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公开(公告)号：US4106744A
公开(公告)日：1978-08-15
申请号：US768172
申请日：1977-02-14
CPC分类号： H01J49/421 , H01J9/14 , Y10S425/043
摘要： A process for producing mass filters for use in mass spectrometers. Several electrodes having precisely shaped surfaces must be held in precisely determined positions with respect to each other. Insulators are placed into position on the surface of a mandrel and a layer of metal is deposited over the mandrel and insulators to form a composite unitary structure, including the electrodes. The deposited metal overlying the insulators is then removed, electrically isolating the electrodes.
摘要翻译： 生产用于质谱仪的质量过滤器的方法。 具有精确成形表面的几个电极必须相对于彼此保持在精确确定的位置。 将绝缘体放置在心轴表面上的适当位置，并且在心轴和绝缘体上沉积金属层以形成包括电极的复合单一结构。 然后去除覆盖绝缘体的沉积金属，电绝缘电极。
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公开(公告)号：US4040870A
公开(公告)日：1977-08-09
申请号：US588390
申请日：1975-06-19
申请人： Robert A. Holzl
发明人： Robert A. Holzl
CPC分类号： C23C16/00 , C23C28/023
摘要： A method of depositing a hard metal alloy is described wherein a volatile halide of titanium is reduced off the surface of a substrate and then reacted with a volatile halide of boron, carbon or silicon to effect the deposition on a substrate of an intermediate compound of titanium in a liquid phase. The liquid compound on the substrate is then reacted in the presence of hydrogen to produce a hard deposit containing titanium and boron, carbon or silicon. Also described are products which may be produced by the above method.
摘要翻译： 描述了一种沉积硬质合金的方法，其中钛的挥发性卤化物从衬底的表面上被还原，然后与硼，碳或硅的挥发性卤化物反应，以使其沉积在钛的中间体化合物 在液相中。 然后将底物上的液体化合物在氢存在下反应，生成含有钛和硼，碳或硅的硬质沉积物。 还描述了可以通过上述方法制备的产品。
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公开(公告)号：US4008976A
公开(公告)日：1977-02-22
申请号：US570551
申请日：1975-04-30
申请人： Robert A. Holzl
发明人： Robert A. Holzl
CPC分类号： B21D37/205 , B23B27/148 , B23P15/28 , Y10T407/27 , Y10T408/78
摘要： A cutting tool and method for making same are described in which a hard metal alloy coating is thermochemically deposited on the body of the tool to form a long wearing, high strength, layer. At least one cutting edge is machined in the layer.
摘要翻译： 描述了一种切割工具及其制造方法，其中将硬质合金涂层热固化沉积在工具的主体上以形成长的穿着，高强度的层。 在该层中至少加工一个切削刃。
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公开(公告)号：US4591514A
公开(公告)日：1986-05-27
申请号：US701065
申请日：1985-02-13
申请人： Robert A. Holzl
发明人： Robert A. Holzl
CPC分类号： C04B41/87 , C04B41/5053 , C04B41/52 , C04B41/89
摘要： A method of forming a coated article is described. The article is composed of a carbon body having a thermochemically deposited coating which renders the body resistant to oxidation at high temperatures. A volatile gaseous halide of silicon is partially reduced to form a lower halide in a first reaction zone having a first pressure and separated from the body. The lower halide is flowed into a second reaction zone maintained at a pressure lower than the pressure in the first reaction zone. A gaseous alloying agent is introduced into the second reaction zone. The agent includes one or more elements selected from the group consisting of carbon, oxygen, aluminum, and nitrogen. As a consequence, a liquid phase intermediate compound is deposited on the substrate body which is thereafter thermochemically reacted to produce a coating of the silicon alloy. The coating has a non-columnar grain distribution with substantially equiaxial grains of an average diameter of less than one micron and forms a correspondingly fine crack mosaic upon stressing due to differences in thermal coefficients of expansion between the coating and the body. The lower halide and the alloying agent are controlled so as to produce a coating wherein the amount of silicon is substantially in excess of stoichiometry.
