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    Carbon dioxide-blown overbased calcium alkylphenolate lubricating compositions
    43.
    发明授权
    Carbon dioxide-blown overbased calcium alkylphenolate lubricating compositions 失效
    二氧化碳吹制高碱性烷基酚钙润滑组合物

    公开(公告)号：US4320016A

    公开(公告)日：1982-03-16

    申请号：US78346

    申请日：1979-09-24

    Applicant: Benjamin H. Zoleski ,  Gayle P. Herbert ,  Rodney L. Sung ,  Robert M. Scarberry

    Inventor： Benjamin H. Zoleski ,  Gayle P. Herbert ,  Rodney L. Sung ,  Robert M. Scarberry

    IPC: C10M159/22 ,  C10M1/38

    CPC classification number: C10M159/22 ,  C10M2219/087 ,  C10M2219/088 ,  C10M2219/089

    Abstract: A lubricating oil composition containing a blend of sulfurized calcium alkylphenolate having an alkylphenol to calcium metal rate of about 1.0 to 1.4 and a Ca content of 0.5 to 12 wt. % prepared by: (1) reacting at a temperature between 250.degree. and 410.degree. F. an alkylphenol with calcium alkoxyalkoxide to form a first reaction mixture utilizing between about 45 and 90 wt. % of the stoichiometric amount required to convert the alkylphenol to calcium alkylphenolate: (2) contacting the reaction mixture with sulfur at a temperature between about 440.degree. and 460.degree. F. in the presence of between about 13 and 20 wt. % of a lubricating oil based on the step 2 second reaction mixture, (3) contacting the second reaction mixture with calcium alkoxyalkoxide at a temperature between about 400.degree. and 425.degree. F.; first and second additions totaling about 280 percent of the stoichiometric amount of calcium alkoxyalkoxide to form said calcium alkylphenolate; (4) hydrolyzing the blown mixture by steam sparging with at least 100% of the stoichiometric amount of steam required for complete hydrolysis of the calcium-2-methoxyethoxide to calcium hydroxide at a temperature ranging from 350.degree. to 410.degree. F., blowing the hydrolyzed mixture with about 20% of the stoichiometric amount of CO.sub.2 required for partial carbonation to form a blend of 20% carbonate overbased sulfurized calcium alkylphenolate and 80% hydroxide overbased sulfurized calcium alkylphenolate and adding thereto at a temperature of 340.degree. to 350.degree. F. a diluent oil.

    Abstract translation: 一种润滑油组合物，其含有烷基酚与硫酸化的烷基酚钙与钙金属速率约为1.0-1.4，Ca含量为0.5-12重量％的共混物。 通过以下方法制备的：（1）在250-410°F的温度下使烷基酚与烷氧基烷氧基烷烃反应形成第一反应混合物，其中使用约45-90wt。 将烷基酚转化为烷基酚盐酸盐所需的化学计量量的百分比：（2）在约440℃至460℃之间的温度下，将反应混合物与硫接触，在约13至20重量％ 基于步骤2第二反应混合物的润滑油的％;（3）在约400至425°F的温度下使第二反应混合物与烷氧基烷氧基烷烃接触; 第一和第二次加入总计约280％的化学计量的烷氧基烷烃氧化物以形成所述烷基酚钙; （4）通过蒸汽喷射将吹入的混合物水解成至少100％的化学计量量的蒸汽，所述蒸汽在350-410°F的温度下完全水解为氢氧化钙。 水解混合物，其中约20％的部分碳酸化所需的CO 2的化学计量量形成20％碳酸盐高碱性硫化烷基酚钙盐和80％氢氧化物高碱性硫化烷基酚钙酸盐的共混物，并在340°至350°F的温度下加入。 稀释油。

    Novel fuel composition containing alcohol
    44.
    发明授权
    Novel fuel composition containing alcohol 失效
    含有酒精的新型燃料组合物

    公开(公告)号：US4282007A

    公开(公告)日：1981-08-04

    申请号：US189528

    申请日：1980-09-22

    Applicant: Rodney L. Sung

    Inventor： Rodney L. Sung

    IPC: C10L1/02 ,  C10L1/232 ,  C10L1/22 ,  C10L1/18

    CPC classification number: C10L1/232 ,  C10L1/023

    Abstract: A novel fuel composition contains ethanol or gasohol plus, as a corrosion inhibitor, a reaction product of aminotriazole and polyisobutenyl succinic acid anhydride.

    Abstract translation: 一种新型燃料组合物含有乙醇或油醇，作为腐蚀抑制剂，氨基三唑和聚异丁烯基琥珀酸酐的反应产物。

    Sulfurized calcium alkylphenolate compositions
    46.
    发明授权
    Sulfurized calcium alkylphenolate compositions 失效
    硫酸烷基酚钙组合物

    公开(公告)号：US3969235A

    公开(公告)日：1976-07-13

    申请号：US500965

    申请日：1974-08-26

    Applicant: Rodney L. Sung ,  Harry Chafetz ,  Benjamin H. Zoleski ,  Walter D. Foucher, Jr.

