Multi-layer catalyst for producing phthalic anhydride
    2.
    发明授权
    Multi-layer catalyst for producing phthalic anhydride 失效
    用于生产邻苯二甲酸酐的多层催化剂

    公开(公告)号:US07718561B2

    公开(公告)日:2010-05-18

    申请号:US11597307

    申请日:2005-05-22

    IPC分类号: C07D307/89

    摘要: The present invention relates to a catalyst for preparing phthalic anhydride by gas phase oxidation of o-xylene and/or naphthalene, comprising at least three catalyst zones which have different compositions and, from the gas inlet side toward the gas outlet side, are referred to as first, second and third catalyst zone, the catalyst zones having in each case an active composition comprising TiO2, and the active composition content decreasing from the first catalyst zone disposed toward the gas inlet side to the third catalyst zone disposed toward the gas outlet side, with the proviso that (a) the first catalyst zone has an active composition content between about 7 and 12% by weight, (b) the second catalyst zone has an active composition content in the range between 6 and 11% by weight, the active composition content of the second catalyst zone being less than or equal to the active composition content of the first catalyst zone, and (c) the third catalyst zone has an active composition content in the range between 5 and 10% by weight, the active composition content of the third catalyst zone being less than or equal to the active composition content of the second catalyst zone. Also described is a preferred process for preparing such a catalyst and the preferred use of the titanium dioxide used in accordance with the invention.

    摘要翻译: 本发明涉及通过邻二甲苯和/或萘的气相氧化制备邻苯二甲酸酐的催化剂,其包括至少三个具有不同组成的催化剂区域和从气体入口侧朝向气体出口侧的催化剂区域 作为第一,第二和第三催化剂区域,催化剂区域在每种情况下都具有包含TiO 2的活性组合物,并且活性组合物含量从朝向气体出口侧设置的气体入口侧至第三催化剂区域的第一催化剂区域减少 条件是(a)第一催化剂区的活性组合物含量在约7至12重量%之间,(b)第二催化剂区的活性组成含量在6重量%至11重量%的范围内, 第二催化剂区的活性组合物含量小于或等于第一催化剂区的活性组合物含量,和(c)第三催化剂区具有活性组分 n含量在5至10重量%的范围内,第三催化剂区的活性组成含量小于或等于第二催化剂区的活性组合物含量。 还描述了制备这种催化剂的优选方法和根据本发明使用的二氧化钛的优选用途。

    METHOD FOR APPLYING A WASH COAT SUSPENSION TO A CARRIER STRUCTURE
    5.
    发明申请
    METHOD FOR APPLYING A WASH COAT SUSPENSION TO A CARRIER STRUCTURE 有权
    将洗衣架悬挂用于承载结构的方法

    公开(公告)号:US20100311573A1

    公开(公告)日:2010-12-09

    申请号:US12601876

    申请日:2008-06-02

    IPC分类号: B01J31/12 B01J27/198

    摘要: A method for applying a washcoat suspension to a support structure. To provide coatings with largely uniform thickness starting from washcoat suspensions, the method uses a device (10) set up to produce, by means of a process gas (40), a fluid bed of support structures in which the support structures circulate elliptically or toroidally, the method comprising the steps of: a) charging the device (10) with support structures and producing a support-structure fluid bed by means of a process gas (40), wherein the support structures circulate in the fluid bed elliptically or toroidally, preferably toroidally; b) impregnating the support structures with a washcoat suspension by spraying the support structures circulating elliptically or toroidally in the fluid bed with the washcoat suspension; c) drying the support structures sprayed with the washcoat suspension; and d) optionally calcining the support structures loaded with the solids contents of the washcoat suspension.

    摘要翻译: 将洗涂层悬浮液施加到支撑结构的方法。 为了从洗涂层悬浮液开始提供具有大致均匀厚度的涂层,该方法使用设置成通过工艺气体(40)产生支撑结构的流化床的装置(10),其中支撑结构在其中椭圆形或环形地循环 所述方法包括以下步骤:a)用所述支撑结构对所述装置(10)进行充填,并借助于处理气体(40)产生支撑结构流体床,其中所述支撑结构在所述流体床中以椭圆或环形方式循环, 优选环形; b)用修补基面涂层悬浮液浸渍载体结构,通过喷涂在流化床中用洗涂层悬浮液椭圆形或环形循环的支撑结构; c)干燥用洗涂层悬浮液喷涂的支撑结构; 和d)任选地煅烧装载有固体涂料悬浮液的固体含量的载体结构。

    PROCESS FOR PREPARING NANOCRYSTALLINE MIXED METAL OXIDES
    6.
    发明申请
    PROCESS FOR PREPARING NANOCRYSTALLINE MIXED METAL OXIDES 失效
    制备纳米结构金属氧化物的方法

    公开(公告)号:US20100015446A1

    公开(公告)日:2010-01-21

    申请号:US12440303

    申请日:2007-09-07

    申请人: Hans Jörg Wölk

    发明人: Hans Jörg Wölk

    摘要: The present invention relates to a process for the preparation of nanocrystalline mixed metal oxide particles from at least two different starting compounds, comprising the steps of a) introducing a stoichiometric mixture of the starting compounds into a reaction chamber by means of a carrier fluid, b) subjecting the starting compound to a pulsating thermal treatment in a treatment zone under a pulse in the reaction chamber, c) formation of nanocrystalline mixed metal oxide particles, d) the removal from the reactor of the nanocrystalline mixed metal oxide particles obtained in steps b) and c), wherein the stoichiometric mixture of the starting compounds takes place at a temperature of >50° C. Further, the present invention relates to a nanocrystalline mixed metal oxide, in particular for use as a catalyst, obtainable by the process according to the invention.

    摘要翻译: 本发明涉及从至少两种不同的起始化合物制备纳米晶混合金属氧化物颗粒的方法,包括以下步骤:a)通过载体流体将起始化合物的化学计量混合物引入反应室,b )在反应室中以脉冲方式在处理区域进行脉动热处理,c)形成纳米晶混合金属氧化物颗粒,d)从反应器中除去步骤b中获得的纳米晶混合金属氧化物颗粒 )和c),其中起始化合物的化学计量混合物在> 50℃的温度下进行。此外,本发明涉及纳米晶体混合金属氧化物,特别是用作催化剂,可通过以下方法获得: 涉及本发明。

    Laminated pressed articles
    7.
    发明授权

    公开(公告)号:US07135127B2

    公开(公告)日:2006-11-14

    申请号:US10149349

    申请日:2000-12-12

    申请人: Stefan O. Dick

    发明人: Stefan O. Dick

    IPC分类号: H01J7/18

    摘要: A disk-shaped wafer is described which is based on an inorganic sorbent and a binder, with a thickness of less than 700 microns, which can be obtained by pressing a mixture of the inorganic sorbent, about 20 to 60% by weight of the binder and about 10 to 15% by weight water at a pressure of at least 70 MPa; and calcining the resulting green wafer at temperatures of at least about 500° C. until the water content is substantially removed.