公开(公告)号：US20080219914A1

公开(公告)日：2008-09-11

申请号：US11916148

申请日：2006-05-26

Applicant: Clint Guy Smallman ,  Geoffrey John Davies ,  Johannes Lodewikus Myburgh

Inventor： Clint Guy Smallman ,  Geoffrey John Davies ,  Johannes Lodewikus Myburgh

IPC: C01B31/06 ,  B01J3/06

CPC classification number: B01J3/062 ,  B01J2203/061 ,  B01J2203/062 ,  B01J2203/0655 ,  B01J2203/068

Abstract: The invention relates to a method for manufacture of diamond, the method including the steps of providing a first coating of solvent metal or solvent metal alloy on a diamond seed to create a coated diamond seed, situating the coated diamond seed adjacent a catalyst system comprising a solvent metal and/or a source of carbon, and subjecting the coated diamond seed and catalyst system to increased temperature wherein the melting point of the first coating is at least 20 deg C. below that of the catalyst system. The invention further relates to a compact comprising a plurality of diamond seeds wherein at least one seed includes a first coating comprising a solvent metal and/or solvent metal based alloy, the compact further comprising a catalyst system comprising a solvent metal and/or a source of carbon wherein the melting point of the first coating is at least 20 deg C. below that of the catalyst system.

Abstract translation: 本发明涉及一种用于制造金刚石的方法，该方法包括以下步骤：在金刚石种子上提供溶剂金属或溶剂金属合金的第一涂层以产生涂覆的金刚石晶种，将涂覆的金刚石晶粒定位在催化剂体系附近，该催化剂体系包含 溶剂金属和/或碳源，并且使经涂覆的金刚石晶种和催化剂体系升温，其中第一涂层的熔点低于催化剂体系的熔点至少20℃。 本发明还涉及包含多个金刚石种子的压块，其中至少一种种子包括包含溶剂金属和/或溶剂金属基合金的第一涂层，该压块还包括包含溶剂金属和/或源的催化剂体系 的碳，其中第一涂层的熔点低于催化剂体系的熔点至少20℃。

公开(公告)号：US20060210465A1

公开(公告)日：2006-09-21

申请号：US11366293

申请日：2006-03-02

Applicant: Richard Clark

Inventor： Richard Clark

IPC: C01B31/06

CPC classification number: B01J3/062 ,  B01J3/065 ,  B01J2203/0625 ,  B01J2203/0655 ,  B01J2203/068 ,  C01B32/25

Abstract: A material treatment heater tube is provided in which the axial thermal conductivity is less than 10% of the circumferential thermal conductivity.

Abstract translation: 提供了一种材料处理加热器管，其中轴向导热率小于圆周热导率的10％。

公开(公告)号：US20060177362A1

公开(公告)日：2006-08-10

申请号：US11042858

申请日：2005-01-25

Applicant: Mark D'Evelyn ,  Robert Giddings ,  Fred Sharifi ,  Subhrajit Dey ,  Huicong Hong ,  Joseph Kapp ,  Ashok Khare

Inventor： Mark D'Evelyn ,  Robert Giddings ,  Fred Sharifi ,  Subhrajit Dey ,  Huicong Hong ,  Joseph Kapp ,  Ashok Khare

IPC: B01D9/00

CPC classification number: B01J3/008 ,  B01J3/002 ,  B01J3/03 ,  B01J3/046 ,  B01J3/06 ,  B01J2203/0665 ,  B01J2203/068 ,  B01J2219/00135 ,  B01J2219/00155 ,  B01J2219/00162 ,  Y02P20/544 ,  Y10T117/10 ,  Y10T117/1024 ,  Y10T117/1092

Abstract: An apparatus and method for processing materials in supercritical fluids is disclosed. The apparatus includes a capsule configured to contain a supercritical fluid, a high strength enclosure disposed about the capsule and a sensor configured to sense pressure difference between an interior and an exterior of the capsule. The apparatus also includes a pressure control device configured to adjust pressure difference of the capsule in response to the pressure difference sensed by the sensor. The apparatus further includes at least one dividing structure disposed within the capsule that divides the capsule into a seed growing chamber and a nutrient chamber.

