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    Single-phase, storage-stable polyol compositions containing salts and the use thereof in the production of polyurethanes
    41.
    发明授权
    Single-phase, storage-stable polyol compositions containing salts and the use thereof in the production of polyurethanes 失效
    含有盐的单相，储存稳定的多元醇组合物及其在生产聚氨酯中的用途

    公开(公告)号：US4436841A

    公开(公告)日：1984-03-13

    申请号：US497640

    申请日：1983-05-24

    申请人： Werner Rasshofer ,  Wolfgang Reichmann ,  Adolf Richartz ,  Manfred Dietrich

    发明人： Werner Rasshofer ,  Wolfgang Reichmann ,  Adolf Richartz ,  Manfred Dietrich

    IPC分类号： C08G18/66 ,  C08K5/053 ,  C09K3/00 ,  C08G18/14 ,  C08G18/65

    CPC分类号： C08G18/6674 ,  C08K5/053 ,  C08G2120/00 ,  C08G2130/00 ,  Y10S521/914

    摘要： A single-phase, storage-stable, emulsifier-free polyol mixture comprising 100 parts of a relatively high molecular weight polyoxyalkylene polyol of OH number from 20 to 120, which has at least 5% and less than 80% by weight, of terminal oxyethylene blocks; from 1 to 100 parts of a low molecular weight diol mixture which is a reaction product of ethylene glycol, butane diol-1,4, or a mixture of ethylene glycol and butane diol-1,4, with from 0.05 to 0.50 mols of alkyl oxiranes; from 0.1 to 5 parts of solubilizing additives comprising one or more salts, the cations of which are from Groups I, II and III of the Periodic Table, ammonium or mono- to tetra-alkyl ammonium ions, and the anions of which are produced by removing at least one proton from an acid having a K.sub.s value of at least 10.sup.-7 ; and, optionally, other compounds having isocyanate-reactive hydrogen atoms and other auxiliaries and additives for polyurethane production. Also polyurethanes produced using these polyol mixtures.

    摘要翻译： 一种单相，储存稳定，不含乳化剂的多元醇混合物，其包含100份具有20-120的OH数量的相对高分子量的聚氧化烯多元醇，其具有至少5重量％且小于80重量％的末端氧化乙烯 块 1至100份低分子量二醇混合物，其是乙二醇，丁二醇-1,4-或乙二醇和丁二醇-1,4-的混合物与0.05至0.50摩尔烷基的反应产物 环氧乙烷 0.1至5份包含一种或多种盐的增溶添加剂，其阳离子来自周期表第I，II和III族，铵或一至四烷基铵离子，其阴离子由 从Ks值至少为10-7的酸中除去至少一个质子; 和任选的具有异氰酸酯反应性氢原子的其它化合物和用于聚氨酯生产的其它助剂和添加剂。 还使用这些多元醇混合物制备聚氨酯。

    Polyamines and processes for the production of such polyamines and of polyurethane plastics therefrom
    42.
    发明授权
    Polyamines and processes for the production of such polyamines and of polyurethane plastics therefrom 失效
    用于生产这种多胺和聚氨酯塑料的多胺和方法

    公开(公告)号：US4386218A

    公开(公告)日：1983-05-31

    申请号：US308326

    申请日：1981-10-05

    申请人： Werner Rasshofer ,  Dieter Dieterich ,  Holger Meyborg

    发明人： Werner Rasshofer ,  Dieter Dieterich ,  Holger Meyborg

    IPC分类号： C07C275/62 ,  B01J23/02 ,  B01J31/08 ,  C07B61/00 ,  C07C271/20 ,  C07C271/26 ,  C07C273/18 ,  C07C275/00 ,  C07C275/14 ,  C08G18/00 ,  C08G18/10 ,  C08G18/32 ,  C08G18/50 ,  C08G18/65 ,  C08G18/83 ,  C07C127/15 ,  C07C127/24

