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    Proton conducting polymer membrane comprising phosphonic acid groups containing polyazoles and the use thereof in fuel cells
    31.
    发明授权
    Proton conducting polymer membrane comprising phosphonic acid groups containing polyazoles and the use thereof in fuel cells 失效
    包含含有多唑的膦酸基的质子导电聚合物膜及其在燃料电池中的用途

    公开(公告)号：US07736778B2

    公开(公告)日：2010-06-15

    申请号：US10530002

    申请日：2003-10-02

    Applicant: Oemer Uensal ,  Joachim Kiefer ,  Gordon Calundann ,  Michael Sansone ,  Brian Benicewicz ,  Eui Wong Choe

    Inventor： Oemer Uensal ,  Joachim Kiefer ,  Gordon Calundann ,  Michael Sansone ,  Brian Benicewicz ,  Eui Wong Choe

    IPC: H01M8/10 ,  B01J49/00 ,  C08J5/20 ,  B01J41/12

    CPC classification number: C08G73/18 ,  B01D71/62 ,  B01D71/82 ,  H01M8/1027 ,  H01M8/103 ,  H01M8/1044 ,  H01M8/1048

    Abstract: A proton-conducting polymer membrane comprising polyazoles containing phosphonic acid groups is obtainable by a process comprising: A) mixing one or more aromatic or heteroaromatic tetraamino compounds with one or more aromatic or heteroaromatic carboxylic acids or derivatives thereof which contain at least two acid groups per carboxylic acid monomer, with at least part of the tetraamino compounds or the carboxylic acids comprising at least one phosphonic acid group, or mixing of one or more aromatic or heteroaromatic diaminocarboxylic acids, of which at least part comprises phosphonic acid groups, in polyphosphoric acid to form a solution or dispersion; B) optionally heating the solution or dispersion obtained by step A) under inert gas to temperatures of up to 350° C. to form polyazole polymers; C) applying a layer using the mixture from step A) or B) to a support, thus forming a membrane, and D) partially hydrolyzing the polyphosphoric acid moieties of the membrane from step C) until it is self-supporting.

    Abstract translation: 包含含有膦酸基团的多偶唑的质子传导性聚合物膜可以通过以下方法获得，该方法包括：A）将一种或多种芳族或杂芳族四氨基化合物与一种或多种芳族或杂芳族羧酸或其衍生物混合，所述芳族或杂芳族羧酸或其衍生物含有至少两个酸基团 羧酸单体，其中至少部分四氨基化合物或羧酸包含至少一个膦酸基团，或将至少部分包含膦酸基团的一种或多种芳族或杂芳族二氨基羧酸在多磷酸中混合至 形成溶液或分散体; B）任选地将惰性气体下的步骤A）得到的溶液或分散体加热到高达350℃的温度，形成聚唑聚合物; C）使用来自步骤A）或B）的混合物将层施加到载体上，从而形成膜，以及D）从步骤C）部分水解膜的多磷酸部分直到其自支撑。

    Liquid crystal polymers
    32.
    发明授权
    Liquid crystal polymers 有权
    液晶聚合物

    公开(公告)号：US07317066B2

    公开(公告)日：2008-01-08

    申请号：US11511540

    申请日：2006-08-29

    Applicant: Brian Benicewicz ,  Jiping Shao

    Inventor： Brian Benicewicz ,  Jiping Shao

    IPC: C08G63/00

    CPC classification number: C08G63/605 ,  C07C63/34 ,  C09K19/3809

    Abstract: Liquid crystal polyester derived from phenylene-naphthalene monomers and one or more comonomers display an improved balance of properties, including low melt viscosity, fast cycle time in molding, very low mold shrinkage, high tensile and/or flexural strength, solvent resistance, excellent barrier properties, low water absorption, low thermal expansion coefficient, excellent thermostability, and/or low flammability. The phenylene-naphthalene monomers are The one or more comonomers include 4-hydroxybenzoic acid, 2-hydroxy-6-naphthoic acid, terephthalic acid, isophthalic acid, and derivatives and combinations thereof.

