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公开(公告)号：US08486580B2
公开(公告)日：2013-07-16
申请号：US12988297
申请日：2008-06-12
IPC分类号： H01M4/00
CPC分类号： H01M8/1226 , H01M4/861 , H01M8/0271 , H01M8/243 , H01M8/2485
摘要： The present invention provides electrochemical device structures having integrated seals, and methods of fabricating them. According to various embodiments the structures include a thin, supported electrolyte film with the electrolyte sealed to the support. The perimeter of the support is self-sealed during fabrication. The perimeter can then be independently sealed to a manifold or other device, e.g., via an external seal. According to various embodiments, the external seal does not contact the electrolyte, thereby eliminating the restrictions on the sealing method and materials imposed by sealing against the electrolyte.
摘要翻译： 本发明提供具有集成密封件的电化学装置结构及其制造方法。 根据各种实施方案，结构包括薄的负载的电解质膜，电解质密封到载体上。 支架的周边在制造过程中是自密封的。 然后可以例如经由外部密封件将周边独立地密封到歧管或其他装置。 根据各种实施例，外部密封件不接触电解质，从而消除了对通过密封电解质施加的密封方法和材料的限制。
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公开(公告)号：US20110053041A1
公开(公告)日：2011-03-03
申请号：US12865956
申请日：2008-02-13
CPC分类号： C22C30/02 , C22C29/12 , C22C32/0021 , H01M4/9066 , H01M8/1253 , H01M2008/1293 , Y02E60/525 , Y02P70/56
摘要： Copper-based cermets and methods of preparing them are provided. The Cu-based cermets have interpenetrating networks of copper alloy and stabilized zirconia that are in intimate contact and display high electronic connectivity through the copper alloy phase. In certain embodiments, methods of preparing the cermets involving sintering a mixture of ceramic and copper-based powders in a reducing atmosphere at a temperature above the melting point of the copper or copper alloy are provided. Also provided are electrochemical structures having the Cu-based cermet, e.g., as an anode structure or a barrier layer between an anode and a metal support. Applications of the cermet compositions and structures include use in high-operating-temperature electrochemical devices, including solid oxide fuel cells, hydrogen generators, electrochemical flow reactors, etc.
摘要翻译： 提供铜基金属陶瓷及其制备方法。 铜基金属陶瓷具有铜合金和稳定化氧化锆的互穿网络，其通过铜合金相紧密接触并显示出高电子连接性。 在某些实施方案中，提供了制备金属陶瓷的方法，所述方法包括在铜或铜合金的熔点以上的温度下在还原气氛中烧结陶瓷和铜基粉末的混合物。 还提供了具有Cu基金属陶瓷的电化学结构，例如阳极结构或阳极和金属载体之间的阻挡层。 金属陶瓷组合物和结构的应用包括用于高工作温度电化学装置，包括固体氧化物燃料电池，氢发生器，电化学流动反应器等。
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公开(公告)号：US07829213B2
公开(公告)日：2010-11-09
申请号：US11796659
申请日：2007-04-27
CPC分类号： H01M8/2425 , H01M8/0202 , H01M8/0297 , H01M8/1226 , H01M8/2483 , Y02P70/56 , Y10T29/4911 , Y10T29/49114
摘要： A pre-fabricated electrochemical device having a dense electrolyte disposed between an anode and a cathode preferably deposited as thin films is bonded to a porous electrically conductive support. A second porous electrically conductive support may be bonded to a counter electrode of the electrochemical device. Multiple electrochemical devices may be bonded in parallel to a single porous support, such as a perforated sheet to provide a planar array. Planar arrays may be arranged in a stacked interconnected array. A method of making a supported electrochemical device is disclosed wherein the method includes a step of bonding a pre-fabricated electrochemical device layer to an existing porous metal or porous metal alloy layer.
摘要翻译： 设置在优选沉积为薄膜的阳极和阴极之间的具有致密电解质的预制电化学装置被接合到多孔导电支撑体上。 第二多孔导电支撑件可以结合到电化学装置的对电极。 多个电化学装置可以与单个多孔载体（例如穿孔板）平行地结合以提供平面阵列。 平面阵列可以布置在堆叠的互连阵列中。 公开了一种制造负载电化学装置的方法，其中该方法包括将预制的电化学装置层接合到现有的多孔金属或多孔金属合金层的步骤。
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公开(公告)号：US07740966B2
公开(公告)日：2010-06-22
申请号：US11512521
申请日：2006-08-30
IPC分类号： H01M8/10
CPC分类号： H01M8/0232 , H01M4/8621 , H01M4/8885 , H01M8/0206 , H01M8/0247 , H01M8/025 , H01M8/0271 , H01M8/0273 , H01M8/04097 , H01M8/1007 , H01M8/2415 , H01M8/243 , H01M8/2484 , H01M2008/1293 , Y02P70/56
摘要： Multiple stacks of tubular electrochemical cells having a dense electrolyte disposed between an anode and a cathode preferably deposited as thin films arranged in parallel on stamped conductive interconnect sheets or ferrules. The stack allows one or more electrochemical cell to malfunction without disabling the entire stack. Stack efficiency is enhanced through simplified gas manifolding, gas recycling, reduced operating temperature and improved heat distribution.