    CPC分类号： C08G18/83 ,  C07C273/1809 ,  C08G18/10 ,  C08G18/5048

    摘要： A compound having a terminal isocyanate group is hydrolyzed to produce a polyamine having a urethane and/or a urea and/or a biuret group. More particularly, a carbamate is made by mixing an isocyanate prepolymer having urethane and/or urea and/or biuret groups present with aqueous base solutions at a temperature of from 0.degree. to 0.degree. C. and in quantities such that the equivalent ratio of hydroxyl to isocyanate groups is between from 0.3:1 to .gtoreq.1.01 to 1. The carbamate is then treated with an acid ion exchanger to form an amine. The amine is then removed from any other material which may be present. A preferred polyamine thus-produced corresponds to the general formula: ##STR1## in which each R radical may represent a divalent straight or branched-chain aliphatic radical; a divalent cycloaliphatic radical; a 4,4'- and/or a 2,4'-dicyclohexylmethane radical; or a 2,4- and/or 2,6-methyl cyclohexane radical. Such an amine may be reacted with a polyisocyanate and optionally with other known additives to form a polyurethane plastic or foam.

    摘要翻译： 将具有末端异氰酸酯基的化合物水解以制备具有氨基甲酸酯和/或脲和/或缩二脲基的多胺。 更具体地，氨基甲酸酯是通过在0℃至0℃的温度下混合存在有氨基甲酸酯和/或脲和/或缩二脲基的异氰酸酯预聚物和/或缩二脲基与碱水溶液形成的，其量使得羟基的当量比 到异氰酸酯基团之间的比例为0.3:1至> / = 1.01:1。然后用酸式离子交换剂处理氨基甲酸酯以形成胺。 然后将胺从可能存在的任何其它材料中除去。 如此制备的优选的多胺对应于通式：其中每个R基团可以表示二价直链或支链脂族基团; 二价脂环族基团; 4,4'-和/或2,4'-二环己基甲基基团; 或2,4-和/或2,6-甲基环己烷基。 这样的胺可以与多异氰酸酯和任选地与其它已知的添加剂反应以形成聚氨酯塑料或泡沫。

    Process for the preparation of compounds having s-triazine units and epoxide groups
    43.
    发明授权
    Process for the preparation of compounds having s-triazine units and epoxide groups 失效
    制备具有三嗪单元和环氧基团的化合物的方法

    公开(公告)号：US4384102A

    公开(公告)日：1983-05-17

    申请号：US336659

    申请日：1982-01-04

    申请人： Werner Rasshofer ,  Gerhard Grogler ,  Richard Kopp

    发明人： Werner Rasshofer ,  Gerhard Grogler ,  Richard Kopp

    IPC分类号： C07D405/14 ,  C07D405/12 ,  C08G18/00 ,  C08G18/79 ,  C08G18/80 ,  C08G18/77

    CPC分类号： C07D405/12 ,  C08G18/003 ,  C08G18/8058

    摘要： Compounds having both s-triazine units and epoxide groups present are prepared by reacting an epoxide containing an isocyanate-reactive group with a triisocyanate corresponding to the formula: ##STR1## in which X is as defined herein. These reactants are used in quantities such that the equivalent ratio of isocyanate groups to isocyanate-reactive groups is maintained at less than or equal to 1 to 1. The compounds thus produced are particularly useful as reactive cross-linkers in the production of polyurethanes and polyepoxides.

    摘要翻译： 通过使含有异氰酸酯反应性基团的环氧化物与对应于下式的其中X如本文所定义的下式的三异氰酸酯反应来制备具有均三嗪单元和环氧基团的化合物。 这些反应物的用量使得异氰酸酯基团与异氰酸酯反应性基团的当量比保持在小于或等于1比1。由此制备的化合物特别可用作聚氨酯和聚环氧化物生产中的反应性交联剂 。

    Molded polyurethane articles prepared from recycled polyols and processes for their production and use
    47.
    发明授权
    Molded polyurethane articles prepared from recycled polyols and processes for their production and use 失效
    由回收多元醇制备的模制聚氨酯制品及其生产和使用方法

