摘要:
A method for preparing the linezolid (compound 1), which comprises the steps of: (1) carrying out the debenzyl reaction of compound 4 in solvent, to obtain the compound 5 or its acetic acid salt; (2) carrying out the acetylation reaction in the amino of the compound 5 or its acetic acid salt obtained in step (1) in solvent to obtain the compound 1. The intermediates to prepare the compound 1 and the acetic acid salt of compound 5. The present preparation method is easy to obtain the chiral materials and the chiral materials are cheap, the process and the post treatment are simple, the intermediate products and the end product are easy to be purified, the total yield is high, their purities are also high, this preparation method is easy to be used in the industry manufacture.
摘要:
Methods for allocating a physical downlink control channel (PDCCH) to reduce a number of PDCCH candidates in a search space for carrier aggregation on a user equipment (UE) are disclosed. The method comprises the step of selecting a control channel element (CCE) aggregation level for a PDCCH allocation for each of a plurality of user equipments (UEs) at an evolved NodeB (eNB). The operation of identifying a transmission mode for each of a plurality of component carriers (CCs) associated with the PDCCH at the eNB follows. The next operation of the method is assigning each CC's downlink control information (DCI) into CCEs in a PDCCH search space in the PDCCH starting at a CCE location based on the CC's transmission mode and the CCE aggregation level for the UE receiving the CC.
摘要:
An adjustable USB female connector includes a metal top shell, an insulated main body with connection pins which are compatible with USB interface protocol, and a metal bottom shell. The connection pins are fixed on the insulated main body. The insulated main body is fastened in the metal top shell. The metal top shell is slidably connected to the metal bottom shell, and the total thickness of the metal top shell and the metal bottom shell is variant. In a first orientation, the thickness of the USB female connector is the smallest, and the thickness is smaller than that of the standard USB female connector. In a second orientation, the metal bottom shell is pulled out, the thickness of the USB female connector increases and reaches the thickness of the standard USB female connector.
摘要:
Group size indications may be distributed from a base station to a mobile station in the form of assignment-advanced-MAP transmit control signaling. The signaling control information may be sent to a station, such as a mobile station, using a table that indicates the size of a group based on coding rates, such as one-half and one-quarter coding rates. Waste may be controlled by determining a size based on using an unoccupied resource in a group that is adjacent to data resource for data transmission by the station. However, an unoccupied resource in a group that is not adjacent to a data resource is not used for data transmission and is, therefore, wasted.
摘要:
A USB flash disk includes a metal head with a cavity, a support received in the cavity and a USB flash disk chip disposed on the support. The support includes an upper support and a lower support. One end of the upper support is connected to an end of the lower support. The upper support and the lower support form a receiving cavity therebetween to receive the USB flash disk chip. The upper support is provided with a latching structure with an opening on an outer surface thereof. The opening is defined at one end of the upper support connected to the lower support. The latching structure includes an inclined block located in a middle portion thereof and a latching groove defined on the latching structure away from the end of the upper support connecting to the lower support. An inner wall of the cavity is provided with a latching block latched in the latching groove. The USB flash disk chip includes an integrated circuit packaged inside configured for storing, the USB flash disk chip is provided with a first set of metal contacts on a surface thereof compliant with the USB interface protocol. The users can independently choose the characteristics of each component of the USB flash disk and then complete the USB flash disk assembly according to their own preferences.
摘要:
The present invention discloses an integrated analysis device for simultaneously detecting exhaled breath condensates (EBCs) and volatile organic compounds (VOCs) in human exhaled breath. The device comprises a module for sampling, separating and enriching a detected object, an EBCs detection module and a combined VOCs detection module. The module for sampling, separating and enriching a detected object is connected with the EBCs detection module via a syringe pump for sample injection. The module for sampling, separating and enriching a detected object is connected with the combined VOCs detection module by a capillary separation column. In the present invention, it is achieved that EBCs and VOCs in human exhaled breath are simultaneously sampled, separated and condensed; the heavy metal ions, cell factors, etc. in the collected EBCs are detected with a light addressable potentiometric sensor (LAPS); the condensed VOCs can be quantitatively detected by the combined VOCs detection module with a high sensitivity; and a heating rod and a platinum resistor can be conveniently replaced because a separated outlet heating piece is designed in the combined VOCs detection module.
摘要:
The invention provides an iridium-containing organic electroluminescent material, the formula of which is H: wherein R is C1-C8 alkyl. The molecule of the iridium-containing organic electroluminescent material contains benzimidazole group with electron transmission function and the benzimidazole has alkyl and fluorobenzyl group, which can improve the electron injection and transmission function of the electroluminescent material, and enable the electroluminescent material to have higher internal quanta efficiency and electroluminescent efficiency. The invention also provides a preparation method of the iridium-containing organic electroluminescent material, and an organic electroluminescent device using the material.
摘要:
The invention relates to a counter electrode for a dye-sensitized solar cell and a manufacturing method thereof. The counter electrode comprises a conductive substrate and an acid doped polyaniline layer coated on at least one surface of the conductive substrate. The conductivity of the counter electrode is increased, the recombination probability of I3− and a conduction band electron is decreased, the bond strength of the acid doped polyaniline layer and the conductive substrate is enhanced, the electronic transmission rate and the conductivity of the counter electrode for the external circuit are further increased, and the production cost is reduced. The manufacturing method can simplify the production process, produce the stable performance counter electrode, increase the production efficiency, and reduce the requirement for production equipment, thus suitable for industrial production.
摘要:
An organic electroluminescence device comprises the following structure: a conductive base (110), a hole injection layer (120), a light emission layer (140), and a cathode layer (170) are laminated in sequence. The material of the hole injection layer (120) comprises a conductive polymer and an azo initiator. A nano-network structure is provided on the connecting surface of the hole injection layer (120) and the light emission layer (140). After being heated to a higher temperature, the azo initiator can be decompounded to release N2, thus the nano-network structure is formed on the surface of the hole injection layer (120). The nano-network structure can efficiently increase the contacting area of the hole injection layer (120) and the adjacent layer. The injection efficiency of the hole is improved. A manufacturing method of the organic electroluminescence device is also provided.
摘要:
The present invention relates to a fiber distribution hub. The fiber distribution hub comprises a base case comprising at least one port portion for introducing an optical cable, wherein the optical cable includes a first fiber; a splitter case releasably attached to the base case; a splice tray rotatably hinged to the splitter case; and a cover engagable with the base case to enclose the splitter case and the splice tray. The first fiber is connected to a second fiber in the splice tray, and the second fiber is connected with a splitter in the splitter case to separate the second fiber into a plurality of separate third fibers. Thus, the invention provides a compact and modular fiber distribution hub. In addition, the fiber distribution hub can join optical fibers by mechanical splices, fusion splices and fiber optic connectors in a single unit.