METHOD AND ARRANGEMENT FOR PROVIDING CHALCOGENS
    31.
    发明申请
    METHOD AND ARRANGEMENT FOR PROVIDING CHALCOGENS 审中-公开
    用于提供CHALCOGENS的方法和装置

    公开(公告)号:US20150368789A1

    公开(公告)日:2015-12-24

    申请号:US14824806

    申请日:2015-08-12

    Abstract: A method and an arrangement for providing chalcogens as thin layers on substrates, in particular on planar substrates prepared with precursor layers and composed of any desired materials, preferably on substrates composed of float glass, is achieved by forming an inlet- and outlet-side gas curtain for an oxygen-tight closure of a transport channel in a vapour deposition head, introducing an inert gas into the transport channel for displacing atmospheric oxygen, introducing one or more substrates to be coated, the substrates being temperature-regulated to a predetermined temperature, into the transport channel, introducing a chalcogen vapour/carrier gas mixture from a source into the transport channel at the vapour deposition head above the substrates and forming a selenium layer on the substrates by PVD at a predetermined pressure, and removing the substrates after a predetermined process time has elapsed.

    Abstract translation: 通过形成入口和出口侧气体来实现在基底上,特别是在由前体层制备并由任何所需材料制成的平面基底上,优选在浮法玻璃上形成的基底上,提供作为薄层的硫属元素的方法和装置。 用于气相沉积头中的输送通道的不透气闭合的窗帘,将惰性气体引入输送通道中以排出大气氧,引入待涂覆的一个或多个基底,将基底温度调节到预定温度, 将来自源的硫属元素蒸气/载气混合物引入到基板上方的蒸镀头处的输送通道中,并通过PVD以预定压力在基板上形成硒层,并在预定的压力下除去基板 处理时间已过。

    PROCESS FOR PRODUCTION OF MAGNESIUM FLUORIDE SOL SOLUTIONS FROM ALKOXIDES COMPRISING ADDITION OF MAGNESIUM SALTS
    36.
    发明申请
    PROCESS FOR PRODUCTION OF MAGNESIUM FLUORIDE SOL SOLUTIONS FROM ALKOXIDES COMPRISING ADDITION OF MAGNESIUM SALTS 审中-公开
    从包含镁盐添加物的烷氧化物生产氟化镁溶液的方法

    公开(公告)号:US20150231587A1

    公开(公告)日:2015-08-20

    申请号:US14428989

    申请日:2013-09-18

    Applicant: NANOFLUOR GmbH

    Inventor: Erhard Kemnitz

    Abstract: The invention relates to a method for obtaining a magnesium fluoride (MgF2) sol solution, comprising the steps of providing a magnesium alkoxide precursor in a non-aqueous solvent and adding 1.85 to 2.05 molar equivalents of non-aqueous hydrofluoric acid, characterized in that the reaction proceeds in the presence of a second magnesium fluoride precursor selected from the group of salts of strong, volatile acids, such as a chloride, bromide, iodide, nitrate or triflate of magnesium, or of a catalytic amount of a strong, volatile acid; and/or an additive non-magnesium fluoride precursor selected from the group of salts of strong, volatile acids, such as a chloride, bromide, iodide, nitrate or triflate of lithium, antimony, tin calcium, strontium, barium, aluminium, silicium, zirconium, titanium or zinc. The invention further relates to sol solutions, method of applying the sol solutions of the invention to surfaces as a coating, and to antireflective coatings obtained thereby.

    Abstract translation: 本发明涉及一种获得氟化镁(MgF 2)溶胶溶液的方法,包括以下步骤:在非水溶剂中提供醇镁前体,并加入1.85-2.05摩尔当量的非水性氢氟酸,其特征在于: 反应在存在选自强挥发性酸如氯化物,溴化物,碘化物,硝酸盐或氟化三氟甲磺酸盐或催化量的强挥发酸的盐的第二氟化镁前体的存在下进行; 和/或选自锂,锑,锡钙,锶,钡,铝,硅等的强挥发性酸如氯化物,溴化物,碘化物,硝酸盐或三氟甲磺酸盐的盐的添加剂非氟化镁前体, 锆,钛或锌。 本发明还涉及溶胶溶液,将本发明的溶胶溶液涂布到作为涂层的表面上的方法以及由此获得的抗反射涂层。