摘要翻译： 描述形成涂层制品的方法。 该制品由具有热化学沉积涂层的碳体组成，其使得机体耐高温氧化。 部分还原硅的挥发性气态卤化物，以在具有第一压力并与体分离的第一反应区中形成较低的卤化物。 较低的卤化物流入维持在低于第一反应区的压力的压力的第二反应区。 将气态合金剂引入第二反应区。 该试剂包括一种或多种选自碳，氧，铝和氮的元素。 因此，液相中间体化合物沉积在基板主体上，然后热化学反应以产生硅合金的涂层。 该涂层具有非圆柱形晶粒分布，其平均直径小于1微米的基本上等轴晶粒，并且由于涂层和体之间的热膨胀系数的差异而在应力时形成相应的细裂纹马赛克。 控制下卤化物和合金剂以产生其中硅的量基本上超过化学计量的涂层。
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公开(公告)号：US4079254A
公开(公告)日：1978-03-14
申请号：US768174
申请日：1977-02-14
CPC分类号： H01J49/421 , H01J9/14 , Y10S425/043
摘要： A process for producing mass filters for use in mass spectrometers. Several electrodes having precisely shaped surfaces must be held in precisely determined positions with respect to each other. Insulators are placed into position on the surface of a mandrel and a layer of metal is deposited over the mandrel and insulators to form a composite unitary structure, including the electrodes. The deposited metal overlying the insulators is then removed, electrically isolating the electrodes.
摘要翻译： 生产用于质谱仪的质量过滤器的方法。 具有精确成形表面的几个电极必须相对于彼此保持在精确确定的位置。 将绝缘体放置在心轴表面上的适当位置，并且在心轴和绝缘体上沉积金属层以形成包括电极的复合单一结构。 然后去除覆盖绝缘体的沉积金属，电绝缘电极。
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公开(公告)号：US5076982A
公开(公告)日：1991-12-31
申请号：US103613
申请日：1987-10-01
CPC分类号： C04B38/0006 , A63C5/12 , C04B38/0695 , C04B41/4505 , C04B41/81 , C23C16/325 , C23C16/345
摘要： A method for making a lightweight structure having a high stiffness to weight ratio comprising providing a substrate defining at least a pair of outer surfaces spaced from each other, boring at least one hole through the structure to provide at least one void passage extending through the substrate between the outer surfaces, coating the outer surfaces of the substrate and the surfaces of the passage with a chemical vapor deposited material to a thickness of about one millimeter, plugging the void passage with a plug of a substrate material, and further coating the coated outer surfaces of the substrate and the ends of the plugs with a chemical vapor deposited material to form a continuous monolithic structure thereon.
摘要翻译： 一种用于制造具有高刚性重量比的轻质结构的方法，包括提供限定至少一对彼此间隔开的一对外表面的基底，镗孔穿过所述结构的至少一个孔，以提供延伸穿过所述基底的至少一个空隙通道 在外表面之间，用化学气相沉积材料将衬底的外表面和通道的表面涂覆至约1毫米的厚度，用空心通道用衬底材料的塞子堵塞，并进一步涂覆涂覆的外部 用化学气相沉积材料将基片的表面和塞的端部形成在其上的连续的整体结构。
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公开(公告)号：US4716064A
公开(公告)日：1987-12-29
申请号：US793828
申请日：1985-10-31
IPC分类号： B32B3/24 , A63C5/12 , B32B3/12 , B32B3/30 , C04B38/00 , C04B38/06 , C04B41/45 , C04B41/81 , C23C16/32 , C23C16/34
CPC分类号： C04B41/009 , A63C5/12 , C04B38/0006 , C04B38/0695 , C04B41/4505 , C04B41/81 , C23C16/325 , C23C16/345 , Y10T428/236 , Y10T428/24157 , Y10T428/24174
摘要： A composite structure having a high stiffness to weight ratio includes a substrate, e.g. graphite, defining at least a pair of outer surfaces which are spaced from each other and having a volume or void passages extending through the substrate between the outer surfaces. At least one stiffening element extends between the outer surfaces within this volume. The stiffening element defines a volume and has at least one wall intersecting each of the outer surfaces. The stiffening element and the outer surfaces are made up of a chemically vapor deposited material having the desired high stiffness to weight ratio and being formed as a monolithic structure having a thickness of at least about 1 millimeter. These structures have such diverse uses as aircraft parts and skis.