摘要翻译： 多层堆叠的管状电化学电池具有设置在阳极和阴极之间的致密电解质，优选沉积为平行布置在冲压的导电互连片或套圈上的薄膜。 该堆叠允许一个或多个电化学电池故障而不使整个堆叠失效。 通过简化的气体歧管，气体回收，降低的操作温度和改善的热分布来提高堆积效率。
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5.发明申请INTERLOCKING STRUCTURE FOR HIGH TEMPERATURE ELECTROCHEMICAL DEVICE AND METHOD FOR MAKING THE SAME 审中-公开高温电化学装置的互锁结构及其制造方法公开(公告)号：US20100143824A1
公开(公告)日：2010-06-10
申请号：US12664646
申请日：2008-04-15
CPC分类号： H01M8/0232 , H01M4/8657 , H01M4/8889 , H01M8/124 , H01M8/1246 , Y02E60/525 , Y02P70/56
摘要： Layered structures and associated fabrication methods that serve as the foundation for preparing high-operating-temperature electrochemical cells have a porous ceramic layer and a porous metal support or current collector layer bonded by mechanical interlocking which is provided by interpenetration of the layers and/or roughness of the metal surface. The porous layers can be infiltrated with catalytic material to produce a functioning electrochemical electrode.
摘要翻译： 作为制备高工作温度电化学电池的基础的分层结构和相关的制造方法具有多孔陶瓷层和通过机械互锁结合的多孔金属支撑件或集电器层，其通过层间和/或粗糙度相互提供而提供 的金属表面。 多孔层可以用催化材料渗透以产生功能化的电化学电极。
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公开(公告)号：US07670475B2
公开(公告)日：2010-03-02
申请号：US12334776
申请日：2008-12-15
IPC分类号： C25B1/24
CPC分类号： H01M8/124 , B01D53/326 , B01D2257/2027 , Y02P70/56
摘要： A process and apparatus for the electrolytic separation of fluorine from a mixture of gases is disclosed. Also described is the process and apparatus for the generation of fluorine from fluorine/fluoride containing solids, liquids or gases.
摘要翻译： 公开了一种从气体混合物中电解氟分离氟的方法和装置。 还描述了用于从含氟/氟化物的固体，液体或气体产生氟的方法和装置。
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公开(公告)号：US20080131723A1
公开(公告)日：2008-06-05
申请号：US11791269
申请日：2005-11-23
CPC分类号： B23K9/285 , B23K1/0008 , B23K9/291 , C04B37/026 , C04B2237/125 , C04B2237/348 , C04B2237/405 , C04B2237/406 , H01M8/0208 , H01M8/0271 , H01M8/0273 , H01M8/0297 , H01M2008/1293 , Y02P70/56 , Y10T428/12549 , Y10T428/12597
摘要： A CTE modified braze composition that can be utilized to manufacture a strong, gastight joint where at least one of the joining members comprises a ceramic (e.g., a ceramic or a cermet). The braze composition is formulated so as to reduce the thermal stress that results from the mismatch of thermal expansion coefficients between a ceramic joining member and the braze or other joining members. The braze composition comprises a braze alloy in powder, paste or bulk form mixed with one or more particulate or fibrous fillers that exhibit a low (i.e., no more than 6 ppm/K) or negative coefficient of thermal expansion. The braze composition can be used to join members, at least one of which comprises ceramic, and to a composite member produced by joining the two or more members.
