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公开(公告)号：US5481033A
公开(公告)日：1996-01-02
申请号：US362334
申请日：1994-12-22
Applicant: Gregory R. Alms , Michael R. Samuels
Inventor： Gregory R. Alms , Michael R. Samuels
IPC: C07C51/50 , C07C51/42 , C07C51/43 , C07C51/487 , C07C63/38
CPC classification number: C07C51/42 , C07C51/487
Abstract: Disclosed is a process for the purification of aromatic dicarboxylic acids in which the salt of an aliphatic diamine and an aromatic dicarboxylic acid is formed in an aqueous solvent, recrystallized, and contacted with an aliphatic dicarboxylic acid in an aqueous solvent such that the aromatic dicarboxylic acid is recoverable in the form of a purified precipitate. The remaining aqueous solute is a salt of the aliphatic diamine and aliphatic dicarboxylic acid and can be used as a starting material in the manufacture of certain polyamides (nylons). The invention is particularly applicable for purifying 2,6-naphthalene dicarboxylic acid, which is difficult otherwise to purify.
Abstract translation: 公开了一种芳族二羧酸的纯化方法，其中脂族二胺和芳族二羧酸的盐在水性溶剂中形成，重结晶，并与脂族二羧酸在水性溶剂中接触，使得芳族二羧酸 可以以纯化的沉淀物的形式回收。 剩余的水溶质是脂族二胺和脂族二羧酸的盐，可用作制造某些聚酰胺（尼龙）的原料。 本发明特别适用于纯化难以净化的2,6-萘二甲酸。
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公开(公告)号：US5466773A
公开(公告)日：1995-11-14
申请号：US396032
申请日：1995-02-28
Applicant: Michael R. Samuels , Marion G. Waggoner
Inventor： Michael R. Samuels , Marion G. Waggoner
CPC classification number: C08G63/605
Abstract: Novel thermotropic liquid crystalline polyesters derived from t-butylhydroquinone, terephthalic acid, 2,6-naphthalene dicarboxylic acid and 4-hydroxybenzoic acid are described. These polymers are useful as molding resins.
Abstract translation: 描述了衍生自叔丁基氢醌，对苯二甲酸，2,6-萘二甲酸和4-羟基苯甲酸的新型热致液晶聚酯。 这些聚合物可用作模制树脂。
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公开(公告)号：US4668454A
公开(公告)日：1987-05-26
申请号：US743903
申请日：1985-06-12
Applicant: Wilton H. Dickerson, Jr. , Che-Hsiung Hsu , Michael R. Samuels
Inventor： Wilton H. Dickerson, Jr. , Che-Hsiung Hsu , Michael R. Samuels
IPC: D01D11/06 , D01F6/62 , D01F6/84 , D06M11/00 , D06M11/13 , D06M13/17 , D06M13/188 , D06M13/192 , D06M13/53 , D06M101/00 , D06M101/16 , D06M101/30 , D06M101/32 , B05D1/00
Abstract: Use of surfactant in coating of yarn from anisotropic melt-forming polyester with alkali metal salts enhances heat-strengthening acceleration effect.
Abstract translation: 使用表面活性剂在各向异性熔融成型聚酯中用碱金属盐涂覆纱线可提高热强化加速效果。
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公开(公告)号：US4180614A
公开(公告)日：1979-12-25
申请号：US861567
申请日：1977-12-16
Applicant: Rudolph J. Angelo , Richard N. Blomberg , Fritz P. Boettcher , Richard M. Ikeda , Michael R. Samuels
Inventor： Rudolph J. Angelo , Richard N. Blomberg , Fritz P. Boettcher , Richard M. Ikeda , Michael R. Samuels
IPC: B05D7/24 , C08G12/08 , C08G69/32 , C08G73/00 , C08G73/08 , C08G73/10 , C08G73/14 , C08J7/04 , B32B27/34 , B32B27/08 , B32B27/28 , B32B27/36
CPC classification number: B05D1/60 , C08G12/08 , C08G69/32 , C08G73/00 , C08G73/08 , C08G73/1028 , C08G73/1067 , C08G73/14 , C08J7/047 , C08J2477/00 , C08J2479/00 , Y10S428/91 , Y10S428/911 , Y10S428/913 , Y10T428/265 , Y10T428/31681 , Y10T428/31736
Abstract: Films, sheets or foils are given a gas-barrier coating of an aromatic polyamide, polyimide, polyamide-imide, polyhydrazide, polyamide-hydrazide, or polyazomethine by direct vapor-phase condensation polymerization of their respective monomers. The monomers are introduced in an inert diluent gas, mixed and reacted in the presence of the surface to be coated. The surface is maintained above the critical minimum deposition temperature of the monomers but below about 300.degree. C. The coating is formed to a thickness between about 0.1 and 0.6 mil.
