, moisture-curable acrylic-silane coating compositions having improved potlife
    24.
    发明授权
    Ambient temperature, moisture-curable acrylic-silane coating compositions having improved potlife 失效
    环境温度，湿气固化丙烯酸 - 硅烷涂料组合物具有改善的适用期

    公开(公告)号：US4043953A

    公开(公告)日：1977-08-23

    申请号：US574194

    申请日：1975-05-02

    申请人： Wen-Hsuan Chang ,  Marvis E. Hartman ,  Roger L. Scriven

    发明人： Wen-Hsuan Chang ,  Marvis E. Hartman ,  Roger L. Scriven

    IPC分类号： C08K5/5415 ,  C09D143/04 ,  C08L91/00

    CPC分类号： C09D143/04 ,  C08K5/54 ,  C08K5/5415

    摘要： The potlife of an ambient temperature, moisture-curable coating composition comprising an acrylic-silane interpolymer and a cure-accelerating catalyst is increased by the addition to the composition of from about 0.5 percent to about 15 percent by weight of interpolymer solids of a monomeric hydrolytically reactive organo-silicon compound represented by the structural formula:X.sub.n Si(OR).sub.4-nwherein X is an organic radical having from 1 to 12 carbon atoms, R is methyl, ethyl, 2-methoxyethyl, 2-ethoxyethyl, or an acyl group containing 5 or less carbon atoms and n is 0, 1 or 2.

    摘要翻译： 包含丙烯酸 - 硅烷互聚物和固化促进催化剂的环境温度，湿气可固化涂料组合物的适用期通过加入组合物中增加约0.5重量％至约15重量％的单体水解的互聚物固体 由结构式表示的反应性有机硅化合物：

    Acid or anhydride grafted chlorinated polyolefin reacted with monoalcohol and polyepoxide
    25.
    发明授权
    Acid or anhydride grafted chlorinated polyolefin reacted with monoalcohol and polyepoxide 失效
    酸或酸酐接枝的氯化聚烯烃与一元醇和聚环氧化物反应

    公开(公告)号：US4997882A

    公开(公告)日：1991-03-05

    申请号：US376441

    申请日：1989-07-07

    申请人： Jonathan T. Martz ,  James B. O'Dwyer ,  Marvis E. Hartman

    发明人： Jonathan T. Martz ,  James B. O'Dwyer ,  Marvis E. Hartman

    IPC分类号： B05D3/10 ,  B05D7/02 ,  C08F8/14 ,  C08G59/14 ,  C08J7/04 ,  C09D163/00

    CPC分类号： C08J7/047 ,  C08F8/14 ,  C08J2323/02 ,  C08J2451/00

    摘要： Disclosed is an ungelled, modified chlorinated polyolefin resin suitable for providing a highly adherent, solvent resistant film on a thermoplastic polyolefin substrate. The modified chlorinated polyolefin resin is prepared by grafting an unsaturated polycarboxylic acid and/or an unsaturated acid anhydride onto a chlorinated polyolefin resin to form an acid- and/or anhydride-modified chlorinated polyolefin resin. The resulting acid- and/or anhydride-modified chlorinated polyolefin resin is reacted with an organic monohydric alcohol to form an esterified product containing acid functionality. The resulting esterified product is reacted with a polyepoxide to form the ungelled modified chlorinated polyolefin resin.Also disclosed is a method of preparing an ungelled modified chlorinated polyolefin resin of the invention, a coating composition containing a resin of the invention, and a method of forming a hardened film from the coating composition on a thermoplastic polyolefin substrate.

    摘要翻译： 公开了一种未凝胶化的改性氯化聚烯烃树脂，其适于在热塑性聚烯烃基材上提供高粘附性，耐溶剂性的膜。 通过将不饱和多羧酸和/或不饱和酸酐接枝到氯化聚烯烃树脂上以形成酸和/或酸酐改性的氯化聚烯烃树脂来制备改性氯化聚烯烃树脂。 将所得酸和/或酸酐改性的氯化聚烯烃树脂与有机一元醇反应形成含有酸官能团的酯化产物。 所得酯化产物与聚环氧化物反应形成未凝胶化的改性氯化聚烯烃树脂。 还公开了制备本发明的未凝胶化改性氯化聚烯烃树脂的方法，含有本发明树脂的涂料组合物和在热塑性聚烯烃基材上由涂料组合物形成硬化膜的方法。

    Adhesion promoters containing optical brightener
    26.
    发明授权
    Adhesion promoters containing optical brightener 失效
    含荧光增白剂的粘合促进剂

    公开(公告)号：US4741860A

    公开(公告)日：1988-05-03

    申请号：US914434

    申请日：1986-10-02

    申请人： Marvis E. Hartman

    发明人： Marvis E. Hartman

    IPC分类号： C08K5/00 ,  C08K5/35 ,  C09D123/28 ,  C08K5/34 ,  C09K11/06

    CPC分类号： C08K5/35 ,  C08K5/0041 ,  C09D123/28

    摘要： A composition comprising a chlorinated polyolefin and an optical brightener is disclosed. The compositions are useful as detectable adhesion promoters for polyolefin substrates. The compositions are applied as a coating to the polyolefin substrate and the coated substrate exposed to an ultraviolet light source to determine uniformity of the coating over the substrate. Uniform coverage is necessary to develop optimum adhesion between the substrate and a subsequently applied paint layer.

