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    METHOD FOR PRODUCING BETA-NITROSTYRENE COMPOUND
    23.
    发明申请
    METHOD FOR PRODUCING BETA-NITROSTYRENE COMPOUND 失效
    生产硝基硝基化合物的方法

    公开(公告)号：US20100130795A1

    公开(公告)日：2010-05-27

    申请号：US12452877

    申请日：2008-07-28

    Applicant: Masahiro Takeda ,  Hiroshi Kadono ,  Kazuo Murakami

    Inventor： Masahiro Takeda ,  Hiroshi Kadono ,  Kazuo Murakami

    IPC: C07C201/10

    CPC classification number: C07C201/12 ,  C07C205/09

    Abstract: A method for producing a β-nitrostyrene compound is provided in which a benzaldehyde derivative represented by the following formula (I): and nitromethane are condensed in an acetic acid solvent in the presence of a primary amine. This method allows production of a β-nitrostyrene compound at a high yield in the industrially-safe reaction temperature range.

    Abstract translation: 提供一种生产一种硝基苯乙烯化合物的方法，其中由下式（I）表示的苯甲醛衍生物和硝基甲烷在乙酸溶剂中在伯胺存在下缩合。 该方法允许在工业安全的反应温度范围内以高产率生产一种 - 硝基苯乙烯化合物。

    4-hydroxy-2'-nitrobutyrophenone and tetrahydro-2-(o-nitrophenyl)-2-furanol useful as intermediates in the preparation of a crop-selective herbicide
    24.
    发明授权
    4-hydroxy-2'-nitrobutyrophenone and tetrahydro-2-(o-nitrophenyl)-2-furanol useful as intermediates in the preparation of a crop-selective herbicide 失效
    4-羟基-2'-硝基苯丙酮和四氢-2-（邻硝基苯基）-2-呋喃醇可用作制备作物选择性除草剂的中间体

    公开(公告)号：US5281726A

    公开(公告)日：1994-01-25

    申请号：US997844

    申请日：1992-12-29

    Applicant: David A. Cortes

    Inventor： David A. Cortes

    IPC: C07C201/12 ,  C07C201/10 ,  C07C205/11 ,  C07C205/45 ,  C07D307/20 ,  C07C49/80 ,  C07C49/82

    CPC classification number: C07D307/20 ,  C07C205/45

    Abstract: There are provided 4-Hydroxy-2'-nitrobutyrophenone and tetrahydro-2-(o-nitrophenyl)-2-furanol and mixtures thereof, important intermediates in the preparation of the crop-selective herbicidal agent 1-{[o-(cyclopropylcarbonyl)phenyl]sulfamoyl}-3-(4,6-dimethoxy-2-pyrimidinyl)urea. Also provided is a method for the preparation of 4-halo-2'-nitrobutyrophenone, useful as an intermediate in the preparation of 1-{[o-(cyclopropylcarbonyl)phenyl]sulfamoyl}-3-(4,6-dimethoxy-2-pyrimidinyl)urea.

    Abstract translation: 提供4-羟基-2'-硝基苯丙酮和四氢-2-（邻硝基苯基）-2-呋喃醇及其混合物，其是制备作物选择性除草剂1 - （（邻 - （环丙基羰基） 苯基）氨磺酰）-3-（4,6-二甲氧基-2-嘧啶基）脲。 还提供了制备4-卤代-2'-硝基苯丙酮的方法，其可用作制备1 - （（邻 - （环丙基羰基）苯基）氨磺酰基）-3-（4,6-二甲氧基-2 - 嘧啶基）脲。

    Catalytic preparation of nitroalkanes
    26.
    发明授权
    Catalytic preparation of nitroalkanes 失效
    催化制备硝基烷烃

    公开(公告)号：US4431842A

    公开(公告)日：1984-02-14

    申请号：US446076

    申请日：1982-12-01

    Applicant: William V. Hayes

    Inventor： William V. Hayes

    IPC: C07B61/00 ,  B01J23/00 ,  C07C67/00 ,  C07C201/00 ,  C07C201/10 ,  C07C205/02 ,  C07C76/02

    CPC classification number: C07C201/10

    Abstract: A process of making nitroalkanes which comprises reacting a lower alkanol, e.g. methanol, and nitric acid (HNO.sub.3) in the vapor phase in the presence of a catalyst which is an oxide or a salt of a metal of Group II of the periodic table, e.g. calcium chloride.

    Abstract translation: 制备硝基烷烃的方法，其包括使低级链烷醇如 甲醇和硝酸（HNO 3）在催化剂存在下的气相中，该催化剂是周期表第II族金属的氧化物或盐。 氯化钙。

    Method for synthesizing 3,5-dichloroanisole from 1,3,5-trichlorobenzene
    29.
    发明授权
    Method for synthesizing 3,5-dichloroanisole from 1,3,5-trichlorobenzene 有权
    从1,3,5-三氯苯合成3,5-二氯苯甲醚的方法

    公开(公告)号：US08901361B2

    公开(公告)日：2014-12-02

    申请号：US13522291

    申请日：2011-01-12

    Applicant: Eric Pasquinet ,  Anne Wuillaume ,  Didier Poullain ,  Etienne Kosciusko-Morizet

    Inventor： Eric Pasquinet ,  Anne Wuillaume ,  Didier Poullain ,  Etienne Kosciusko-Morizet

    IPC: C07C17/00 ,  C07C22/00 ,  C07C25/00 ,  C07C41/01 ,  C07C209/10 ,  C07C209/18 ,  C07C41/16 ,  C07C201/10

    CPC classification number: C07C41/01 ,  C07C41/16 ,  C07C201/10 ,  C07C209/10 ,  C07C209/18 ,  C07C43/225 ,  C07C205/06 ,  C07C211/52

    Abstract: A method for synthesizing 3,5-dichloroanisole from 1,3,5-trichloro-benzene is proved. The method may comprises: a) the reaction between 1,3,5-trichloro-benzene and a methanolate of an alkaline or alkaline-earth metal in a first solvent chosen from among dimethylsulfoxide and 1,1,3,3-tétramethylurea, b) the precipitation of the product resulting from step a) in a second solvent which is not included among substances considered carcinogenic, mutagenic and/or toxic for reproduction by Regulation (EC) no 1272/2008 of the European Parliament and of the Council of 16 Dec. 2008, then c) the recovery of the precipitate thus obtained. The method may be applied to synthesize 1,3,5-triamino-2,4,6-trinitrobenzene in which 3,5-dichloroanisole is an intermediate product.

    Abstract translation: 证明了从1,3,5-三氯苯合成3,5-二氯苯甲醚的方法。 该方法可以包括：a）在选自二甲基亚砜和1,1,3,3-三甲基脲的第一溶剂中的1,3,5-三氯苯和碱金属或碱土金属的甲醇盐之间的反应，b ）通过欧盟议会和理事会第1272/2008号条例（EC）第1272/2008号规定的步骤a）在第二溶剂中的沉淀，该第二溶剂不包括在被认为是致癌，致突变和/或有毒生殖的物质中 然后c）如此获得的沉淀物的回收。 该方法可用于合成其中3,5-二氯苯甲醚为中间产物的1,3,5-三氨基-2,4,6-三硝基苯。

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