摘要翻译： 具有高刚度和重量比的复合结构包括基底，例如， 石墨，限定至少一对彼此间隔开的外表面，并具有在外表面之间延伸通过基底的体积或空隙通道。 至少一个加强元件在该体积内的外表面之间延伸。 加强元件限定体积并且具有与每个外表面相交的至少一个壁。 加强元件和外表面由化学气相沉积材料制成，具有所需的高刚度和重量比，并且形成为具有至少约1毫米厚度的整体结构。 这些结构具有诸如飞机部件和滑雪板的多种用途。
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公开(公告)号：US4515860A
公开(公告)日：1985-05-07
申请号：US416628
申请日：1982-09-10
申请人： Robert A. Holzl
发明人： Robert A. Holzl
IPC分类号： B32B9/00 , C01B31/36 , C04B41/50 , C04B41/52 , C04B41/87 , C04B41/88 , C04B41/89 , C23C11/00 , C23C11/08
CPC分类号： C04B41/009 , C04B41/5053 , C04B41/52 , C04B41/87 , C04B41/89 , Y10T428/2916 , Y10T428/2918 , Y10T428/292 , Y10T428/2933 , Y10T428/2962 , Y10T428/30
摘要： A coated article and method of forming the same. The article is composed of a carbon body having a thermochemically deposited coating which renders the body resistant to oxidation at high temperatures. The coating is formed of a silicon alloy having a non-columnar grain distribution with substantially equiaxial grains of an average diameter of less than one micron. The amount of silicon in the coating is in excess of the alloy stoichiometry, producing infusion of silicon, with such at or above its melting temperature, into the cracked mosaic of the coating, to form an oxidative resistant glass filler.
摘要翻译： 涂布制品及其形成方法。 该制品由具有热化学沉积涂层的碳体组成，其使得机体耐高温氧化。 该涂层由具有平均直径小于1微米的基本上等轴晶粒的非柱状晶粒分布的硅合金形成。 涂层中硅的量超过合金化学计量，在其熔融温度等于或大于其熔融温度下产生硅浸入到涂层的裂纹马赛克中，以形成耐氧化玻璃填料。
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公开(公告)号：US4239819A
公开(公告)日：1980-12-16
申请号：US968074
申请日：1978-12-11
申请人： Robert A. Holzl
发明人： Robert A. Holzl
IPC分类号： C04B41/50 , C04B41/87 , C23C16/30 , C23C16/32 , C23C16/34 , C23C16/38 , C23C16/42 , C23C16/448 , C30B25/02 , C23C11/08
CPC分类号： C04B41/009 , C04B41/5053 , C04B41/87 , C23C16/303 , C23C16/32 , C23C16/325 , C23C16/345 , C23C16/38 , C23C16/42 , C23C16/4481 , C23C16/4488 , C30B25/02 , C30B29/605 , Y10T428/12576 , Y10T428/12667 , Y10T428/12674 , Y10T428/12826 , Y10T428/256 , Y10T428/31678
摘要： A method of depositing a hard, fine grained metal or semi-metal alloy is described wherein a volatile halide of the metal or semi-metal is partially reduced and then deposited as a liquid phase intermediate compound onto a substrate in the presence of an alloying gas. The liquid phase deposited on the substrate is then thermochemically reacted to produce the hard, fine grained alloy. Also described are products which may be produced by the above method.
摘要翻译： 描述了沉积硬的细粒金属或半金属合金的方法，其中金属或半金属的挥发性卤化物被部分还原，然后在合金气体存在下作为液相中间体化合物沉积到基底上 。 然后将沉积在基底上的液相热化学反应以产生硬的细晶粒合金。 还描述了可以通过上述方法制备的产品。
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公开(公告)号：US4202080A
公开(公告)日：1980-05-13
申请号：US25568
申请日：1979-03-30
CPC分类号： H01J49/421 , C23C16/01 , H01J9/14 , Y10T29/4981 , Y10T29/49982
摘要： A process for producing mass filters for use in mass spectrometers. Several electrodes having precisely shaped surfaces must be held in precisely determined positions with respect to each other. Insulators are placed into position on the surface of a mandrel and a layer of metal is deposited over the mandrel and insulators to form a composite unitary structure, including the electrodes. The deposited metal overlying the insulators is then removed, electrically isolating the electrodes.
摘要翻译： 生产用于质谱仪的质量过滤器的方法。 具有精确成形表面的几个电极必须相对于彼此保持在精确确定的位置。 将绝缘体放置在心轴表面上的适当位置，并且在心轴和绝缘体上沉积金属层以形成包括电极的复合单一结构。 然后去除覆盖绝缘体的沉积金属，电绝缘电极。
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