摘要翻译： CTE改性的钎焊组合物，其可用于制造强气密接头，其中至少一个接合构件包括陶瓷（例如陶瓷或金属陶瓷）。 配制钎焊组合物以便减少由陶瓷接合部件和钎焊或其它接合部件之间的热膨胀系数失配引起的热应力。 钎焊组合物包括与表现出低（即不超过6ppm / K）或负的热膨胀系数的一种或多种颗粒或纤维填料混合的粉末，糊状或块状的钎焊合金。 钎焊组合物可以用于连接构件，其中至少一个包括陶瓷，以及通过连接两个或更多个构件制成的复合构件。
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8.发明授权公开(公告)号：US06605316B1
公开(公告)日：2003-08-12
申请号：US09626629
申请日：2000-07-27
IPC分类号： B05D512
CPC分类号： H01M4/8885 , B01D53/326 , B01D2257/108 , C25B9/00 , H01M4/9025 , H01M4/9033 , H01M4/905 , H01M4/9066 , H01M8/004 , H01M8/1213 , H01M8/1226 , H01M8/1231 , H01M8/1246 , H01M8/1253 , H01M8/126 , H01M8/1266 , H01M8/2425 , H01M8/243 , H01M8/2483 , H01M2008/1293 , H01M2300/0074 , Y02E60/525 , Y02P70/56 , Y10T29/49115
摘要： Provided are low-cost, mechanically strong, highly electronically conductive porous substrates and associated structures for solid-state electrochemical devices, techniques for forming these structures, and devices incorporating the structures. The invention provides solid state electrochemical device substrates of novel composition and techniques for forming thin electrode/membrane/electrolyte coatings on the novel or more conventional substrates. In particular, in one embodiment the invention provides techniques for co-firing of device substrate (often an electrode) with an electrolyte or membrane layer to form densified electrolyte/membrane films 5 to 20 microns thick. In another embodiment, densified electrolyte/membrane films 5 to 20 microns thick may be formed on a pre-sintered substrate by a constrained sintering process. In some cases, the substrate may be a porous metal, alloy, or non-nickel cermet incorporating one or more of the transition metals Cr, Fe, Cu and Ag, or alloys thereof.
摘要翻译： 提供了低成本，机械强度高的电子导电多孔基底和用于固态电化学装置的相关结构，用于形成这些结构的技术以及结合该结构的装置。 本发明提供了用于在新颖或更传统的基底上形成薄电极/膜/电解质涂层的新型组成和技术的固态电化学装置基板。 特别地，在一个实施例中，本发明提供了用于通过电解质或膜层共同烧制器件衬底（通常为电极）以形成5至20微米厚的致密化电解质/膜膜的技术。 在另一个实施方案中，可以通过约束烧结工艺在预烧结衬底上形成5至20微米厚的致密化电解质/膜膜。 在一些情况下，衬底可以是掺入一种或多种过渡金属Cr，Fe，Cu和Ag的多孔金属，合金或非镍金属陶瓷，或其合金。
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公开(公告)号：US07468120B2
公开(公告)日：2008-12-23
申请号：US11121272
申请日：2005-05-02
CPC分类号： H01M8/124 , B01D53/326 , B01D2257/2027 , Y02P70/56
摘要： A process and apparatus for the electrolytic separation of fluorine from a mixture of gases is disclosed. Also described is the process and apparatus for the generation of fluorine from fluorine/fluoride containing solids, liquids or gases.
摘要翻译： 公开了一种从气体混合物中电解氟分离氟的方法和装置。 还描述了用于从含氟/氟化物的固体，液体或气体产生氟的方法和装置。
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公开(公告)号：US20080268323A1
公开(公告)日：2008-10-30
申请号：US11791270
申请日：2005-11-28
IPC分类号： H01M2/08
CPC分类号： H01M2/08 , B32B2315/02 , C04B35/016 , C04B37/006 , C04B37/026 , C04B2235/3213 , C04B2235/3227 , C04B2237/125 , C04B2237/348 , H01M8/0271 , H01M8/2404 , H01M8/243 , Y02P70/56 , Y10T29/4911
摘要： Several members make up a joint in a high-temperature electrochemical device, wherein the various members perform different functions. The joint is useful for joining multiple cells (generally tubular modules) of an electrochemical device to produce a multi-cell segment-in-series stack for a solid oxide fuel cell, for instance. The joint includes sections that bond the joining members to each other; one or more seal sections that provide gas-tightness, and sections providing electrical connection and/or electrical insulation between the various joining members. A suitable joint configuration for an electrochemical device has a metal joint housing, a first porous electrode, a second porous electrode, separated from the first porous electrode by a solid electrolyte, and an insulating member disposed between the metal joint housing and the electrolyte and second electrode. One or more brazes structurally and electrically connects the first electrode to the metal joint housing and forms a gas tight seal between the first electrode and the second electrode.
摘要翻译： 几个构件在高温电化学装置中构成接头，其中各种构件执行不同的功能。 该接头可用于连接电化学装置的多个电池（通常为管状模块），以产生例如用于固体氧化物燃料电池的多电池段串联堆叠。 接头包括将接合构件彼此接合的部分; 提供气密性的一个或多个密封部分，以及在各种连接部件之间提供电连接和/或电绝缘的部分。 用于电化学装置的合适的接头构造具有金属接头壳体，第一多孔电极，第二多孔电极，通过固体电解质与第一多孔电极分离，以及设置在金属接头壳体和电解质之间的绝缘构件，第二多孔电极 电极。 一个或多个钎焊结构地和电连接第一电极和金属接头壳体，并在第一电极和第二电极之间形成气密密封。
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