Abstract translation: 公开了一种在超临界流体中处理材料的装置和方法。 所述装置包括：胶囊，其被配置为容纳超临界流体，围绕所述胶囊设置的高强度外壳;以及被配置为感测所述胶囊的内部和外部之间的压力差的传感器。 该装置还包括压力控制装置，该压力控制装置被配置为响应于由传感器感测到的压差而调节胶囊的压力差。 该装置还包括设置在胶囊内的至少一个分割结构，其将胶囊分成种子生长室和营养室。

公开(公告)号：US20060016127A1

公开(公告)日：2006-01-26

申请号：US11175017

申请日：2005-07-05

Applicant: Chien-Min Sung

Inventor： Chien-Min Sung

IPC: B24D18/00

CPC classification number: B01J3/062 ,  B01J2203/061 ,  B01J2203/062 ,  B01J2203/0625 ,  B01J2203/0645 ,  B01J2203/0655 ,  B01J2203/066 ,  B01J2203/068 ,  B01J2203/0685 ,  B22F2005/001 ,  B22F2999/00 ,  B23D61/18 ,  B23D65/00 ,  B23P15/28 ,  B24D3/08 ,  B24D7/066 ,  B24D18/00 ,  B24D99/005 ,  B24D2203/00 ,  C04B35/52 ,  C09K3/1409 ,  C09K3/1445 ,  C22C1/051 ,  C22C26/00 ,  C22C2204/00 ,  E21B10/5676 ,  Y10T428/2991 ,  B22F2207/03 ,  B22F1/0011 ,  B22F3/004 ,  B22F2003/1046

Abstract: An improved method for synthesizing superabrasive particles provides high quality industrial superabrasive particles with high yield and a narrow size distribution. The synthesis method can include forming a growth precursor of a substantially homogeneous mixture of raw material and catalyst material or layers of raw material and metal catalyst. The growth precursor can have a layer of adhesive over at least a portion thereof. A plurality of crystalline seeds can be placed in a predetermined pattern on the layer of adhesive. The growth precursor can be maintained at a temperature and pressure at which the superabrasive crystal is thermodynamically stable for a time sufficient for a desired degree of growth. Advantageously, the patterned placement of crystalline seeds and disclosed processes allow for production of various morphologies of synthetic diamonds, including octahedral and cubic diamonds, and improved growth conditions generally. As a result, the grown superabrasive particles typically have a high yield of high quality particles and a narrow distribution of particle sizes.

Abstract translation: 合成超级磨料颗粒的改进方法提供高产率和窄尺寸分布的高质量工业超研磨颗粒。 合成方法可以包括形成原料和催化剂材料或原料和金属催化剂层的基本上均匀的混合物的生长前体。 生长前体可在其至少一部分上具有一层粘合剂。 多个结晶种子可以以预定图案放置在粘合剂层上。 生长前体可以保持在超磨料晶体在热力学稳定的温度和压力下达足以达到所需生长程度的时间。 有利地，结晶晶种的图案化布置和所公开的方法允许生产合成金刚石的各种形态，包括八面体和立方晶体，以及通常改善的生长条件。 结果，生长的超级磨料颗粒通常具有高产率的高质量颗粒和窄的粒度分布。

公开(公告)号：US20040040490A1

公开(公告)日：2004-03-04

申请号：US10398219

申请日：2003-04-09

Applicant: JAPAN SCIENCE AND TECHNOLOGY CORPORATION

Inventor： Shoji Yamanaka ,  Xuean Chen

IPC: C30B001/00

CPC classification number: B01J3/062 ,  B01J2203/0675 ,  B01J2203/068

Abstract: null-ZrNCl polycrystalline powder prepared by chemical transport method and NH4Cl are mixed in a molar ratio of 1:2. The mixture is encapsulated in a Au capsule (6 mm in inner diameter and 6 mm in depth) of a reaction vessel 2, which is then enclosed in a highly heat-conductivitive sodium chloride block as an electrically insulating pressure medium 6. The mixture held in the sodium chloride block is placed in a carbon tube 8 for serving as a heater. In a cubic-pressing apparatus using a pyrophyllite 12 as a pressure-transmitting medium, the mixture is heated at 900null C. for 2 hours under an applied pressure of 3 GPa. After the mixture is allowed to stand until it is cooled down to room temperature, the Au capsule is taken out and light green null-ZrNCl single crystals are obtained. A large single crystal among them had a hexagonal plate-like habit and is transparent with dimensions about 2 mm in diameter, and 0.3 mm in thickness.