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公开(公告)号：US06929848B2
公开(公告)日：2005-08-16
申请号：US10227998
申请日：2002-08-26
Applicant: Michael R. Samuels , Subhotosh Khan , Mikhail R. Levit
Inventor： Michael R. Samuels , Subhotosh Khan , Mikhail R. Levit
IPC: B32B5/24 , B29B13/10 , B32B5/28 , B32B15/14 , B32B27/12 , D04H1/00 , D04H13/00 , H01L23/14 , H05K1/03 , B32B3/00 , B32B5/06
CPC classification number: H05K1/0366 , B29B13/10 , B32B15/14 , B32B27/12 , D04H1/4374 , D04H1/4382 , H05K1/036 , H05K2201/0129 , H05K2201/0141 , H05K2201/015 , H05K2201/0251 , H05K2201/0278 , H05K2201/0293 , Y10S428/901 , Y10T428/24917 , Y10T428/249924 , Y10T428/24994 , Y10T428/249941 , Y10T442/30
Abstract: A sheet comprising thermoplastic polymer (TP) and short high tensile modulus fibers, in which the concentration of TP in the middle of the sheet is higher than at the surface of the sheet, useful for making prepregs with a thermoset resin.
Abstract translation: 包含热塑性聚合物（TP）和短的高拉伸模量纤维的片材，其中片材中部的TP浓度高于片材表面的TP浓度，可用于制备具有热固性树脂的预浸料。
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Patent Agency Ranking
公开(公告)号：US5250654A
公开(公告)日：1993-10-05
申请号：US878150
申请日：1992-05-04
Applicant: Gregory R. Alms , Michael R. Samuels , Marion G. Waggoner
Inventor： Gregory R. Alms , Michael R. Samuels , Marion G. Waggoner
IPC: D01F6/84 , B29D99/00 , B29K67/00 , C08G63/60 , C08J5/00 , C08J5/04 , C08J5/18 , C08L67/00 , C08L67/03 , D01F6/92 , C08G63/00 , C08G63/02
CPC classification number: C08G63/605
Abstract: This invention relates to thermotropic liquid crystalline polyester compositions containing recurring units derived from hydroquinone, 4,4'-dihydroxybiphenyl, terephthalic acid, 2,6-naphthalenedicarboxylic acid, 4,4'-bibenzoic acid, and 4-hydroxybenzoic acid which are characterized as having melting points less than 365.degree. C., breaking elongations greater than or equal to 1.5%, and heat distortion temperatures greater than 200.degree. C.This invention further relates to the same compositions containing 20 to 40 weight percent of at least one glass reinforcing/filling agent and which are characterized as having melting points less than 365.degree. C., breaking elongations greater than or equal to 1.8%, and heat distortion temperatures greater than 230.degree. C.The compositions are useful as films, fibers, and shaped or molded articles.
Abstract translation: 本发明涉及含有源自氢醌，4,4'-二羟基联苯，对苯二甲酸，2,6-萘二甲酸，4,4'-二苯甲酸和4-羟基苯甲酸的重复单元的热致液晶聚酯组合物，其特征在于 熔点低于365℃，断裂伸长率大于或等于1.5％，热变形温度大于200℃。本发明还涉及含有20-40重量％的至少一种玻璃增强剂的相同组合物 其特征在于具有小于365℃的熔点，断裂伸长率大于或等于1.8％，热变形温度大于230℃。该组合物可用作膜，纤维和成形或 模制品。
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公开(公告)号：US5115080A
公开(公告)日：1992-05-19
申请号：US602853
申请日：1990-10-24
Applicant: Marion G. Waggoner , Michael R. Samuels
Inventor： Marion G. Waggoner , Michael R. Samuels
IPC: C08G63/18 , C08G63/189 , C08G63/19 , C08G63/191 , C09K19/38
CPC classification number: C08G63/191 , C08G63/189 , C09K19/3838
Abstract: This invention relates to thermotropic liquid crystalline polyester compositions containing recurring units derived from 2-methylhydroquinone, terephthalic acid, 2,6-napthalenecarboxylic acid, and hydroquinone, characterized as having a heat distortion temperature of greater than 200.degree. C. and improved elongation. The inclusion of a reinforcing/filling agent selected from the group consisting of glass reinforcing agents, glass fillers, carbon metasilicate, calcium carbonate, talc, titanium dioxide, and calcined aluminum silicate in said compositions, and also in those same compositions lacking recurring units of hydroquinone, results in an improvement in the elongation of said compositions. The inclusion of carbon fiber into these compositions results in no significant decrease in the elongation of said compositions. The compositions are useful as films, fibers, and shaped articles.