    Abstract translation: 衍生自亚苯基萘单体和一种或多种共聚单体的液晶聚酯具有改进的性能平衡，包括低熔体粘度，成型周期快，模具收缩率低，抗拉强度和/或抗弯强度高，耐溶剂性，优异的阻隔性 性能，吸水率低，热膨胀系数低，热稳定性好，和/或低易燃性。 亚苯基萘单体是一种或多种共聚单体包括4-羟基苯甲酸，2-羟基-6-萘甲酸，对苯二甲酸，间苯二甲酸及其衍生物和组合。

    Proton conducting polymer membrane comprising phoshphonic acid groups containing polyazoles and the use thereof in fuel cells
    35.
    发明申请
    Proton conducting polymer membrane comprising phoshphonic acid groups containing polyazoles and the use thereof in fuel cells 失效
    质子导电聚合物膜，其包含含有多唑的磷酸基团及其在燃料电池中的用途

    公开(公告)号：US20060008690A1

    公开(公告)日：2006-01-12

    申请号：US10530002

    申请日：2003-10-02

    Applicant: Oemer Uensal ,  Joachim Kiefer ,  Gordon Calundann ,  Michael Sansone ,  Brian Benicewicz ,  Eui Choe

    Inventor： Oemer Uensal ,  Joachim Kiefer ,  Gordon Calundann ,  Michael Sansone ,  Brian Benicewicz ,  Eui Choe

    IPC: H01M8/10 ,  C08J5/22 ,  H01M4/86

    CPC classification number: C08G73/18 ,  B01D71/62 ,  B01D71/82 ,  H01M8/1027 ,  H01M8/103 ,  H01M8/1044 ,  H01M8/1048

    Abstract: The present invention relates to proton-conducting polymer membranes which comprise polyazoles containing phosphonic acid groups and are obtainable by a process comprising the steps A) mixing of one or more aromatic and/or heteroaromatic tetraamino compounds with one or more aromatic and/or heteroaromatic carboxylic acids or derivatives thereof which contain at least two acid groups per carboxylic acid monomer, with at least part of the tetraamino compounds and/or the carboxylic acids comprising at least one phosphonic acid group, or mixing of one or more aromatic and/or heteroaromatic diaminocarboxylic acids, of which at least part comprises phosphonic acid groups, in polyphosphoric acid to form a solution and/or dispersion, B) heating of the solution and/or dispersion obtainable according to step A) under inert gas at temperatures of up to 350° C. to form polyazole polymers, C) application of a layer using the mixture from step A) and/or B) to a support, D) treatment of the membrane formed in step C) until it is self-supporting.

    Abstract translation: 本发明涉及包含含有膦酸基团的多唑类的质子传导聚合物膜，并且可通过包括以下步骤的方法获得：a）将一种或多种芳族和/或杂芳族四氨基化合物与一种或多种芳族和/或杂芳族羧酸 每个羧酸单体含有至少两个酸基的酸或其衍生物，至少部分四氨基化合物和/或羧酸包含至少一个膦酸基团，或一种或多种芳族和/或杂芳族二氨基羧酸 酸，其至少部分包含膦酸基团，在多磷酸中形成溶液和/或分散体; B）在惰性气体下，在高达350℃的温度下加热根据步骤A）可获得的溶液和/或分散体 C.形成聚唑聚合物，C）使用来自步骤A）和/或B）的混合物将层施加到载体上，D）处理膜 在步骤C）中形成，直到其自支撑为止。

    Phosphonate and phosphonic acid RAFT agents and monomers, along with methods of their manufacture and use
    37.
    发明授权
    Phosphonate and phosphonic acid RAFT agents and monomers, along with methods of their manufacture and use 有权
    膦酸酯和膦酸RAFT试剂和单体，以及其制备和使用方法

    公开(公告)号：US09359453B2

    公开(公告)日：2016-06-07

    申请号：US14484990

    申请日：2014-09-12

    Applicant: Brian Benicewicz ,  Anand Viswanath ,  Alexandra Nicole Green

    Inventor： Brian Benicewicz ,  Anand Viswanath ,  Alexandra Nicole Green

    IPC: C08F2/38 ,  C07C329/00 ,  C07F9/40 ,  C07F9/38

    CPC classification number: C08F2/38 ,  C07C329/00 ,  C07F9/3808 ,  C07F9/4006 ,  C08F2438/03