    摘要翻译： 公开了包含氯化聚烯烃和荧光增白剂的组合物。 该组合物可用作聚烯烃基材的可检测的粘合促进剂。 将组合物作为涂层施加到聚烯烃基材上，并将涂覆的基材暴露于紫外光源以确定涂层在基材上的均匀性。 需要均匀的覆盖以发展基材和随后涂覆的涂料层之间的最佳粘合。

    Carboxylated amide polymers and coating compositions containing same
    27.
    发明授权
    Carboxylated amide polymers and coating compositions containing same 失效
    羧化酰胺聚合物和含有它们的涂料组合物

    公开(公告)号：US4174333A

    公开(公告)日：1979-11-13

    申请号：US957118

    申请日：1978-11-02

    申请人： Marvis E. Hartman ,  Thomas R. Hockswender

    发明人： Marvis E. Hartman ,  Thomas R. Hockswender

    IPC分类号： B65D65/42 ,  C08G59/00 ,  C08G59/16 ,  C08G59/58 ,  C08G69/00 ,  C09D163/00 ,  C08G59/14 ,  C08L63/00

    CPC分类号： C08G59/58 ,  C08G69/00

    摘要： Carboxylated amide polymers and coating compositions containing same are especially useful for the coating of food and beverage containers. The carboxylated amide polymers are the reaction product of (1) a compound of formula: ##STR1## wherein A is the organic residue resulting from a ring opening reaction of a 1,2-epoxy group on a polyepoxide with ammonia or amine, R.sub.1 is hydrogen or a C.sub.1-4 alkyl group, R.sub.2 is a C.sub.2-12 alkylene group, x is 0 or 1, y is from 0 to 4, R.sub.3 is hydrogen or a C.sub.1-6 alkyl group, R.sub.4 is hydrogen or a C.sub.1-6 alkyl group, provided at least one R.sub.1, R.sub.3 or R.sub.4 is hydrogen, and n is at least 1.0 with (2) a cyclic anhydride of a dibasic carboxylic acid. The carboxylated amide polymers can be made water reducible by neutralizing the polymer with an organic or inorganic base and used in aqueous coating compositions.

    摘要翻译： 羧酸酰胺聚合物和含有它们的涂料组合物对于食品和饮料容器的涂覆特别有用。 羧化酰胺聚合物是（1）下式化合物的反应产物：其中A是由聚环氧化物上的1,2-环氧基与氨或胺的开环反应得到的有机残基，R1是 氢或C1-4烷基，R2是C2-12亚烷基，x是0或1，y是0-4，R3是氢或C1-6烷基，R4是氢或C1-6 烷基，提供至少一个R 1，R 3或R 4为氢，n为至少1.0，（2）二元羧酸的环状酸酐。 羧化酰胺聚合物可以通过用有机或无机碱中和聚合物制成水可稀释并用于水性涂料组合物中。

    Extensible coatings
    28.
    发明授权
    Extensible coatings 失效
    可扩展涂层

    公开(公告)号：US3954899A

    公开(公告)日：1976-05-04

    申请号：US567219

    申请日：1975-04-11

    申请人： Wen-Hsuan Chang ,  Marvis E. Hartman

    发明人： Wen-Hsuan Chang ,  Marvis E. Hartman

    IPC分类号： C08J7/04 ,  C09D175/06 ,  C08L61/20 ,  C08L61/26

    CPC分类号： C08J7/047 ,  C09D175/06 ,  C08J2475/00 ,  Y10T428/2419

    摘要： Cured coatings having a high degree of extensibility and other desirable properties are obtained from compositions comprising a hydroxyl-containing, urethane reaction product containing a polyester component and an amine-aldehyde resin. Preferred compositions contain a polymeric polyol of low glass transition temperature. These compositions are storage-stable in one package, and the cured coatings are adherent, durable and highly extensible. These coatings are particularly useful on resilient and rubbery substrates, such as form rubber, polyurethane foam and vinyl foam, and on soft metal surfaces such as mild steel and aluminum.

    摘要翻译： 具有高延展性和其它所需性能的固化涂层由包含含羟基的含聚酯组分和胺 - 醛树脂的氨基甲酸酯反应产物的组合物获得。 优选的组合物含有低玻璃化转变温度的聚合多元醇。 这些组合物在一个包装中是储存稳定的，并且固化的涂层是粘附的，耐用的和高度可延展的。 这些涂层特别适用于弹性和橡胶基材，例如橡胶，聚氨酯泡沫和乙烯基泡沫塑料，以及软质金属表面，如软钢和铝。