    Inventor： Rodney L. Sung ,  Harry Chafetz ,  Benjamin H. Zoleski ,  Walter D. Foucher, Jr.

    IPC: C10M163/00 ,  C10M135/30 ,  C10M159/12 ,  C10M159/22 ,  C10N10/04 ,  C10N30/04 ,  C10N30/10 ,  C10N40/25 ,  C10M1/38

    CPC classification number: C10M159/22 ,  C10M2215/04 ,  C10M2215/086 ,  C10M2215/26 ,  C10M2215/28 ,  C10M2217/046 ,  C10M2217/06 ,  C10M2219/087 ,  C10M2219/088 ,  C10M2219/089 ,  C10M2219/10 ,  C10M2219/102 ,  C10M2219/104 ,  C10M2219/106 ,  C10M2221/00 ,  C10M2223/12 ,  C10M2229/041 ,  C10N2270/02

    Abstract: A lubricating oil composition containing sulfurized calcium alkylphenolate detergent dispersant of superior resistance to oxidation prepared by (1) reacting at a temperature between 200.degree. and 425.degree.F. alkylphenol with a first addition of calcium alkoxyalkoxide to form a calcium alkylphenolate containing first reaction mixture utilizing between about 45 and 90 wt. % of the stoichiometric amount required to convert the alkylphenol to calcium alkylphenolate, (2) contacting the calcium alkylphenolate first reaction mixture with sulfur at a temperature between about 440.degree. and 460.degree.F. in the presence of between about 13 and 20 wt. % of a hydrocarbon lubricating oil based on step 2 second reaction mixture, and (3) contacting the second reaction mixture with a second addition of calcium alkoxyalkoxide at a temperature between about 350.degree. and 425.degree.F., said first and second addition totalling between about 100 and 120% of the stoichiometric amount of calcium alkoxyalkoxide to form said calcium alkylphenolate, said steps 1 and 3 being advantageously conducted while blowing their respective reaction mixtures with inert gas, step 2 being conducted while sequentially blowing step 2 reaction mixture with inert gas, carbon dioxide and inert gas.

    Abstract translation: （1）在200〜425°F的烷基苯酚温度下反应，首先加入烷氧基烷氧基烷烃，形成含有第一反应混合物的烷基酚钙，利用 约45-90重量％ 将烷基酚转化为烷基酚盐酸钙所需的化学计量量的百分比，（2）在约440至460℃之间的温度下，在约13至20重量％的存在下，使烷基酚钙盐与第一反应混合物与硫接触。 基于步骤2的第二反应混合物的烃类润滑油的％，和（3）使第二反应混合物在约350°至425°F的温度下第二次加入烷氧基烷氧基烷烃之间接触，所述第一和第二加成合计在 约100和120％的化学计量的烷氧基烷氧基烷烃形成所述烷基酚钙，所述步骤1和3有利地在惰性气体吹送各自的反应混合物的同时进行，步骤2进行，同时依次用惰性气体吹送步骤2的反应混合物 ，二氧化碳和惰性气体。

    Ori-inhibited motor fuel composition and storage stable concentrate
    47.
    发明授权
    Ori-inhibited motor fuel composition and storage stable concentrate 失效
    方向抑制运动燃料组成和储存稳定的浓缩物

    公开(公告)号：US5061291A

    公开(公告)日：1991-10-29

    申请号：US440636

    申请日：1989-12-28

    Applicant: Rodney L. Sung

    Inventor： Rodney L. Sung

    IPC: C08F8/32 ,  C10L1/14 ,  C10L1/2383

    CPC classification number: C10L1/143 ,  C08F8/32 ,  C10L1/146 ,  C10L1/2383

    Abstract: A motor fuel composition which inhibits engine ORI and intake valve deposit formation comprises a mixture of hydrocarbons boiling in the range of 90.degree.-450.degree. F. and the reaction product of a hydrocarbyl-substituted dibasic acid anhydride and a polyoxyalkylene diamine; it may optionally additionally comprise a polymeric component which is a polyolefin polymer, copolymer, or the corresponding aminated or hydrogenated polymer or copolymer, or mixtures thereof, of a C.sub.2 -C.sub.10 hydrocarbon. Motor fuel compositions of the instant invention show improved ORI control in comparison with typical commercial fuel compositions. The instant invention is advantageous in that it may be produced and stored as a precipitation-resistant concentrate composition.

    Abstract translation: 抑制发动机ORI和进气阀沉积物形成的机动车燃料组合物包括在90-450°F范围内沸腾的烃和烃基取代的二元酸酐与聚氧化烯二胺的反应产物的混合物; 可任选地另外包含聚合物组分，其是C2-C10烃的聚烯烃聚合物，共聚物或相应的胺化或氢化聚合物或共聚物或其混合物。 与典型的商业燃料组合物相比，本发明的机动车燃料组合物显示出改进的ORI控制。 本发明的优点在于其可以作为防沉淀浓缩物组合物生产和储存。

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