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公开(公告)号：US5110896A
公开(公告)日：1992-05-05
申请号：US625132
申请日：1990-12-10
Applicant: Marion G. Waggoner , Michael R. Samuels
Inventor： Marion G. Waggoner , Michael R. Samuels
CPC classification number: C08G63/605 , C09K19/3809
Abstract: This invention relates to thermotropic liquid crystalline polyester compositions containing recurring units derived from hydroquinone, 4-4'-dihydroxybiphenyl, terephthalic acid, 2,6-naphthalenedicarboxylic acid, and 4-hydroxybenzoic acid which are characterized as having melting points less than 365.degree. C., breaking elongations greater than or equal to 1.5%, and heat distortion temperatures greater than 200.degree. C.This invention further relates to the same compositions containing 20 to 40 weight percent of at least one glass reinforcing/filling agent and which are characterized as having melting points less than 365.degree. C., breaking elongations greater than or equal to 2.0%, and heat distortion temperatures greater than 230.degree. C.The compositions are useful as films, fibers, and shaped or molded articles.
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公开(公告)号：US5525700A
公开(公告)日：1996-06-11
申请号：US423520
申请日：1995-04-17
Applicant: Michael R. Samuels , Marion G. Waggoner
Inventor： Michael R. Samuels , Marion G. Waggoner
CPC classification number: C08J5/18 , C08G63/605 , C08J2367/04 , Y10T428/31786
Abstract: This invention relates to liquid crystalline polymers (LCPs) derived from (I) hydroquinone and/or 4,4'-biphenol and/or bis(4-hydroxylphenyl) ether, (II) terephthalic acid, (lII) 2,6-naphthalene dicarboxylic acid and/or 4,4'-bibenzoic acid, (IV) 4-hydroxybenzoic acid, (V) 6-hydroxy-2-naphthoic acid, and optionally (VI) an aliphatic diol in specified ratios. In addition to forming exceptionally tough films, the LCPs are useful as molding resins or for blending with other thermoplastic polymers.
Abstract translation: 本发明涉及衍生自（I）氢醌和/或4,4'-联苯酚和/或双（4-羟基苯基）醚，（II）对苯二甲酸，（II）2,6-萘的液晶聚合物（LCP） （IV）4-羟基苯甲酸，（V）6-羟基-2-萘甲酸和任选的（Ⅵ）特定比例的脂族二醇。 除了形成非常坚韧的膜之外，LCP可用作模塑树脂或与其它热塑性聚合物共混。
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公开(公告)号：US5397502A
公开(公告)日：1995-03-14
申请号：US72976
申请日：1993-06-10
Applicant: Marion G. Waggoner , Michael R. Samuels , David F. Adcock
Inventor： Marion G. Waggoner , Michael R. Samuels , David F. Adcock
IPC: C09K19/38 , C08G63/60 , C08K3/00 , C08K3/16 , C08K3/20 , C08K3/26 , C08K3/30 , C08K5/098 , C08L67/00 , C08L67/03 , C09K19/52 , C09K19/00 , C08K5/04 , C08G63/00
CPC classification number: C08G63/605 , C08K3/0041 , C09K19/3809 , C09K19/52
Abstract: The heat resistance of polyester liquid crystalline polymers containing repeat units in selected ratios derived from hydroquinone, 4,4'-biphenol, terephthalic acid, 4-hydroxybenzoic acid, and one or both of 4,4'-bibenzoic acid and 2,6-naphthalene dicarboxylic acid is improved by the addition thereto of 15 to 3000 ppm of an alkali metal or 50 to 3000 ppm magnesium or calcium.
Abstract translation: 含有由氢醌，4,4'-联苯酚，对苯二甲酸，4-羟基苯甲酸和4,4'-联苯甲酸和2,6-二羟基苯甲酸中的一种或两者的选定比例的重复单元的聚酯液晶聚合物的耐热性， 通过添加15〜3000ppm的碱金属或50〜3000ppm的镁或钙来改善萘二甲酸。
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