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    TUNING NANO-SCALE GRAIN SIZE DISTRIBUTION IN MULTILAYERED ALLOYS ELECTRODEPOSITED USING IONIC SOLUTIONS, INCLUDING Al-Mn AND SIMILAR ALLOYS
    1.
    发明申请
    TUNING NANO-SCALE GRAIN SIZE DISTRIBUTION IN MULTILAYERED ALLOYS ELECTRODEPOSITED USING IONIC SOLUTIONS, INCLUDING Al-Mn AND SIMILAR ALLOYS 有权
    使用离子溶液电沉积的多层合金中的纳米尺寸分布，包括Al-Mn和类似合金

    公开(公告)号：US20140374263A1

    公开(公告)日：2014-12-25

    申请号：US14235834

    申请日：2012-08-02

    申请人： Wenjun Cai ,  Christopher A. Schuh

    发明人： Wenjun Cai ,  Christopher A. Schuh

    IPC分类号： C25D21/12 ,  C25D5/10 ,  C25D3/56

    CPC分类号： C25D21/12 ,  C25D3/56 ,  C25D3/66 ,  C25D3/665 ,  C25D5/10 ,  C25D5/18 ,  C25D17/10

    摘要： Al—Mnx/Al—Mny multilayers with a wide range of structures ranging from microcrystalline to nanocrystalline and amorphous were electrodeposited using a single bath method under galvanostatic control from room temperature ionic liquid. By varying the Mn composition by −1-3 at. % between layers, the grain sizes in one material can be systematically modulated between two values. For example, one specimen alternates between grain sizes of about 21 and 52 nm, in an alloy of average composition of 10.3 at. % Mn. Nanoindentation testing revealed multilayers with finer grains and higher Mn content exhibited better resistance to plastic deformation. Other alloy systems also are expected to be electrodeposited under similar circumstances.

    摘要翻译： 在室温离子液体的恒电流控制下，使用单浴法电沉积具有范围广泛的结构范围从微晶到纳米晶和无定形的Al-Mnx / Al-Mny多层。 通过将Mn组成改变为-13 at。 层之间的％，一种材料中的晶粒尺寸可以在两个值之间进行系统调制。 例如，一个样品在平均组成为10.3英寸的合金中在约21和52nm的晶粒尺寸之间交替。 ％Mn。 纳米压痕测试揭示了具有更细晶粒的多层膜，较高的Mn含量表现出更好的抗塑性变形能力。 预期其他合金系统也将在类似的情况下电沉积。

    SINTERED NANOCRYSTALLINE ALLOYS
    2.
    发明申请
    SINTERED NANOCRYSTALLINE ALLOYS 审中-公开
    烧结纳米晶体合金

    公开(公告)号：US20140271325A1

    公开(公告)日：2014-09-18

    申请号：US14214282

    申请日：2014-03-14

    申请人： Christopher A. Schuh ,  Mansoo Park

    发明人： Christopher A. Schuh ,  Mansoo Park

    IPC分类号： B22F3/10

    CPC分类号： C22C27/04 ,  B22F1/0044 ,  B22F3/10 ,  B22F3/1035 ,  B22F2998/10 ,  C22C1/045 ,  C22C27/06 ,  C22C2200/04

    摘要： Provided in one embodiment is a method, comprising: sintering a plurality of nanocrystalline particulates to form a nanocrystalline alloy, wherein at least some of the nanocrystalline particulates may include a non-equilibrium phase comprising a first metal material and a second metal material, and the first metal material may be soluble in the second metal material. The sintered nanocrystalline alloy may comprise a bulk nanocrystalline alloy.

    摘要翻译： 在一个实施方案中提供了一种方法，其包括：烧结多个纳米晶体微粒以形成纳米晶体合金，其中所述纳米晶体微粒中的至少一些可包括包含第一金属材料和第二金属材料的非平衡相，并且 第一金属材料可溶于第二金属材料。 烧结的纳米晶体合金可以包括块状纳米晶体合金。

    Nanostructured alloy coated threaded metal surfaces and methods of producing same
    4.
    发明申请
    Nanostructured alloy coated threaded metal surfaces and methods of producing same 审中-公开
    纳米结构合金涂层螺纹金属表面及其制造方法