    公开(公告)号：US5879608A

    公开(公告)日：1999-03-09

    申请号：US740551

    申请日：1996-10-30

    申请人： Adolf Lammeck ,  Werner Rasshofer

    发明人： Adolf Lammeck ,  Werner Rasshofer

    IPC分类号： C08G18/40 ,  C08G18/83 ,  C08G101/00 ,  C08J11/24 ,  B27N3/08 ,  B28B19/00 ,  B29C51/00 ,  B29C53/00

    CPC分类号： C08J11/24 ,  C08J2375/04 ,  Y02W30/706

    摘要： Molded polyurethane articles are made by reacting polyisocyanates with polyol compositions obtained by chemical decomposition of polyurethane and/or polyurea waste in a mold. The polyol compositions employed in this invention have an OH value of from about 100 to about 500 mg KOH/g, a water content of from 0 to about 5 wt. % and a viscosity at 20.degree. C. of more than 2,000 mPa.multidot.s. These molded polyurethane articles preferably have a sandwich structure in which the core is a polyurethane and there is at least one outer layer made from an optionally fiber-reinforced plastic material. These molded polyurethane articles are useful in the motor vehicle, furniture, machine and equipment manufacturing industries.

    摘要翻译： 聚氨酯制品是通过使多异氰酸酯与通过在模具中化学分解聚氨酯和/或聚脲废物获得的多元醇组合物而制成的。 用于本发明的多元醇组合物的OH值为约100至约500mg KOH / g，水含量为0至约5wt。 ％，在20℃下的粘度超过2,000mPax。 这些模制的聚氨酯制品优选具有夹心结构，其中芯是聚氨酯，并且存在由任选的纤维增强塑料材料制成的至少一个外层。 这些模塑聚氨酯制品可用于机动车辆，家具，机器和设备制造业。

    Composite structures
    50.
    发明授权
    Composite structures 失效
    复合结构

    公开(公告)号：US5009950A

    公开(公告)日：1991-04-23

    申请号：US323454

    申请日：1989-03-14

    申请人： Joachim Wagner ,  Karl Peltzer ,  Werner Rasshofer

    发明人： Joachim Wagner ,  Karl Peltzer ,  Werner Rasshofer

    IPC分类号： B32B25/14 ,  B32B18/00 ,  B32B27/08 ,  B32B27/40 ,  C08G18/50 ,  C08G18/65

    CPC分类号： B32B27/08 ,  Y10T428/2495 ,  Y10T428/263 ,  Y10T428/31551 ,  Y10T442/67

    摘要： The present invention is directed to composite structures by thermoplastically shaping an assembly of at least two flat thermoplastically formable plastic materials placed in layers one above the other and optionally at least one upper, lower and/or intermediate layer containing a reinforcing or filler material under such conditions of temperature and pressure that shaping is accompanied by intimate union of the individual layers of the assembly, characterized in that at least one of the flat plastic materials is based on a polyisocyanate polyaddition product having a density of at least 0.8 g/cm.sup.3 which has been prepared by the reaction of(a) aromatic polyisocyanates,(b) compounds having a molecular weight of 1800 to about 12000 and containing a statistical average of at least 2.5 isocyanate-reactive groups, optionally(c) diamines in the molecular weight range of 108 to 400 containing two primary and/or secondary aromatically bound amino groups, and optionally(d) (cyclo)alkanepolyols and/or (cyclo)alkanepolyamines in the molecular weight range of 60 to 1799 optionally containing ether groups,by a single stage or multi-stage process at an isocyanate index of 60 to 140, wherein at least one of components (c) or (d) is used in a quantity such that the total quantity of components (c) and (d) is at least 5% by weight, based on the weight of component (b).

    摘要翻译： 本发明涉及复合结构，其通过将至少两个平坦的可塑成形塑料材料的组件热塑成形，一个层叠在另一层之上，以及任选地至少一层含有增强或填充材料的上，下和/或中间层 温度和压力的条件是成形伴随着组件的各个层的紧密结合，其特征在于，所述扁平塑料材料中的至少一种基于密度为至少0.8g / cm 3的多异氰酸酯加聚产物，其具有 通过（a）芳族多异氰酸酯的反应制备，（b）分子量为1800至约12000的化合物，并且含有至少2.5个异氰酸酯反应性基团的统计平均值，任选（c）分子量范围内的二胺 108至400，其含有两个伯和/或二次芳香结合的氨基，以及任选的（d）（环）烷撑多糖 通过在异氰酸酯指数为60至140的单级或多级方法，任选地含有醚基的分子量范围为60至1799的（环）链烷多胺和/或（环）链烷多胺，其中至少一种组分（c）或 （d）的使用量使得组分（c）和（d）的总量基于组分（b）的重量为至少5重量％。