Abstract translation: 通过化学转移法和NH4Cl制备的β-ZrNCl多晶粉末以1:2的摩尔比混合。 将混合物包封在反应容器2的Au胶囊（内径6mm，深度为6mm）中，然后将其封入作为电绝缘压力介质6的高导热性氯化钠块中。混合物保持 在氯化钠块中放置在用作加热器的碳管8中。 在使用叶腊石12作为压力传递介质的立方压制装置中，将混合物在3GPa的施加压力下在900℃下加热2小时。 使混合物静置直至冷却至室温后，取出Au胶囊，得到浅绿色的β-ZrNCl单晶。 它们中的大单晶具有六角形板状习惯，并且是透明的，其直径大约为2mm，厚度为0.3mm。

公开(公告)号：US20040031434A1

公开(公告)日：2004-02-19

申请号：US10643330

申请日：2003-08-19

Inventor： Russell P. VandenBiesen ,  Gregory R. Herro ,  Dean T. VandenBiesen

IPC: C30B033/06

CPC classification number: B01J3/065 ,  B01J2203/061 ,  B01J2203/0655 ,  B01J2203/068 ,  C30B23/00 ,  C30B29/04

Abstract: This invention is a method of making a synthetic gem comprising elements recovered from remains of a species of the Kingdom Animalia, comprising the steps of collecting substantially pure carbon from the remains and creating gems from the carbon using crystal growth sublimation.

Abstract translation: 本发明是一种制备合成宝石的方法，其包括从动物界的种类的残余物回收的元素，其包括以下步骤：从残余物中收集基本上纯的碳，并使用晶体生长升华从碳中产生宝石。

公开(公告)号：US06616725B2

公开(公告)日：2003-09-09

申请号：US09934459

申请日：2001-08-21

Applicant: Hyun Sam Cho ,  John Chen ,  Kyung Yul Han

Inventor： Hyun Sam Cho ,  John Chen ,  Kyung Yul Han

IPC: B24D300

CPC classification number: B22F1/025 ,  B01J3/062 ,  B01J2203/061 ,  B01J2203/062 ,  B01J2203/063 ,  B01J2203/0635 ,  B01J2203/0645 ,  B01J2203/0655 ,  B01J2203/066 ,  B01J2203/068 ,  C04B35/52 ,  C04B35/5626 ,  C04B35/5831 ,  C04B35/6303 ,  C04B35/645 ,  C04B2235/386 ,  C04B2235/402 ,  C04B2235/404 ,  C04B2235/405 ,  C04B2235/427 ,  C04B2235/428 ,  C04B2235/5276 ,  C04B2235/528 ,  C04B2235/5436 ,  Y10T428/30

Abstract: A self-grown monopoly compact grit and high pressure, high temperature process for preparing the same. The high pressure, high temperature sintered/synthesized monopoly compact grit is used in various industrial tools such as saw blades, grinding wheels, cutting tools and drill bits. Further, the monopoly compact grit of the present invention is produced from a seed of a mono-crystal of diamond or cubic boron nitride surrounded by either a self-grown crystal layer or an integrally bonded poly-crystalline sintered compact layer. The self-grown crystal layer is a new grown crystal structure where the seed crystal grows into a new phase through a normal diamond or cubic boron nitride synthesis process in the presence of a catalyst metal solvent. The compact layer is composed of about 50 to about 90 volume percent of diamond or cubic boron nitride, a typical binder material, which is a catalyst for crystal-to-crystal bonding, and a cementing agent which is a binding agent capable of forming stable carbide and nitride bonds.

Abstract translation: 自生成垄断的紧凑砂砾和高压，高温工艺制备相同。 高压，高温烧结/合成的垄断压实砂砾用于各种工业工具，如锯片，砂轮，切削工具和钻头。 此外，本发明的垄断压块砂砾由金刚石或立方氮化硼的单晶种子生产，其由自生长晶体层或整体结合的多晶烧结致密层包围。 自生晶体层是新生长的晶体结构，其中晶种在催化剂金属溶剂存在下通过正常的金刚石或立方氮化硼合成工艺生长成新相。 致密层由约50至约90体积％的金刚石或立方氮化硼组成，典型的粘合剂材料是用于晶体 - 晶体结合的催化剂，和作为能够形成稳定的粘合剂的粘合剂 碳化物和氮化物键。

公开(公告)号：US06398867B1

公开(公告)日：2002-06-04

申请号：US09413446

申请日：1999-10-06

Applicant: Mark Philip D'Evelyn ,  Kristi Jean Narang

Inventor： Mark Philip D'Evelyn ,  Kristi Jean Narang

IPC: C30B1110

CPC classification number: B01J3/062 ,  B01J2203/0665 ,  B01J2203/068

Abstract: A gallium nitride growth process forms crystalline gallium nitride. The process comprises the steps of providing a source gallium nitride; providing mineralizer; providing solvent; providing a capsule; disposing the source gallium nitride, mineralizer and solvent in the capsule; sealing the capsule; disposing the capsule in a pressure cell; and subjecting the pressure cell to high pressure and high temperature (HPHT) conditions for a length of time sufficient to dissolve the source gallium nitride and precipitate the source gallium nitride into at least one gallium nitride crystal. The invention also provides for gallium nitride crystals formed by the processes of the invention.