    Abstract: An intermediate compound for forming a RAFT agent is provided that can have the formula: where n is an integer from 1 to 20; m is an integer from 0 to 20; R1 is H, an alkyl group, or a cyano group; R2 is H, an alkyl group, or a cyano group; Y is OH, COOH, or NH2; and X is OH, COOH, NH2, a nitrobenzyl, benzyl, or para-methyl benzyl group. A RAFT agent is also provided that comprises a thiocarbonylthio-containing organic compound having a phosphonic end group. A method is also provided for forming a polymer chain on a surface of a nanoparticle utilizing the RAFT agent, along with nanoparticles and nanocomposites formed therefrom.

    Abstract translation: 提供一种用于形成RAFT试剂的中间体化合物，其可以具有下式：其中n为1至20的整数; m为0〜20的整数; R1是H，烷基或氰基; R2是H，烷基或氰基; Y是OH，COOH或NH 2; X是OH，COOH，NH 2，硝基苄基，苄基或对甲基苄基。 还提供了包含具有膦酸端基的含硫代羰硫基的有机化合物的RAFT试剂。 还提供了一种利用RAFT剂在纳米颗粒的表面上形成聚合物链的方法，以及由其形成的纳米颗粒和纳米复合材料。

    NANOFILLED POLYMERIC NANOCOMPOSITES WITH TUNABLE INDEX OF REFRACTION
    39.
    发明申请
    NANOFILLED POLYMERIC NANOCOMPOSITES WITH TUNABLE INDEX OF REFRACTION 有权
    具有可弯曲折射率的纳米聚合物纳米复合材料

    公开(公告)号：US20120302700A1

    公开(公告)日：2012-11-29

    申请号：US13575419

    申请日：2011-01-27

    Applicant: Peng Tao ,  Li Yu ,  Brian Benicewicz ,  Richard W. Siegel ,  Linda S. Schadler ,  Anand Viswanath

    Inventor： Peng Tao ,  Li Yu ,  Brian Benicewicz ,  Richard W. Siegel ,  Linda S. Schadler ,  Anand Viswanath

    IPC: C08F8/40 ,  C08L25/06 ,  C08F8/30 ,  C08L83/10 ,  C08F20/32 ,  C08F20/10 ,  C08L33/12 ,  C08L63/00

    CPC classification number: C09C1/3669 ,  B82Y30/00 ,  C01P2002/82 ,  C01P2004/64 ,  C08F2438/03 ,  C08K3/04 ,  C08K7/24 ,  C08K9/04 ,  C08K2201/011 ,  C09C1/36 ,  C09C1/3676 ,  C09C1/3692

    Abstract: The present invention includes a method for preparing a nanoparticle filled nanocomposite material, the method including the steps of providing a plurality of nanoparticles. attaching a first layer of organic ligand to the nanoparticle via a phosphate or phosphonate linkage, covalently attaching a second layer of matrix compatible polymer to said first layer of organic ligand to produce modified nanoparticles, providing a polymer matrix and dispersing the modified nanoparticles in the polymer matrix, wherein the dispersement of the modified nanoparticles into the polymer matrix results in a nanocomposite material, and wherein the modified nanoparticles are modified such that the first layer is proximal to the nanoparticle and the second layer is distal to the nanoparticle. Also within the scope of the invention are modified nanoparticles, alternative nanocomposite materials and methods of making the same.

    Abstract translation: 本发明包括一种制备纳米颗粒填充纳米复合材料的方法，该方法包括提供多个纳米颗粒的步骤。 将第一层有机配体通过磷酸盐或膦酸酯键连接到纳米颗粒上，将第二层基质相容性聚合物共价连接到所述第一层有机配体上以产生改性纳米颗粒，提供聚合物基质并将改性纳米颗粒分散在聚合物 基质，其中所述改性纳米粒子分散到所述聚合物基质中导致纳米复合材料，并且其中所述修饰的纳米颗粒被修饰，使得所述第一层接近所述纳米颗粒，并且所述第二层位于所述纳米颗粒的远侧。 还在本发明的范围内是改性纳米颗粒，替代纳米复合材料及其制备方法。

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