    公开(公告)号：US20100096850A1

    公开(公告)日：2010-04-22

    申请号：US11590241

    申请日：2006-10-31

    申请人： Christopher A. Schuh ,  Pablo A. Castro

    发明人： Christopher A. Schuh ,  Pablo A. Castro

    IPC分类号： F16L25/00 ,  F16B39/00 ,  C25C1/00

    CPC分类号： C25D7/10 ,  C25D5/14 ,  C25D5/18 ,  C25D15/02

    摘要： A method for protecting a threaded metal joint from galling and corrosion includes providing a nanocrystalline coating on the metal surface. The nanocrystalline coating can include a solid or liquid lubricant to protect against wear. Threaded metal joint surfaces coated with the nanocrystalline coating can resist galling under high pressure and high torque, even after several fastening and unfastening operations and also over a long period of time. Protection from corrosion is also provided by the nanocrystalline coating. The method and nanocrystalline coating provide metal surfaces with both lubrication and protection against corrosion. Problems such as removal or leakage, which are associated with protective compounds that use oils, are avoided. The nanocrystalline coatings may be layers of the same material, or layers of differing materials, such as layers with lubricating particles dispersed throughout, and layers without lubricating particles. Such coatings may provide reduced wear, friction, corrosion and galling. Such coated threaded articles are very useful in messy and dirty environments, such as oil production and oil handling industries.

    摘要翻译： 用于保护螺纹金属接头免受磨损和腐蚀的方法包括在金属表面上提供纳米晶体涂层。 纳米晶体涂层可以包括固体或液体润滑剂以防止磨损。 涂覆有纳米晶体涂层的螺纹金属接头表面即使经过多次紧固和松开操作，也可长时间在高压力和高扭矩下可以抵抗磨损。 纳米晶体涂层也提供了防腐蚀。 该方法和纳米晶体涂层为金属表面提供润滑和防腐蚀。 避免与使用油的保护性化合物相关的诸如去除或渗漏的问题。 纳米晶体涂层可以是相同材料或不同材料的层的层，例如具有分散在其中的润滑颗粒的层，以及没有润滑颗粒的层。 这样的涂层可以减少磨损，摩擦，腐蚀和磨损。 这种涂层螺纹制品在混乱和肮脏的环境中非常有用，例如石油生产和油处理行业。

    METHODS FOR THE IMPLEMENTATION OF NANOCRYSTALLINE AND AMORPHOUS METALS AND ALLOYS AS COATINGS
    5.
    发明申请
    METHODS FOR THE IMPLEMENTATION OF NANOCRYSTALLINE AND AMORPHOUS METALS AND ALLOYS AS COATINGS 审中-公开
    纳米晶和非晶态金属和合金作为涂层的实施方法

    公开(公告)号：US20090229984A1

    公开(公告)日：2009-09-17

    申请号：US12401990

    申请日：2009-03-11

    申请人： Christopher A. Schuh ,  Alan C. Lund

    发明人： Christopher A. Schuh ,  Alan C. Lund

    IPC分类号： C25D7/00

    CPC分类号： C25D5/04 ,  C25D3/56 ,  C25D3/562 ,  C25D5/18 ,  C25D7/06 ,  C25D7/0607 ,  C25D7/0614 ,  Y10T428/12014 ,  Y10T428/1216 ,  Y10T428/12174 ,  Y10T428/25 ,  Y10T428/31504

    摘要： Methods for the use of nanocrystalline or amorphous metals or alloys as coatings with industrial processes are provided. Three, specific, such methods have been detailed. One of the preferred embodiments provides a method for the high volume electrodeposition of many components with a nanocrystalline or amorphous metal or alloy, and the components produced thereby. Another preferred embodiment provides a method for application of a nanocrystalline or amorphous coatings in a continuous electrodeposition process and the product produced thereby. Another of the preferred embodiments of the present invention provides a method for reworking and/or rebuilding components and the components produced thereby.