Abstract translation: 氮化镓生长工艺形成结晶氮化镓。 该方法包括以下步骤：提供源氮化镓; 提供矿化剂; 提供溶剂; 提供胶囊; 将源氮化镓，矿化剂和溶剂置于胶囊中; 密封胶囊; 将胶囊置于压力池中; 以及使压力单元经受高压和高温（HPHT）条件一段足以溶解氮化镓源的时间并将源氮化镓沉淀到至少一个氮化镓晶体中。 本发明还提供了通过本发明的方法形成的氮化镓晶体。

公开(公告)号：US20010043903A1

公开(公告)日：2001-11-22

申请号：US09783441

申请日：2001-02-14

Inventor： Marl Philip D'Evelyn ,  Dong-Sil Park ,  Thomas Richard Anthony ,  Clifford Lawrence Spiro ,  Yue Meng ,  Christopher Allen Long

IPC: C01B031/06 ,  B01J003/08

CPC classification number: C30B25/02 ,  B01J3/062 ,  B01J2203/061 ,  B01J2203/062 ,  B01J2203/0655 ,  B01J2203/068 ,  C01B32/25 ,  C30B29/04 ,  C30B31/00 ,  Y10T428/30

Abstract: An element-doped diamond crystal is disclosed herein. The crystal includes at least one dopant element which has a greater concentration toward or near an outermost surface of the crystal than in the center of the crystal. The concentration of the dopant element is at a local minimum at least about 5 micrometers below the surface. The concentration-profile of the dopant element for these diamond crystals causes an expansion of the diamond lattice, thereby generating tangential compressive stresses at the surface of the diamond crystal. These stresses beneficially increase the compressive fracture strength of the diamond.

Abstract translation: 本文公开了元素掺杂金刚石晶体。 所述晶体包括至少一种掺杂元素，所述至少一种掺杂元素朝向或接近晶体的最外表面具有比在晶体中心更大的浓度。 掺杂剂元素的浓度在表面下方至少约5微米的局部最小值。 用于这些金刚石晶体的掺杂剂元素的浓度分布导致金刚石晶格的膨胀，从而在金刚石晶体的表面产生切向压应力。 这些应力有利地增加了金刚石的压缩断裂强度。

公开(公告)号：US06286498B1

公开(公告)日：2001-09-11

申请号：US09399573

申请日：1999-09-20

Applicant: Chien-Min Sung

Inventor： Chien-Min Sung

IPC: B28D102

CPC classification number: E21B10/5676 ,  B01J3/062 ,  B01J2203/061 ,  B01J2203/062 ,  B01J2203/0645 ,  B01J2203/0655 ,  B01J2203/066 ,  B01J2203/068 ,  B01J2203/0685 ,  B22F2005/001 ,  B22F2999/00 ,  B23P15/28 ,  B24D3/08 ,  B24D7/066 ,  B24D99/005 ,  C04B35/52 ,  C22C1/051 ,  C22C26/00 ,  C22C2204/00 ,  B22F2207/03 ,  B22F1/0011 ,  B22F3/004 ,  B22F2003/1046

Abstract: The present invention describes a novel metal bond superabrasive tool that contains a superabrasive such as diamond or CBN grits distributed in a predetermined or an uniform pattern. Such a pattern is produced by fabricating plurality layers of metal matrix with superabrasive grits distributed therein in a predetermined pattern and concentration and subsequently assembling and consolidating the layers into a tool segment. Superabrasive particles may be incorporated during the process of making these layers, or they may be planted afterwards into these layers that contains the metal matrix powder. In the latter case, the planting may be guided by a template with apertures laid in a specific pattern.

Abstract translation: 本发明描述了一种新颖的金属粘结超研磨工具，其包含以预定或均匀图案分布的超级磨料如金刚石或CBN砂粒。 这种图案通过以预定图案和浓度分布在其中的超硬磨料制造多层金属基体而产生，并且随后将层组装和固结成工具段。 可以在制造这些层的过程中引入超级磨料颗粒，或者它们可以后来种植到含有金属基质粉末的这些层中。 在后一种情况下，种植可以由具有以特定图案布置的孔的模板引导。