    Method of producing magnesium fluoride coating, antireflection coating, and optical element
    37.
    发明授权
    Method of producing magnesium fluoride coating, antireflection coating, and optical element 有权
    生产氟化镁涂层,抗反射涂层和光学元件的方法

    公开(公告)号:US09079214B2

    公开(公告)日:2015-07-14

    申请号:US13770890

    申请日:2013-02-19

    Abstract: A method of producing a magnesium fluoride coating includes a step of forming a coating by applying a solution containing a fluorine-containing organic magnesium compound represented by the following formula to a base and a step of heat-treating the coating while the coating is being irradiated with a beam of light with a wavelength of 246 nm or less: Mg(CF3—X—COO)2  (1) wherein X represents a single bond or one of —(CF2)n—, —(CH2)m—, and —CH2CF2— that may have a substituent, where n and m each represent an integer of 1 to 4. The temperature of the heat-treating step can be 250° C. or lower. The coating can be irradiated with a beam of light with a wavelength of 185 nm or less.

    Abstract translation: 氟化镁涂层的制造方法包括通过将含有下式所示的含氟有机镁化合物的溶液涂布在基材上而形成涂层的步骤,以及在涂布被照射时对涂层进行热处理的工序 具有波长为246nm以下的光束:Mg(CF 3-X-COO)2(1)其中X表示单键或 - (CF 2)n - , - (CH 2)m - , - -CH 2 CF 2 - 可以具有取代基,其中n和m各自表示1〜4的整数。热处理步骤的温度可以为250℃以下。 可以用波长为185nm以下的光束照射涂层。

    Methods for improving the strength of glass substrates
    39.
    发明授权
    Methods for improving the strength of glass substrates 有权
    提高玻璃基板强度的方法

    公开(公告)号:US08834962B2

    公开(公告)日:2014-09-16

    申请号:US13153320

    申请日:2011-06-03

    CPC classification number: C03C17/22 C03C21/008

    Abstract: Methods for improving the strength of glass substrates are described. One such method for strengthening a glass disk substrate for a storage device includes immersing at least a portion of the glass substrate in a solution, the solution including a solvent and a coating material selected from the group consisting of NaOH, KOH, and KNO3, removing the glass substrate from the solution, allowing the solvent to evaporate from the glass substrate, and heating the glass substrate at a preselected temperature for a preselected duration, where the preselected temperature is sufficient to substantially melt the coating material and is less than a transition temperature of the glass substrate.

    Abstract translation: 描述了提高玻璃基板的强度的方法。 用于加强用于存储装置的玻璃盘基片的一种这样的方法包括将至少一部分玻璃基底浸入溶液中,该溶液包括溶剂和选自NaOH,KOH和KNO 3的涂层材料,除去 来自溶液的玻璃基底,允许溶剂从玻璃基底蒸发,并在预选温度下加热玻璃基片预选的时间,其中预选温度足以使涂层材料基本上熔化并且小于转变温度 的玻璃基板。

    PHYSICAL VAPOR DEPOSITED LAYERS FOR PROTECTION OF GLASS SURFACES
    40.
    发明申请
    PHYSICAL VAPOR DEPOSITED LAYERS FOR PROTECTION OF GLASS SURFACES 有权
    物理蒸气沉积层保护玻璃表面

    公开(公告)号:US20140093711A1

    公开(公告)日:2014-04-03

    申请号:US14043354

    申请日:2013-10-01

    Abstract: A scratch-resistant glass substrate is prepared by forming a hard, scratch-resistant layer over a major surface of the substrate. The layer is formed from an inorganic material such as a metal oxide, metal nitride, metal carbide, or metal boride using, for example, physical vapor deposition such as reactive or non-reactive sputtering at a process temperature of less than 500° C. The inorganic layer is resistant to micro-ductile scratching, which can safeguard the visible appearance of the glass substrate in use. The glass substrate can include chemically-strengthened glass.

    Abstract translation: 通过在基材的主表面上形成硬的耐划伤层来制备耐刮擦玻璃基材。 该层由诸如金属氧化物,金属氮化物,金属碳化物或金属硼化物的无机材料形成,使用例如在小于500℃的工艺温度下的物理气相沉积如反应性或非反应性溅射。 无机层耐微韧性刮擦,可以保护使用中的玻璃基板的可见外观。 玻璃基板可以包括化学强化的玻璃。

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