    摘要翻译： 提供了使用纳米晶体或无定形金属或合金作为工业工艺涂层的方法。 三，具体，这些方法已经详细说明了。 其中一个优选实施例提供了一种用纳米晶体或无定形金属或合金的许多部件的高体积电沉积以及由此产生的部件的方法。 另一个优选的实施方案提供了一种在连续电沉积方法中应用纳米晶体或无定形涂层的方法以及由此产生的产品。 本发明的另一个优选实施例提供了一种用于返修和/或重建部件及其制造的部件的方法。

    Method for producing alloy deposits and controlling the nanostructure thereof using negative current pulsing electro-deposition
    6.
    发明申请
    Method for producing alloy deposits and controlling the nanostructure thereof using negative current pulsing electro-deposition 有权
    使用负电流脉冲电沉积法生产合金沉积物并控制其纳米结构的方法

    公开(公告)号：US20090057159A1

    公开(公告)日：2009-03-05

    申请号：US12231918

    申请日：2008-09-08

    申请人： Andrew J. Detor ,  Christopher A. Schuh

    发明人： Andrew J. Detor ,  Christopher A. Schuh

    IPC分类号： C25D3/56

    CPC分类号： C25D5/18 ,  C25D3/56 ,  Y10T428/12493 ,  Y10T428/12771 ,  Y10T428/12806

    摘要： Bipolar current electrodeposits a nanocrystalline grain size. Polarity Ratio relates the absolute value of time integrated amplitude of negative polarity and positive polarity current. Grain size can be controlled in alloys of two or more components, one of which being a metal, and one of which being most electro-active. Typically the more electro-active material is preferentially lessened in the deposit during negative current. The deposit is relatively crack and void free. Grain size is typically a function of deposit composition, which is typically a function of Polarity Ratio. Specified grain size can be achieved by selecting a corresponding Polarity Ratio. Coatings can be in layers, each having a grain size, which can vary layer to layer and also in a graded fashion. A finished article may be built upon a substrate of electro-conductive plastic, or metal, including steels, aluminum, brass. The substrate may remain, or be removed.

    摘要翻译： 双极电流电沉积纳米晶粒度。 极性比与负极性和正极性电流的时间积分幅度的绝对值相关。 可以以两种或多种组分的合金来控制晶粒尺寸，其中一种是金属，其中一种是大多数电活性的。 通常在负电流期间，沉积物中优先减少更多的电活性材料。 沉积物相对破裂和无空隙。 晶粒尺寸通常是沉积物组成的函数，其通常是极性比的函数。 可以通过选择相应的极性比来实现指定的粒度。 涂层可以是层，每层具有粒度，其可以一层到另一层也可以分级地变化。 成品可以建立在导电塑料或金属的基底上，包括钢，铝，黄铜。 衬底可以保留或被移除。

    Articles incorporating alloy deposits having controlled, varying nanostructure
    9.
    发明授权
    Articles incorporating alloy deposits having controlled, varying nanostructure 有权
    含有受控，变化的纳米结构的合金沉积物的制品

    公开(公告)号：US08728630B2

    公开(公告)日：2014-05-20

    申请号：US12317080

    申请日：2008-12-19

    申请人： Andrew J. Detor ,  Christopher A. Schuh

    发明人： Andrew J. Detor ,  Christopher A. Schuh

    IPC分类号： B32B15/01

    CPC分类号： C25D5/18 ,  C25D3/56 ,  Y10T428/12493 ,  Y10T428/12771 ,  Y10T428/12806

    摘要： Bipolar wave current, is used to electrodeposit a nanocrystalline grain size. Polarity Ratio is the ratio of absolute value of time integrated amplitude of negative and positive polarity current. Grain size can be controlled in alloys of two or more components, at least one of which is a metal, and at least one of which is most electro-active. Typically, the more electro-active material is preferentially lessened during negative current. Current density, duration of pulse portions, and bath composition are determined with reference to relations showing grain size as a function of deposit composition, and deposit composition as a function of Polarity Ratio, or a single relation showing grain size as a function of Polarity ratio. A specified size can be achieved by selecting a corresponding Polarity Ratio. Coatings can be layered, each having an average grain size, which can vary layer to layer and also graded through a region.

    摘要翻译： 双极波电流用于电沉积纳米晶粒度。 极性比是负极和正极性电流的时间积分幅度的绝对值之比。 可以以两种或多种组分的合金来控制晶粒尺寸，其中至少一种是金属，并且其中至少一种是最具电活性的。 通常，在负电流期间，优先减少更多的电活性材料。 参考关于显示作为沉积组成的函数的晶粒尺寸和作为极性比的函数的沉积物组成的关系或者表示作为极性比的函数的晶粒尺寸的单一关系的关系来确定电流密度，脉冲部分的持续时间和浴组成 。 可以通过选择相应的极性比来实现指定的尺寸。 涂层可以是层状的，每个具有平均粒度，其可以层间变化，并且还通过区域分级。